Cryogen-free scanning gate microscope for the characterization of Si/Si0.7Ge0.3 quantum devices at milli-Kelvin temperatures

Silicon can be isotopically enriched, allowing for the fabrication of highly coherent semiconductor spin qubits. However, the conduction band of bulk Si exhibits a six-fold valley degeneracy which may adversely impact the performance of silicon quantum devices. To date, the spatial characterization of valley states in Si has remained limited. Moreover, techniques for probing valley states in functional electronic devices are needed. Here, we describe a cryogen-free scanning gate microscope for the characterization of Si/Si0.7Ge0.3 quantum devices at mK temperatures. The newly built instrument is the first cryogen-free scanning gate microscope capable of forming and measuring a quantum dot on a Si/SiGe device with an overlapping gate structure without compromising the ability to host multiple DC and microwave lines for quantum control experiments. The microscope is based on the Pan-walker design, with coarse positioning piezostacks and a fine scanning piezotube. A tungsten microscope tip is attached to a tuning fork for active control of the tip-to-sample distance. To reduce vibration noise from the pulse tube cooler, we utilize both active and passive vibration isolation mechanisms and achieve a root-mean-square noise in z of ∼2 nm. Our microscope is designed to characterize fully functioning Si/Si0.7Ge0.3 quantum devices. As a proof of concept, we use the microscope to manipulate the charge occupation of a Si quantum dot, opening up a range of possibilities for the exploration of quantum devices and materials.