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Performance of mechanochemically activated supplementary cementitious materials in cement pastes and mortars

Sofiane Amroun, Anagha Iyer, Prannoy Suraneni

Abstract Mechanochemical activation (MCA) is a rapidly emerging technology for producing supplementary cementitious materials (SCMs). However, performance data on MCA SCMs is lacking. Here, we investigated the potential use of four low-grade materials as sources of alternative SCMs following MCA treatment. The studied materials were municipal solid waste incineration bottom ash…

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Toward continuous shrinkage measurement of poured earth: practical setup and underlying shrinking mechanisms

Yi Du, Ellina Bernard, Janis Justs, Guillaume Habert et al.

Abstract Continuous shrinkage measurement in earth-based materials remains technically challenging, particularly for high-water-content mixtures with low initial stiffness. In this study, a semi-cylindrical experimental setup, combined with digital image correlation (DIC) for measurements of surface strains and a linear variable differential transformer (LVDT) for interior stra…

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Materials and Structures·2026Open access
Interlaboratory evaluation of experimental setups for textile reinforcements

Jonas De Wachter, Pegah Zare, Julian Konzilia, Lazar Azdejkovic et al.

Abstract Reliable test methods that provide reproducible results are essential for the mechanical characterisation and standardisation of textile reinforced concrete (TRC). This paper presents the results of an interlaboratory study comprising uniaxial tensile tests and bond tests on TRC with various textile configurations. All laboratories conducted the experiments in accordan…

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Materials and Structures·2026Open access
Sugarcane bagasse ash as an alkali activator: production and characterization of geopolymer mortars with partial sodium silicate replacement

Lívia Costa da Silva, Afonso Rangel Garcez de Azevedo, Markssuel Teixeira Marvila, Carlos Maurício Fontes Vieira

Abstract Portland cement production accounts for about 9% of global CO 2 emissions, underscoring the need for alternative materials with a lower environmental impact. In this context, geopolymers emerge as a promising option, offering good mechanical performance, chemical stability, and a reduced carbon footprint. Among the residues with potential for geopolymer applications is…

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Materials and Structures·2026Open access
Chemo-morphological evaluation of the blending behaviour of PMB and polymer-modified RAP binder

Isabeau Kokken, Bowen Li, Antonio Roberto, Johannes Mirwald et al.

Abstract Polymer-modified reclaimed asphalt pavement (PM-RAP) is increasingly available for recycling, but the complex ageing and degradation of styrene-butadiene-styrene (SBS)-modified binders hinder its effective reuse in surface layers. This paper aims to understand the chemo-morphological blending behaviour between aged PM-RAP binders and fresh polymer-modified bitumen (PMB…

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Materials and Structures·2026Open access
Mechanical and microstructural properties of user-friendly one-part alkali-activated mortars via low-grade calcined clay

Oğuzhan Öztürk, Jitong Zhao, Cesare Signorini, Thomas Köberle et al.

Abstract Alkali-activated materials (AAMs) have emerged as a promising alternative to traditional cement-based binders. However, their adoption is restricted by non-user-friendly production processes, the need for curing at elevated temperatures when higher amounts of aluminosilicate sources are used and the limited availability or regional dependency of precursors and activato…

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Materials and Structures·2026Open access
Chemo‑mechanical assessment of ageing and performance trade‑offs in bio‑based rejuvenators for RAP‑rich binders

Ali Foroutan Mirhosseini, Arman Hamidi, Thor Asbjørn Lunaas

Abstract This study investigates the ageing behavior and performance trade‑offs of three bio‑based rejuvenators (namely, Anova, Sylvaroad, and Tall‑Oil Pitch (TOP)) in a 30% RAP binder system using a chemo‑mechanical framework combining Linear Amplitude Sweep (LAS), Multiple Stress Creep Recovery (MSCR) and Fourier Transform Infrared (FTIR). All binders were evaluated after sho…

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Materials and Structures·2026Open access
Partial replacement of asphalt binder with heavy fraction of hydrothermal liquefaction bio-crude oil

Mahsa Tofighian, Ramez Hajj

Abstract Growing interest in the use of bio-derived materials in asphalt pavements is driven by their potential cost benefits and environmental sustainability. Among emerging technologies, hydrothermal liquefaction (HTL) has shown significant potential for converting wet biomass to bio-oil. This study evaluates the potential of bio-asphalt from HTL to partially replace conventi…

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Materials and Structures·2026Open access
Development of sustainable hydraulic lime mortars with the incorporation of rice husk ash for the conservation of cultural heritage

Maria Antonietta Zicarelli, Marta Caroselli, Francesco Parisi, Michela Ricca et al.

Abstract This research investigates the potential utilization of rice husk ash (RHA), an agricultural by-product, in lime-based mortars for the conservation of cultural heritage. While RHA has been extensively studied as a supplementary cementitious material in the construction sector, its application in lime-based mortars for the conservation of historic surfaces remains large…

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Materials and Structures·2026Open access
Multiscale characterization of Arroyo del Toro limestone under varying moisture conditions: correlation between dynamic and static elastic moduli for structural assessment

Carlos Garduño, Pablo Pachón, Víctor Compán, Felipe García-Sánchez

Abstract The mechanical characterization of natural stone under varying moisture conditions is a critical issue for structural assessment, particularly when only non-destructive techniques are feasible. This study aims to characterize the Arroyo del Toro limestone and to establish reliable relationships between dynamic and static elastic moduli for application in finite element…

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Materials and Structures·2026Open access
Improved pumpability in 3D concrete printing using vibration induced active rheology control

Nilusha Nissanka, Pathmanathan Rajeev, Jay Sanjayan

Abstract In 3D concrete printing (3DCP), achieving rapid development of high static yield stress after extrusion is critical to ensure buildability for preventing collapse of freshly printed concrete. Commonly, this is achieved by incorporating buildability enhancing additives during the initial mixing stage. However, high dosage of such additives often increases flow resistanc…

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