journal article·2026-02-16Open access

Effects of Provisional Cement Cleaning Methods on Resin–Dentin Bond Strength Following Immediate Dentin Sealing with Different Adhesive Systems

Zeynep Aydin, Cemile Kedici Alp, Osman F. Aydin

Abstract

This study evaluated the effects of different provisional luting cement removal methods on the shear bond strength (SBS) of resin cement to dentin following immediate dentin sealing (IDS) performed with two adhesive systems. A total of 168 extracted, caries-free human third molars were used, of which 144 were allocated for SBS testing and 24 for scanning electron microscopy (SEM) analysis. Specimens were assigned according to the IDS protocol (no IDS, IDS with OptiBond FL, or IDS with G2-Bond), followed by provisional cementation using an eugenol-free temporary cement. Contaminated surfaces were subsequently cleaned with a hand scaler, aluminum oxide (Al2O3) air abrasion, or Katana Cleaner prior to final bonding with a dual-cure resin cement. SBS was measured after 24 h of water storage, and surface morphology was evaluated by SEM at 2500× magnification. IDS significantly increased SBS under uncontaminated conditions, with G2-Bond-based IDS exhibiting higher bond strength values than specimens without IDS. However, provisional cement contamination significantly reduced SBS regardless of the cleaning method applied, and none of the tested protocols fully restored the bond strength observed in uncontaminated IDS-treated dentin. SEM analysis revealed residual cement remnants and surface alterations after cleaning, even in specimens that appeared macroscopically clean. Within the limitations of this in vitro study, IDS enhances resin–dentin bonding when contamination is avoided; however, current mechanical and chemical cleaning methods are insufficient to completely recover bond strength compromised by provisional cement contamination, highlighting the importance of preventing contamination and preserving IDS layer integrity during indirect restorative procedures.
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Research context

OpenAlex topics: Dental materials and restorations · Endodontics and Root Canal Treatments · Dental Erosion and Treatment

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

Department of Restorative Dentistry, Faculty of Dentistry, Gazi University, Emek, Ankara 06490, Türkiye

Department of Restorative Dentistry, Faculty of Dentistry, Ankara Medipol University, Çankaya, Ankara 06570, Türkiye

Funding

Gazi University Scientific Research Projects Coordination Unit

References (41)

Show source-provided references
1. Evaluating Residual Dentin Thickness Following Various Mandibular Anterior Tooth Preparations for Zirconia Full-Coverage Single Crowns: An In Vitro Analysis10.11607/prd.1873 ↗
2. The Prosthetic Workflow in the Digital Era10.1155/2016/9823025 ↗
3. Critical Appraisal: Immediate Dentin Sealing for Indirect Bonded Restorations10.1111/j.1708-8240.2008.00232.x ↗
4. Effect of Provisional Cements on the Bond Strength of Various Adhesive Bonding Systems on Dentine10.1111/j.1365-2842.1997.tb00253.x ↗
5. Immediate Dentin Sealing: Effect of Sandblasting on the Layer Thickness
6. Immediate Dentin Sealing: A Fundamental Procedure for Indirect Bonded Restorations10.1111/j.1708-8240.2005.tb00103.x ↗
7. Immediate Dentin Sealing: A Literature Review10.2147/CCIDE.S307939 ↗
8. Adhesive Sealing of Dentin Surfaces In Vitro: A Review
9. Immediate Dentin Sealing Improves Bond Strength of Indirect Restorations10.1016/j.prosdent.2005.10.010 ↗
10. Significance of Immediate Dentin Sealing and Flowable Resin Coating Reinforcement for Unfilled or Lightly Filled Adhesive Systems10.1111/jerd.12700 ↗
11. Influence of Temporary Cement Contamination on Surface Free Energy and Dentin Bond Strength of Self-Adhesive Cements10.1016/j.jdent.2011.11.012 ↗
12. Influence of Temporary Cements on the Bond Strength of Self-Adhesive Cement to the Metal Coronal Substrate10.1590/0103-6440201300362 ↗
13. In Vivo Evaluation of Three Cleansing Techniques for Prepared Abutment Teeth10.1067/mpr.2002.128123 ↗
14. Effect of Zinc Oxide-Eugenol on the Shear Bond Strength of a Commonly Used Bonding System10.1034/j.1600-9657.2000.016006265.x ↗
15. Effect of Dentin Contamination with Hemostatic Agents and Cleaning Techniques on Bonding with Self-Adhesive Resin Cement10.12659/MSM.943353 ↗
16. (2022). Adhesives—Designation of Main Failure Patterns. Standard No. ISO 10365:2022. Available online: https://cdn.standards.iteh.ai/samples/80800/cc2769b3d44a498dbe129fa08906f944/ISO-10365-2022.pdf.
17. Effect of Immediate Dentin Sealing on the Shear Bond Strength of Resin Cement to Porcelain Restoration10.4047/jap.2010.2.2.39 ↗
18. Immediate Dentin Sealing Supports Delayed Restoration Placement10.1016/S0022-3913(07)60052-3 ↗
19. GC Corporation (2024, December 18). G2-Bond Universal Comprehensive Guide. Available online: https://www.gc.dental/europe/sites/europe.gc.dental/files/products/downloads/g2bonduniversal/manual/MAN_g2bonduniversal_Comprehensive_Guide_en.pdf.
20. Brkanović, S., Sever, E.K., Vukelja, J., Ivica, A., Miletić, I., and Krmek, S.J. (2023). Comparison of Different Universal Adhesive Systems on Dentin Bond Strength. Materials, 16.10.3390/ma16041530 ↗
21. Effect of Long-Term Storage on Nanomechanical and Morphological Properties of Dentin–Adhesive Interfaces10.1016/j.dental.2014.11.010 ↗
22. Adhesion–Decalcification Mechanisms of Acid Interactions with Human Hard Tissues10.1002/jbm.1216 ↗
23. High-Resolution Mechanical Mapping of the Adhesive–Dentin Interface: Effect of Co-Monomers in 10-MDP10.1016/j.jmbbm.2021.104389 ↗
24. Adhesive Interfacial Characteristics and Related Bonding Performance of Four Self-Etching Adhesives with Different Functional Monomers Applied to Dentin10.1016/j.jdent.2017.05.010 ↗
25. Can the Hydrophilicity of Functional Monomers Affect Chemical Interaction?10.1177/0022034513514587 ↗
26. Water Absorption of Poly(methyl methacrylate) Containing 4-Methacryloxyethyl Trimellitic Anhydride10.1016/S0142-9612(02)00521-5 ↗
27. Development of MDP-Based One-Step Self-Etch Adhesive: Effect of Additional 4-META on Bonding Performance10.4012/dmj.2012-179 ↗
28. Monomer-Solvent Phase Separation in One-Step Self-Etch Adhesives10.1177/154405910508400214 ↗
29. Systematic Review of the Chemical Composition of Contemporary Dental Adhesives10.1016/j.biomaterials.2007.04.044 ↗
30. Effect of Eugenol-Containing and Eugenol-Free Temporary Cements on Microleakage in Resin-Bonded Restorations
31. Effect of Mechanical and Air-Particle Cleansing Protocols of Provisional Cement on Immediate Dentin Sealing Layer and Subsequent Adhesion of Resin Composite Cement10.1080/01694243.2015.1087254 ↗
32. Removal of Temporary Cements Following an Immediate Dentin Hybridization Approach: Comparison of Mechanical and Chemical Cleaning Methods10.1080/01694243.2017.1381015 ↗
33. Microtensile Bond Strength of Prehybridized Dentin: Storage Time and Surface Treatment Effects
34. Immediate Dentin Sealing of Onlay Preparations: Thickness of Pre-Cured Dentin Bonding Agent and Effect of Surface Cleaning
35. Effects of Tooth Preparation Cleansing Protocols on the Bond Strength of Self-Adhesive Resin Luting Cement to Contaminated Dentin10.2341/07-141 ↗
36. Effect of Decontamination Materials on Bond Strength of Saliva-Contaminated CAD/CAM Resin Block and Dentin10.4012/dmj.2021-268 ↗
37. MDP Is Effective for Removing Residual Polycarboxylate Temporary Cement as an Adhesion Inhibitor10.4012/dmj.2020-132 ↗
38. Effectiveness of Different Cleaning Measures on the Bonding of Resin Cement to Saliva- or Blood-Contaminated Zirconia10.1016/j.jdent.2022.104084 ↗
39. Effect of Curing Conditions on the Dentin Bond Strength of Two Dual-Cure Resin Cements10.1016/j.jpor.2016.12.012 ↗
40. Shear bond strength of a self-adhesive resin cement to dentin surface treated with Nd:YAG and femtosecond lasers10.1007/s10103-020-03138-4 ↗
41. Influence of surface pretreatment on the bond strength of a resin luting cement to saliva-contaminated enamel and dentin10.2341/23-170-L ↗