Influence of different heat treatment programs on properties of sol–gel synthesized (Na0·5K0·5)NbO3 (KNN) thin films
Source abstract
Abstract
Thin films of (Na0·5K0·5)NbO3 (KNN) were synthesized on Pt/Ti/SiO2/Si substrates with repeated spin-coating after fabrication of the precursor solution by a sol–gel process. The KNN precursor solution was prepared from K- and Na-acetate, Nb-pentaethoxide and 1,3-propanediol. Based on three characteristic temperatures derived from thermal analysis (TG–DTA) experiments, five heat treatment programs were developed. All programs lead to single phase perovskite KNN films with random crystal orientation, but only the programs that included a treatment after each single spin-coating step provided pore free surfaces with grains of about 100 nm size. The lowest leakage current at 150 kV cm − 1 was obtained for the temperature program that included pyrolysis and calcination steps after each deposited layer.
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Research context
OpenAlex topics: Ferroelectric and Piezoelectric Materials · Microwave Dielectric Ceramics Synthesis · Multiferroics and related materials
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
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