Surface modification of titanium hydride with epoxy resin via microwave-assisted ball milling
Source abstract
Abstract
Abstract Surface modification of titanium hydride with epoxy resin was carried out via microwave-assisted ball milling and the products were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), thermo-gravimetry (TG) and Fourier transform infrared spectroscopy (FT-IR). A sedimentation test was performed to investigate the compatibility of the modified nano titanium hydride with the epoxy resin. The results show that the epoxy resin molecules were grafted on the surface of nano titanium hydride particles during the microwave-assisted ball milling process, which led to the improvement of compatibility between the nanoparticles and epoxy resin. According to the FT-IR, the grafting site was likely to be located around the epoxy group due to the fact that the epoxy ring was opened. However, compared with microwave-assisted ball milling, the conventional ball milling could not realize the surface modification, indicating that the coupling effect of mechanical force and microwave played a key role during the process.
Source: openaire · Quality: candidate unverified · Source record ↗
Research context
OpenAlex topics: Advanced materials and composites · Metal and Thin Film Mechanics · Advanced ceramic materials synthesis
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (29)
Show source-provided references
1. Surface modification of inorganic nanoparticles for development of organic–inorganic nanocomposites – a review10.1016/j.progpolymsci.2013.02.003 ↗
2. Corrosion protection of steel by epoxy nanocomposite coatings containing various combinations of clay and nanoparticulate zirconia10.1016/j.corsci.2013.05.024 ↗
3. Surface modification of magnesium aluminum hydroxide nanoparticles with poly(methyl methacrylate) via one-pot in situ polymerization10.1016/j.apsusc.2011.10.059 ↗
4. Surface modification of iron particles with polystyrene and surfactants under high-energy ball milling10.1016/j.surfcoat.2013.10.030 ↗
5. Development and characterization of phosphorus-containing siliconized epoxy resin coatings10.1016/j.porgcoat.2009.04.004 ↗
6. Homogeneous nanoparticle dispersion prepared with impurity-free dispersant by the ball mill technique10.1016/j.partic.2013.01.001 ↗
7. Tensile and tribological behaviors of PEEK/nano-SiO2 composites compounded using a ball milling technique10.1016/j.compscitech.2008.06.027 ↗
8. Effects of ball milling dispersion of nano-SiOx particles on impact strength and crystallization behavior of nano-SiOx-poly(phenylene sulfide) nanocomposites10.1002/pen.20547 ↗
9. Using high-temperature mechanochemistry treatment to modify iron oxide and improve the corrosion performance of epoxy coating – I. High-temperature ball milling treatment
10. Using high-temperature mechanochemistry treatment to modify iron oxide and improve the corrosion performance of epoxy coating – II. Effect of grinding temperature
11. Kinetics of microwave-assisted polymerization of ɛ-caprolactone10.1002/app.13318 ↗
12. Mechanical and morphological properties of fly ash/epoxy composites using conventional thermal and microwave curing methods10.1016/j.compscitech.2007.01.016 ↗
13. Rapid N-phthaloylation of chitosan by microwave irradiation10.1016/j.carbpol.2004.04.009 ↗
14. Comparison of the mechanical and physical properties of a carbon fibre epoxy composite manufactured by resin transfer moulding using conventional and microwave heating10.1016/j.compscitech.2008.01.010 ↗
15. Experimental studies on comparison of microwave curing and thermal curing of epoxy resins used for alternative mould materials10.1016/j.jmatprotec.2004.04.248 ↗
16. Microwave-assisted polymerization of d-, l-lactide with stannous octanoateas catalyst
17. Microwave-assisted ring-opening polymerization of ɛ-caprolactone10.1002/pola.10256 ↗
18. Ring-opening polymerization of ɛ-caprolactam and ɛ-caprolactone via microwave irradiation10.1002/pola.10306 ↗
19. Microwave-assisted graft copolymerization of 3-caprolactone onto chitosan via the phthaloyl protection method10.1016/j.carbpol.2005.01.009 ↗
20. A low temperature synthesis of MnFe2O4 nanocrystals by microwave-assisted ball-milling10.1016/j.cej.2012.10.061 ↗
21. Preparation of high saturation magnetic MgFe2O4 nanoparticles by microwave-assisted ball milling10.1016/j.matlet.2012.05.034 ↗
22. Coupling effect of microwave and mechanical forces during the synthesis of ferrite nanoparticles by microwave-assisted ball milling10.1021/ie401890j ↗
23. Surface modification of ultrafine precipitated silica with 3-methacryloxypropyltrimethoxysilane in carbonization process10.1016/j.colsurfa.2012.11.057 ↗
24. Scanning electron microscopy, X-ray diffraction and thermal analysis study of the TiH2 foaming agent10.1016/j.matchar.2012.07.005 ↗
25. Effect of NiLaxFe2−xO4 nanoparticles on the thermal and coating properties of epoxy resin composites10.1016/j.compositesb.2013.02.023 ↗
26. Pyrolysis and fire behaviour of epoxy resin composites based on a phosphorus-containing polyhedral oligomeric silsesquioxane (DOPO-POSS)10.1016/j.polymdegradstab.2011.07.014 ↗
27. Aminealkylthiol and dithiol self-assembly as adhesion promoter between copper substrate and epoxy resin10.1016/j.apsusc.2011.07.080 ↗
28. Interfacial effect of surface modified TiO2 and SiO2 nanoparticles reinforcement in the properties of wood polymer clay nanocomposites10.1016/j.jtice.2012.11.018 ↗
29. Introduction of amino groups on the surface of thin photo definable epoxy resin layers via chemical modification10.1016/j.apsusc.2009.06.043 ↗