Achieving the synergy of superior damage tolerance and oxidation resistance of 2D Cf/ZrB2-SiC composites via fiber heat treatment
Source abstract
Abstract
Abstract The need for synergy of strengthening and anti-oxidation under high-temperature and oxidative environment imposes new demands on nonablative thermal protection materials. Herein, 2D Cf/ZrB2-SiC composite with superior damage tolerance and excellent oxidation resistance were constructed using a simple fiber heat treatment. An enhanced flexural strength of 234 ± 18 MPa and an intermediate work of fracture of 1342 J/m2 were obtained for 2D Cf-HT/ZrB2-SiC composite, increasing by nearly 19.4% and 171.7% as compared with those of Cf-AR/ZrB2-SiC sample, triggered by multiple toughening mechanisms including crack bifurcation, fiber bundles pull-out and bridging. The surface of 2D Cf-HT/ZrB2-SiC composite was covered with a dense silica glass layer and embedded with a few zirconia particles after oxidation at 1500 °C for 1 h, resulting in an excellent oxidation resistance. This work presents a simple approach to achieve the synergy of superior damage tolerance and oxidation resistance of continuous carbon fiber reinforced ceramic matrix composite.
Source: openaire · Quality: candidate unverified · Source record ↗
Research context
OpenAlex topics: Advanced ceramic materials synthesis · Advanced materials and composites · MXene and MAX Phase Materials
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (45)
Show source-provided references
1. Is spark plasma sintering suitable for the densification of continuous carbon fibre - UHTCMCs?10.1016/j.jeurceramsoc.2019.12.004 ↗
2. Oxidation behavior and ablation mechanism of Cf/ZrB2-SiC composite fabricated by vibration-assisted slurry impregnation combined with low-temperature hot pressing10.1016/j.corsci.2019.108181 ↗
3. On the thermal shock resistance and mechanical properties of novel unidirectional UHTCMCs for extreme environments10.1038/s41598-018-27328-x ↗
4. Introduction to H2020 project C 3 HARME – next generation ceramic composites for combustion harsh environment and space10.1080/17436753.2018.1509822 ↗
5. Aero-thermo-chemical characterization of ultra-high-temperature ceramics for aerospace applications10.1016/j.jeurceramsoc.2017.12.043 ↗
6. Advanced structural ceramics in aerospace propulsion10.1038/nmat4687 ↗
7. Enhanced mechanical properties and thermal shock resistance of Cf/ZrB2-SiC composite via an efficient slurry injection combined with vibration-assisted vacuum infiltration10.1016/j.jeurceramsoc.2020.07.003 ↗
8. Enhancing the fracture resistance of carbon fiber reinforced SiC matrix composites by interface modification through a simple fiber heat-treatment process10.1016/j.carbon.2016.08.047 ↗
9. Increasing the strength and toughness of a carbon fiber/silicon carbide composite by heat treatment10.1016/j.carbon.2012.11.001 ↗
10. The effects of thermal exposure on the structural and mechanical integrity of carbon fibres10.1007/BF01129941 ↗
11. Design and optimization of the coating thickness on chopped carbon fbers and sintering temperature for ZrB2-SiC-Cf composites prepared by hot pressing10.1016/j.jeurceramsoc.2019.03.038 ↗
12. ZrB 2 -based composites toughened by as-received and heat-treated short carbon fibers10.1016/j.jeurceramsoc.2016.09.012 ↗
13. A novel vibration-assisted slurry impregnation to fabricate Cf/ZrB2-SiC composite with enhanced mechanical properties10.1016/j.jeurceramsoc.2018.10.029 ↗
14. ASTM C1525-04. Standard Test Method for Determination of Thermal Shock Resistance for Advanced Ceramics by Water Quenching (2020).
15. ISO 19830:2015, Electron Spectroscopies—Minimum Reporting Requirements for Peak Fitting in X-ray Photoelectron Spectroscopy (International Organization for Standardization, Geneva, 2015).
16. Practical guide for curve fitting in x-ray photoelectron spectroscopy10.1116/6.0000377 ↗
17. Influence of thermal treatment on thermo-mechanical stability and surface composition of carbon fiber10.1016/j.apsusc.2013.02.102 ↗
18. Lightweight, flexible SiCN ceramic nanowires applied as effective microwave absorbers in high frequency10.1016/j.cej.2017.12.008 ↗
19. Photoemission studies of fluorine functionalized porous graphitic carbon10.1063/1.3691888 ↗
20. Surface plasma treatment of the electrospun TiO2/PVP composite fibers in different atmosphere10.1016/j.apsusc.2020.146381 ↗
21. XPS study of carbon fiber surfaces treated by thermal oxidation in a gas mixture of O2/(O2+N2)10.1016/S0169-4332(00)00558-4 ↗
22. An efficient hydrothermal transformation approach for construction of controllable carbon coating on carbon fiber from renewable carbohydrate10.1016/j.apsusc.2019.06.186 ↗
23. Effect of microstructure on the modulus of PAN-based carbon fibers during high temperature treatment and hot stretching graphitization10.1007/s10853-006-0519-4 ↗
24. A reconsideration of the relationship between the crystallite size La of carbons determined by X-ray diffraction and Raman spectroscopy10.1016/j.carbon.2006.06.029 ↗
25. Raman spectra of virgin and damaged graphite edge planes10.1016/S0008-6223(97)00141-3 ↗
26. Characterization of PAN-based carbon fibres with laser Raman spectroscopy10.1007/BF00352882 ↗
27. Graphitization thermal treatment of carbon nanofibers10.1016/j.carbon.2013.03.031 ↗
28. Effect of pyrolytic carbon coating on the microstructure and fracture behavior of the Cf/ZrB2-SiC composite10.1016/j.ceramint.2018.07.210 ↗
29. Microstructures and mechanical properties of Cf/ZrB2-SiC composite fabricated by nano slurry brushing combined with low-temperature hot pressing10.1016/j.jallcom.2019.03.147 ↗
30. The effective surface energy of brittle materials10.1007/BF00585484 ↗
31. Rolling compacted fabrication of carbon fiber reinforced ultra-high temperature ceramics with highly oriented architectures and exceptional mechanical feedback10.1016/j.ceramint.2018.04.249 ↗
32. Toughening effect of short carbon fibers in the ZrB2–ZrSi2 ceramic composites10.1016/j.matdes.2015.03.006 ↗
33. High-performance ZrB 2 -SiC-C f composite prepared by low-temperature hot pressing using nanosized ZrB 2 powder10.1016/j.jeurceramsoc.2017.02.008 ↗
34. Architectural engineering inspired method of preparing C f /ZrC-SiC with graceful mechanical responses10.1111/jace.16018 ↗
35. One-step introduction of ZrC-SiC inside carbon fabric to fabricate high homogeneous and damage-tolerant composite inspired by vibration10.1016/j.jeurceramsoc.2019.02.030 ↗
36. R-curve behavior and thermal shock resistance of ceramics10.1111/j.1151-2916.1990.tb06562.x ↗
37. Strong and thermostable hydrothermal carbon coated 3D needled carbon fiber reinforced silicon-boron carbonitride composites with broadband and tunable high-performance microwave absorption10.1016/j.jcis.2020.08.030 ↗
38. Oxidation behaviour of a continuous carbon fibre reinforced ZrB 2 –SiC composite10.1016/j.corsci.2017.04.012 ↗
39. Mechanical, oxidation and ablation properties of C/(C-SiC)CVI-(ZrC-SiC)PIP composites10.1016/j.corsci.2019.108200 ↗
40. Using macroporous graphene networks to toughen ZrC–SiC ceramic10.1016/j.jeurceramsoc.2018.04.037 ↗
41. Effect of carbon nanotube on processing, microstructural, mechanical and ablation behavior of ZrB2-20SiC based ultra-high temperature ceramic composites10.1016/j.carbon.2016.10.002 ↗
42. Preparation of carbon/carbon-ultra high temperature ceramics composites with ultra high temperature ceramics coating
43. Ablation resistance of wedge-shaped C/C-ZrB 2 -ZrC-SiC composites exposed to an oxyacetylene torch10.1016/j.corsci.2016.08.010 ↗
44. Ablation behavior of functional gradient ceramic coating for porous carbon-bonded carbon fiber composites10.1016/j.corsci.2018.07.025 ↗
45. Ultra-high-temperature testing of sintered ZrB2-based ceramic composites in atmospheric re-entry environment10.1016/j.ijheatmasstransfer.2020.119910 ↗