Microwave-assistant synthesis of ordered CuO micro-structures on Cu substrate
Source abstract
Abstract
A mild template-free mixed solution medium with the assistant of microwave method was successfully established to synthesize well-aligned CuO nanostructures. By varying process parameters such as the volume ratio of the mixed solution, different kinds of architectural structures can be controllably synthesized in large quantities. On the basis of the results, it is found that the polarity of the solution plays the key role in controlling the growth of the CuO crystal. The as-prepared CuO products were characterized using diverse techniques including X-ray diffraction, scanning electron microscopy, and transmission electron microscopy. The gas sensor property investigation shows that the sensitivities to ethanol of the as-prepared CuO nanostructures are higher than those of normal CuO nanoparticles.
Source: openaire · Quality: candidate unverified · Source record ↗
Research context
OpenAlex topics: Copper-based nanomaterials and applications · ZnO doping and properties · Gas Sensing Nanomaterials and Sensors
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (33)
Show source-provided references
1. Epitaxial core–shell and core–multishell nanowire heterostructures10.1038/nature01141 ↗
2. Cu/ZnO and Cu/ZnO/SiO2 catalysts studied by low-energy ion scattering10.1021/jp990375a ↗
3. Photoelectrochemical studies on nanocrystalline hematite films10.1021/cm00042a026 ↗
4. Microwave-induced polyol-process synthesis of copper and copper oxide nanocrystals with controllable morphology10.1016/S0925-4005(98)00144-0 ↗
5. Microwave-assisted synthesis of cupric oxide nanosheets and nanowhiskers10.1006/jcat.1998.2257 ↗
6. Synthesis of copper nanowires via a complex-surfactant-assisted hydrothermal reduction process10.1021/jp036023s ↗
7. Solvothermal preparation of Cu2O crystalline particles10.1016/S0022-0248(02)01902-4 ↗
8. Epitaxial electrodeposition of copper(I) oxide on single-crystal gold(100)10.1021/cm990304o ↗
9. Single-crystalline copper nanowires produced by electrochemical deposition in polymeric ion track membranes
10. Solvent effects on the growth and steric stabilization of copper metallic nanoparticles in AOT reverse micelle systems10.1021/jp0354090 ↗
11. Preparation of uniformly dispersed copper nanocluster doped silica glasses by the sol–gel process10.1039/b101059j ↗
12. Solid-state reaction to the synthesis of copper oxide nanorods in the presence of a suitable surfactant10.1039/b008215p ↗
13. Preparation and characterization of CuO nanorods by thermal decomposition of CuC2O4 precursor10.1016/S0025-5408(02)00848-6 ↗
14. Solution-phase synthesis of Cu2O nanocubes10.1021/nl0258776 ↗
15. Sonochemical synthesis and characterization of nanometer-size transition metal oxides from metal acetates10.1021/cm000166z ↗
16. Sonochemical synthesis of amorphous Cu and nanocrystalline Cu2O embedded in a polyaniline matrix10.1039/b005769j ↗
17. Solid-state reaction to the synthesis of copper oxide nanorods10.1016/S0927-0248(97)00233-X ↗
18. A single photochemical route for the formation of both copper nanoparticles and patterned nanostructured films10.1039/B308418C ↗
19. Photochemical formation of copper nanoparticles in poly (N-vinylpyrrolidone)10.1016/S0009-2614(03)00073-3 ↗
20. Temperature dependence of field emission from cupric oxide nanobelt films10.1063/1.1595156 ↗
21. Microwave-enhanced reaction rates for nanoparticle synthesis10.1021/ja052463g ↗
22. Microwave synthesis and optical properties of uniform nanorods and nanoplates of rare earth oxides10.1021/jp0670283 ↗
23. Microwave-assisted synthesis of calcium carbonate (vaterite) of various morphologies in water–ethylene glycol mixed solvents10.1021/jp060939s ↗
24. Monetite formed in mixed solvents of water and ethylene glycol and its transformation to hydroxyapatite10.1021/jp061738r ↗
25. The microwave-assisted polyol synthesis of nanosized hard magnetic material, FePt10.1039/b411829d ↗
26. Sonochemical and microwave-assisted synthesis of linked single-crystalline ZnO rods10.1016/j.matchemphys.2004.08.010 ↗
27. Shape-controlled synthesis of zinc oxide by microwave heating using an imidazolium salt10.1016/j.inoche.2004.06.014 ↗
28. Shape-controlled synthesis of zinc oxide by microwave heating using an imidazolium salt10.1002/ejic.200400258 ↗
29. Microwave-assisted elemental direct reaction route to nanocrystalline copper chalcogenides CuSe and Cu2Te10.1039/b205558a ↗
30. Microwave synthesis of highly aligned ultra narrow semiconductor rods and wires10.1021/ja058148b ↗
31. Synthesis of Cu(OH)2 and CuO nanoribbon arrays on a copper surface10.1021/la0342870 ↗
32. Microwave synthesis of bimetallic nanoalloys and CO oxidation on ceria-supported nanoalloys10.1021/cm9004486 ↗
33. Mechanisms for the shape-control and shape-evolution of colloidal semiconductor nanocrystals10.1002/adma.200390107 ↗