Ageing of commercial austenitic, martensitic and duplex stainless steel surfaces after formation of laser-induced periodic surface structures by fs-laser irradiation
Source abstract
Abstract
• LIPSS were fabricated on different stainless steels using fs-lasers. • All stainless steels exhibit regular LIPSS with similar geometrical properties. • A laser-induced oxide is formed with a two-layered structure. • Ageing depends on extent and chemical composition of superimposed nanoparticles. • Repeated water contact leads to less pronounced ageing. The time-dependent wetting behavior was investigated for commercially available austenitic, martensitic and duplex stainless steel surfaces after femtosecond (fs) laser irradiation. For this purpose, highly regular LIPSS with almost identical geometric properties were generated on the stainless steels in an air environment by near-infrared fs-laser processing ( λ = 1025 nm, τ = 300 fs, f rep = 100 kHz, v = 0.67 m/s, Δx = 6 μm, F = 1.1 J/cm 2 ) and compared to the polished initial surfaces as reference. The wetting with distilled water was evaluated as a function of aging time by contact angle measurements using the sessile drop method. The laser-induced morphological, topographical and chemical alteration of the surface was characterized by scanning electron microscopy, atomic force microscopy, X-ray photoelectron spectroscopy, glow-discharge optical emission spectroscopy as well as high-resolution imaging and scanning transmission electron microscopy. Despite an almost identical LIPSS-based topography alteration, the stainless steels revealed very different ageing behavior. For permanently used samples, it was shown that the ageing effect is less pronounced than for samples that were stored in ambient air following fs-laser irradiation until the wetting measurement. The results obtained make an important contribution to understanding and controlling the ageing effect of metal surfaces and thus facilitate the transfer of LIPSS-based functional surface engineering and design to industrial processes.
Source: openalex_inverted_index · Quality: baseline
Research context
OpenAlex topics: Laser Material Processing Techniques · Surface Roughness and Optical Measurements · Laser and Thermal Forming Techniques
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
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