Evolution of acoustic emission and macro-microscopic fracture characteristics in thermally treated and cryogenically cooled granite
Source abstract
Abstract
Liquid nitrogen (LN2) fracturing is an emerging anhydrous technology with significant potential for reservoir stimulation in Hot Dry Rock (HDR) geothermal exploitation. Understanding the fracture mechanics of rock subjected to LN2 cooling under high-temperature conditions is essential for optimizing stimulation results. In this study, granite samples heated to various temperatures were subjected to LN2 thermal shock. Acoustic emission (AE) technology and a mechanical testing system were employed to investigate the amplitude distribution, spatial signal evolution, and both macroscopic and microscopic fracture behaviors. The results indicate that AE activity and signal strength intensify significantly with increasing heating temperature. While low-amplitude signals predominate, the spatial distribution shifts from localized main fractures below 300 °C to widespread micro-cracking above 300 °C. Surface morphology analysis reveals a surge in roughness, with median roughness height increasing by 75% between 200 and 300 °C, indicating a critical threshold for thermal damage. The maximum crack displacement distance increased by ∼55.2% from 25 to 400 °C, accompanied by increased tortuosity. Correspondingly, the fractal dimension rose by 19.6% to 1.778. Microscopic observations show that at 300 °C and above, fracture surfaces exhibit layered and step-like matrix failure. This is attributed to high thermal stress weakening the structural bonding, facilitating crack propagation along weak zones to form complex fracture networks. These findings demonstrate that sequential high-temperature heating and LN2 cooling significantly enhance fracture network complexity and density while reducing mechanical strength, providing theoretical and practical support for LN2-based HDR stimulation.
Source: crossref · Quality: baseline
Research context
OpenAlex topics: Rock Mechanics and Modeling · Hydraulic Fracturing and Reservoir Analysis · Geothermal Energy Systems and Applications
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
Affiliations
School of Resources and Civil Engineering, Suzhou University 1 , Suzhou, Anhui 234000,
Scientific and Technological Research Platform for Disaster Prevention and Control of Deep Coal Mining, Anhui University of Science and Technology 2 , Huainan 232001,
School of Civil Engineering and Architecture, Xi’an University of Technology 3 , Xi’an 710048,
School of Energy and Mining Engineering, China University of Mining and Technology-Beijing 4 , Beijing 100083,
References (37)
Show source-provided references
1. Geothermal energy: Power plant technology and direct heat applications10.1016/j.rser.2018.06.047 ↗
2. A global review of enhanced geothermal system (EGS)10.1016/j.rser.2017.06.097 ↗
3. Predicting the potential of China’s geothermal energy in industrial development and carbon emission reduction10.3390/su15097508 ↗
4. A review of geothermal energy resources, development, and applications in China: Current status and prospects10.1016/j.energy.2015.08.098 ↗
5. Effect of hydrothermal fluid backfill on the mechanical behaviour of deep granite under high-temperature and high-pressure conditions10.1007/s00603-023-03310-6 ↗
6. An investigation on hydraulic fracturing characteristics in granite geothermal reservoir10.1016/j.engfracmech.2020.107252 ↗
7. LN cooling on mechanical properties and fracture characteristics of hot dry granites involving ANN prediction10.1016/j.renene.2023.119058 ↗
8. Experimental study of thermal-crack characteristics on HDR impacted by liquid nitrogen jet10.1016/j.geothermics.2018.08.002 ↗
9. Experimental study on the physical and mechanical variations of hot granite under different cooling treatments10.1016/j.renene.2021.07.132 ↗
10. 3D multi-scale reconstruction of fractured shale and influence of fracture morphology on shale gas flow10.1007/s11053-021-09861-1 ↗
11. Uncertainty analysis for heat extraction performance from a stimulated geothermal reservoir with the diminishing feature of permeability enhancement10.1016/j.geothermics.2021.102339 ↗
12. Potentially exploitable supercritical geothermal resources in the ductile crust10.1038/ngeo2879 ↗
13. Numerical analysis of transient conjugate heat transfer and thermal stress distribution in geothermal drilling with high-pressure liquid nitrogen jet10.1016/j.applthermaleng.2017.10.042 ↗
14. Permeability evolution and mesoscopic cracking behaviours of liquid nitrogen cryogenic freeze fracturing in low permeable and heterogeneous coal10.1016/j.powtec.2017.10.058 ↗
15. Cryogenic fracturing for reservoir stimulation–laboratory studies10.1016/j.petrol.2014.09.003 ↗
16. Effects of cyclic heating and LN2-cooling on the physical and mechanical properties of granite10.1016/j.applthermaleng.2019.04.046 ↗
17. The influence of liquid nitrogen cooling on fracture toughness of granite rocks at elevated temperatures: An experimental study10.1016/j.engfracmech.2021.107628 ↗
18. Correlating mode-I fracture toughness and mechanical properties of heat-treated crystalline rocks10.1016/j.jrmge.2017.09.009 ↗
19. Research on the anisotropic fracture behaviour and the corresponding fracture surface roughness of shale10.1016/j.engfracmech.2021.107963 ↗
20. An investigation of stimulation mechanisms in enhanced geothermal systems10.1016/j.ijrmms.2014.07.011 ↗
21. Investigation of the fracture modes of red sandstone using XFEM and acoustic emissions10.1016/j.tafmec.2016.03.012 ↗
22. Acoustic emission evolution and hydraulic fracture morphology of changing shale stressed to failure at different injection rates in the laboratory10.1007/s00603-023-03586-8 ↗
23. Study of acoustic emission in a compression test of andesite rock10.1016/j.mspro.2015.04.037 ↗
24. Acoustic emission from failing rock behaviour10.1007/bf01020309 ↗
25. Experimental investigation on mode I fracture characteristics of Longmaxi formation shale after cyclic thermal shock and high-temperature acid etching treatments10.1016/j.engfracmech.2023.109762 ↗
26. Experimental investigation on mode I fracture characteristics of granite after cyclic heating and cooling treatments10.1016/j.engfracmech.2019.106740 ↗
27. Fracture evolution of granite under cyclic thermal shocks: Effects of liquid nitrogen cooling on strength, toughness, and acoustic emission characteristics10.1016/j.tsep.2026.104507 ↗
28. Thermal acoustic emission characteristics and damage evolution of granite under cyclic thermal shock10.1007/s12665-023-11075-y ↗
29. Experimental investigation on the influence on mechanical properties and acoustic emission characteristics of granite after heating and water-cooling cycles10.1007/s40948-023-00627-y ↗
30. Cryogenic quenching of rock using liquid nitrogen as a coolant: Investigation of surface effects10.1016/j.ijheatmasstransfer.2017.11.123 ↗
31. An influence of thermally-induced micro-cracking under cooling treatments: mechanical characteristics of Australian granite10.3390/en11061338 ↗
32. Fracture behaviour and fracture surface roughness of high-temperature granite subjected to liquid nitrogen and water cooling10.1016/j.engfracmech.2024.109987 ↗
33. Fracture behavior of high-temperature granite subjected to liquid nitrogen cooling: Semi-circular bending test and crack evolution analysis10.1016/j.tafmec.2023.104100 ↗
34. Impact of cyclic liquid nitrogen treatment on the pore and fracture structures of shale at different scales and its effect on permeability enhancement10.1016/j.geoen.2022.211367 ↗
35. Fracture evolution and mechanical deterioration of granite under cyclic thermal and liquid nitrogen cryogenic impact10.1063/5.0284662 ↗
36. An approximated box height for differential-box-counting method to estimate fractal dimensions of gray-scale images10.3390/e19100534 ↗
37. Image texture surface analysis using an improved differential box counting based fractal dimension10.1016/j.powtec.2020.01.053 ↗