journal article·2021-09-01Open access

Effect of synthesis method parameters on the photocatalytic activity of tungsten oxide nanoplates

Aiymkul Markhabayeva, Khabibulla Abdullin, Zhanar Kalkozova, Shyryn Nurbolat, Nurxat Nuraje

AIP Advances· Volume 11· Issue 9

Abstract

A simple chemical bath deposition method has been developed to study the formation of nanoplate morphology of tungsten oxide. The obtained materials were characterized by field emission scanning electron microscopy, transmission electron microscopy, x-ray diffractometry, Raman spectroscopy, and UV–vis diffuse reflectance spectroscopy. The photocatalytic activity of the resulting samples was further evaluated by degradation of Rhodamine B under light irradiation. It was found that both synthesis parameters and morphology affected the tungsten oxide photocatalytic activity. Tungsten oxide nanoplates obtained by a simple chemical bath deposition method have demonstrated a higher specific area and higher photocatalytic activity compared to the nanopowders obtained by the hydrothermal method.
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Research context

OpenAlex topics: Transition Metal Oxide Nanomaterials · Advanced Photocatalysis Techniques · Gas Sensing Nanomaterials and Sensors

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

National Nanotechnology Laboratory Open Type, Al-Farabi Kazakh National University 1 , Almaty, Republic of Kazakhstan

Institute of Applied Sciences and Information Technologies 2 , Almaty, Republic of Kazakhstan

Advanced Solar Energy Materials and System Lab, National Laboratory Astana (NLA), Nazarbayev University 3 , Nursultan, Republic of Kazakhstan

Department of Chemical and Materials Engineering, School of Engineering and Digital Science, Nazarbayev University 4 , Nursultan, Republic of Kazakhstan

Funding

Program of Committee of Science of Ministry Education and science Republic Kazakhstan · Program of Committee of Science of Ministry Education of Kazakhstan

References (36)

Show source-provided references
1. Measurement of minority-carrier diffusion lengths using wedge-shaped semiconductor photoelectrodes10.1039/C4EE01580K ↗
2. Photoelectrochemical behavior of hierarchically structured Si/WO3 core-shell tandem photoanodes10.1021/nl404623t ↗
3. Advances on tungsten oxide based photochromic materials: Strategies to improve their photochromic properties10.1039/C7TC04189F ↗
4. Nanocrystalline tungsten oxide thin film: Preparation, microstructure, and photochromic behavior10.1557/JMR.2000.0132 ↗
5. Highly efficient photochromic tungsten oxide@PINPAM composite spheres with a fast response10.1021/acsami.0c20817 ↗
6. Controlling wettability and photochromism in a dual-responsive tungsten oxide film10.1002/ange.200502061 ↗
7. Facile synthesis of tungsten oxide nanostructures for efficient photoelectrochemical water oxidation10.1016/j.jpowsour.2014.07.012 ↗
8. Tungsten oxide clathrates for water oxidation: A first principles study10.1021/cm3032225 ↗
9. Tungsten oxide nanostructures and nanocomposites for photoelectrochemical water splitting10.1039/C9NR03474A ↗
10. Photoactive tungsten-oxide nanomaterials for water-splitting10.3390/nano10091871 ↗
11. Designing of WO3@Co3O4 heterostructures to enhance photoelectrochemical performances10.1021/acs.jpca.9b09173 ↗
12. Thermal treatment effects on the material and gas-sensing properties of room-temperature tungsten oxide nanorod sensors10.1016/j.snb.2008.11.037 ↗
13. AACVD and gas sensing properties of nickel oxide nanoparticle decorated tungsten oxide nanowires10.1039/C8TC00571K ↗
14. Gas sensing properties of nanocrystalline tungsten oxide synthesized by acid precipitation method10.1016/j.snb.2010.06.053 ↗
15. Review on recent progress in the development of tungsten oxide based electrodes for electrochemical energy storage10.1002/cssc.201902071 ↗
16. Phase transformation in tungsten oxide nanoplates as a function of post-annealing temperature and its electrochemical influence on energy storage10.1039/D0NA00423E ↗
17. Transition from battery to pseudocapacitor behavior via structural water in tungsten oxide10.1021/acs.chemmater.6b05485 ↗
18. A novel heterostructure of oriented core/shell tungsten oxide nanorod arrays for electrochromo-pseudocapacitor10.1016/j.scriptamat.2019.08.020 ↗
19. Core–shell (W@WO3) nanostructure to improve electrochemical performance10.1021/acsaem.8b01869 ↗
20. Organic additives-free hydrothermal synthesis and visible-light-driven photodegradation of tetracycline of WO3 nanosheets10.1021/ie4036687 ↗
21. Highly sensitive btex sensors based on hexagonal WO3 nanosheets10.1016/j.snb.2019.04.110 ↗
22. Controlled synthesis of defect-rich ultrathin two-dimensional WO3 nanosheets for NO2 gas detection10.1016/j.snb.2017.02.038 ↗
23. Ru-decorated WO3 nanosheets for efficient xylene gas sensing application10.1016/j.jallcom.2020.154196 ↗
24. Improving methane gas sensing performance of flower-like SnO2 decorated by WO3 nanoplates10.1016/j.talanta.2019.03.014 ↗
25. Facile fabrication of WO3 nanoplates thin films with dominant crystal facet of (002) for water splitting10.1021/cg5012154 ↗
26. Synthesis, assembly, and electrochromic properties of uniform crystalline WO3 nanorods10.1021/jp804035r ↗
27. Controllable assembly of WO3 nanorods/nanowires into hierarchical nanostructures10.1021/jp065170y ↗
28. Ferroelectric WO3 nanoparticles for acetone selective detection10.1021/cm800761e ↗
29. Hydrogen-treated WO3 nanoflakes show enhanced photostability10.1039/C2EE03158B ↗
30. Significant enhancement of the photoelectrochemical activity of WO3 nanoflakes by carbon quantum dots decoration10.1016/j.carbon.2016.04.051 ↗
31. Recent advances in ultrathin two-dimensional nanomaterials10.1021/acs.chemrev.6b00558 ↗
32. Topochemical preparation of WO3 nanoplates through precursor H2WO4 and their gas-sensing performances10.1021/jp205782a ↗
33. Synthesis of WO3 flower-like hierarchical architectures and their sensing properties10.1016/j.jallcom.2015.07.142 ↗
34. 1996
35. Infrared and Raman study of Wo3 tungsten trioxides and WO3, xH2O tungsten trioxide tydrates10.1016/0022-4596(87)90359-8 ↗
36. Characterization of pulsed laser deposited WO3 thin films for electrochromic devices10.1016/S0169-4332(99)00335-9 ↗