The effect of powder shape on the magnetic anisotropy in NdFeB bonded magnets
Source abstract
Abstract
The advent of NdFeB bonded magnets with freedom of shape design is effective in achieving motor size and weight reductions. In this paper, the NdFeB bonded magnets were produced through calendaring molding, and the effect of powder shape on degree of alignment (DOA) of NdFeB bonded magnets was investigated. The magnetic measurement results demonstrate that platelet-shaped anisotropic Master Quality Authenticated (MQA) powders exhibit a significantly higher DOA compared to sphere-shaped anisotropic HDDR powders. Microstructural analysis reveals the presence of an oriented structure induced by mechanical stress in MQA bonded magnets, resulting in magnetic anisotropy. This observation is consistent with the difference in X-ray diffraction (XRD) patterns between the cross-section and surface of MQA bonded magnets. Conversely, spherical HDDR particles display minimal orientation and maintain a random distribution, resulting in magnetic isotropy. The XRD pattern of the cross-section of HDDR bonded magnets closely resembles that of its surface. In summary, our findings highlight the superior potential of platelet-shaped anisotropic MQA powders for achieving enhancing magnetic properties during the calendaring molding process, in contrast to sphere-shaped anisotropic HDDR powders. This study provides valuable insights into the determinants of mechanical particle orientation during the fabrication of anisotropic NdFeB bonded magnets, with implications for the development of high-performance bonded magnets.
Source: crossref · Quality: baseline
Research context
OpenAlex topics: Magnetic Properties of Alloys · Magnetic properties of thin films · Magnetic Properties and Applications
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
Affiliations
Faculty of Materials and Manufacturing, Key Laboratory of Advanced Functional Materials, Ministry of Education of China, Beijing University of Technology , Beijing 100124, China
Funding
National Key R&D Program of China
References (27)
Show source-provided references
1. Polymer-bonded magnets produced by laser powder bed fusion: Influence of powder morphology, filler fraction and energy input on the magnetic and mechanical properties10.1016/j.materresbull.2022.112051 ↗
2. Additive manufacturing of highly dense anisotropic Nd–Fe–B bonded magnets10.1016/j.scriptamat.2020.03.012 ↗
3. Additive manufacturing of near-net-shape bonded magnets: Prospects and challenges10.1016/j.scriptamat.2016.12.035 ↗
4. Current status and recent topics of rare-earth permanent magnets10.1088/0022-3727/44/6/064001 ↗
5. 3D printing of high performance polymer-bonded PEEK-NdFeB magnetic composite materials10.1186/s42252-020-00006-w ↗
6. Recent progress in the development of high-performance bonded magnets using rare earth-Fe compounds10.1080/14686996.2021.1944780 ↗
7. Progress of research on bonded Nd–Fe–B magnets10.1016/s1006-706x(08)60236-8 ↗
8. Perspective and prospects for rare earth permanent magnets10.1016/j.eng.2018.11.034 ↗
9. Pr–Fe and Nd–Fe–based materials: A new class of high-performance permanent magnets (invited)10.1063/1.333571 ↗
10. Nd–Fe–B die-upset and anisotropic bonded magnets (invited)10.1063/1.342394 ↗
11. Present status of the hydrogenation-decomposition-desorption-recombination process as applied to the production of magnets10.1016/0925-8388(93)90356-r ↗
12. Crystallographic alignment in the recombination stage in d-HDDR process of Nd–Fe–B–Ga–Nb powders10.1063/1.4944073 ↗
13. Studies on in situ magnetic alignment of bonded anisotropic Nd–Fe–B alloy powders10.1016/j.jmmm.2016.08.090 ↗
14. Effect of process on the magnetic and mechanical properties of Nd–Fe–B bonded magnets10.1016/j.matdes.2008.06.062 ↗
15. Densification mechanism and its effect on the magnetic properties of Nd–Fe–B bonded magnets through the new high-energy compaction method10.1016/j.jmmm.2019.03.049 ↗
16. Mechanical properties of polyphenylene-sulfide (PPS) bonded Nd–Fe–B permanent magnets10.1016/s0921-5093(03)00400-3 ↗
17. Fused filament fabrication of Nd–Fe–B bonded magnets: Comparison of PA12 and TPU matrices10.1016/j.addma.2020.101745 ↗
18. Development of hard ferrite filled thermoplastic elastomers for the production of permanent magnets10.1016/j.sna.2021.113224 ↗
19. Fabrication of highly dense isotropic Nd–Fe–B nylon bonded magnets via extrusion-based additive manufacturing10.1016/j.addma.2018.04.001 ↗
20. Packing bimodal magnetic particles to fabricate highly dense anisotropic rare earth bonded permanent magnets10.1039/d3ra02349d ↗
21. In-situ magnetic alignment model for additive manufacturing of anisotropic bonded magnets10.1016/j.addma.2021.102096 ↗
22. Alignment of magnetic particles in anisotropic Nd–Fe–B bonded magnets10.1088/1361-6463/abfbf7 ↗
23. Facile preparation of bonded NdFeB/SmFeN hybrid magnets with flexibility, anisotropy and high energy density10.1016/j.jmmm.2023.171084 ↗
24. Calculation of remanence and degree of texture from EBSD orientation histograms and XRD rocking curves in Nd–Fe–B sintered magnets10.1016/j.jmmm.2015.01.046 ↗
25. Crystallographic orientation analysis in HDDR process of anisotropic Nd–Fe–B magnet powders10.1016/j.jmmm.2017.03.014 ↗
26. Enhancement of magnetic properties by Zn addition in Nd–Fe–B hot-deformed magnets produced by spark plasma sintering method10.1016/j.jallcom.2016.06.151 ↗
27. Microstructure of hot-pressed and die-upset NdFeB magnets10.1063/1.339709 ↗