journal article·2023-04

Fire impact on mechanically failed graphite/epoxy composites

Dounia Boushab, Hasnaa Ouidadi, Aniket Mote, Matthew Priddy, Santanu Kundu, Charles U. Pittman, Jaime Grunlan, Qingsheng Wang, Thomas Lacy

Polymer Composites· Volume 44· Issue 4
Publisher page

Abstract

Abstract Aircraft crashes often initiate or accompany fire incidents. Post‐crash fires, in particular, can mask or destroy critical fractographic failure features necessary for accident reconstruction. As a first step in developing a coherent strategy for composite aircraft post‐crash forensic analysis, a series of vertical flame tests were performed on mechanically failed Cytec T40‐800/Cycom® 5215 graphite/epoxy unnotched compression, short beam strength, and in‐plane shear specimens. Visual inspection and scanning electron microscopy were used to examine the specimens fracture surfaces before and after fire testing. The fire‐induced damage included matrix decomposition, melt dripping, char, soot, delamination, and residual thickness increases. The composite thermal degradation was significantly influenced by the specimen stacking sequence, the fracture surface morphology, and the total available free surface area. In addition, microscopic inspection showed that char layers impeded heat conduction and oxygen transfer to the interior of the specimens resulting in less thermal damage to the underlying plies. Moreover, burned specimens with more available free surface area sustained more thermal degradation and fire combustion damage for a given fire exposure duration. Exposed fiber bundles from the fracture surfaces were susceptible to severe thinning and thermal oxidation, which destroyed critical fractographic failure features necessary for accident reconstruction.
Source: crossref · Quality: baseline

Research context

OpenAlex topics: Flame retardant materials and properties · Fiber-reinforced polymer composites · Fire dynamics and safety research

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

J. Mike Walker '66 Department of Mechanical Engineering Texas A&M University College Station Texas USA

Department of Mechanical Engineering Mississippi State University Starkville Mississippi USA

Dave C. Swalm School of Chemical Engineering Mississippi State University Starkville Mississippi USA

Department of Chemistry Mississippi State University Starkville Mississippi USA

Artie McFerrin Department of Chemical Engineering Texas A&M University College Station Texas USA

Funding

Federal Aviation Administration · Mississippi State University · Texas A and M University

References (66)

Show source-provided references
1. Beukers A. · 2011
2. Brown A. · 2012
3. Brown A. · 2013
4. Wright M. T. · 2003
5. Mouritz A. P. · 2007
6. Zhang Z.Thermo‐mechanical behavior of polymer composites exposed to fire. Dissertation Virginia Polytechnic Institute and State University 2010.
7. Santucci J..Get out get out get out': Everyone survives after plane's 'horrific' failed takeoff in Texas.2021USA TODAY (accessed: September 2022).
8. 2018
9. Wood R. H. · 2006
10. O'Donnell M. J. · 2009
11. Righi H. · 2020
12. Mote A.;Ouidadi H.;Boushab D.;Priddy M.;Kundu S.;PittmanJr. C. U.;Grunlan J.;Wang Q.;LacyJr T. E.Post mechanical failure fire damage characterization of graphite/epoxy composites. Proceedings of the American Society for Composites—Thirty‐Sixth Technical Conference on Composite Materials 2021.10.12783/asc36/35890 ↗
13. 10.1016/j.polymdegradstab.2018.04.00410.1016/j.polymdegradstab.2018.04.004 ↗
14. Quintiere J. G. · 2007
15. 10.1007/s10973-022-11279-710.1007/s10973-022-11279-7 ↗
16. 10.1016/j.cej.2021.13203110.1016/j.cej.2021.132031 ↗
17. 10.1017/S143192761100822110.1017/S1431927611008221 ↗
18. 10.1002/fam.248410.1002/fam.2484 ↗
19. 10.1002/fam.111210.1002/fam.1112 ↗
20. 10.1016/j.compositesb.2019.01.08610.1016/j.compositesb.2019.01.086 ↗
21. 10.1016/j.compstruct.2022.11533410.1016/j.compstruct.2022.115334 ↗
22. 10.1016/S0266-3538(00)00204-910.1016/S0266-3538(00)00204-9 ↗
23. 10.1016/j.compositesb.2016.06.05910.1016/j.compositesb.2016.06.059 ↗
24. 10.1016/j.compstruct.2021.11478610.1016/j.compstruct.2021.114786 ↗
25. 10.3390/polym1211260010.3390/polym12112600 ↗
26. 10.1002/pc.2629010.1002/pc.26290 ↗
27. 10.1002/pc.2580610.1002/pc.25806 ↗
28. 10.1002/pc.2578610.1002/pc.25786 ↗
29. Thiyagu C. · Polym. Compos. · 2022 · 44 · 1
30. 10.1002/vnl.2192110.1002/vnl.21921 ↗
31. 10.1002/pc.2575010.1002/pc.25750 ↗
32. 10.1002/pc.2567510.1002/pc.25675 ↗
33. 10.1002/pc.2530910.1002/pc.25309 ↗
34. 10.1016/j.compositesb.2021.10904610.1016/j.compositesb.2021.109046 ↗
35. 10.1016/j.marstruc.2004.03.00310.1016/j.marstruc.2004.03.003 ↗
36. 10.1002/pc.2564110.1002/pc.25641 ↗
37. 10.1002/pc.2625110.1002/pc.26251 ↗
38. 10.1177/07349041930110030510.1177/073490419301100305 ↗
39. Pering G. A. · J. Compos. Mater. · 1980 · 14 · 54
40. 2007 · 57844
41. 10.1016/j.firesaf.2021.10336610.1016/j.firesaf.2021.103366 ↗
42. 10.1177/073490411667942210.1177/0734904116679422 ↗
43. Marker T. R. · 1999
44. Webster H. · 1994
45. Ochs R.Development of the next generation fire test burner for powerplant fire testing applications. Proceeding of IASFPWG London 2010.
46. Mouritz A. P.;Gardiner C. P.;Mathys Z.;Townsend C. R.Post‐fire properties of composites burnt by cone calorimetry and large‐scale fire testing. Proceeding of the ICCM13 Beijing 2001.
47. Hode J. C. · 2012
48. 10.1016/j.applthermaleng.2018.02.02510.1016/j.applthermaleng.2018.02.025 ↗
49. Federal Aviation Administration · 2011
50. Rakow J. F. · 2007
51. Greenhalgh E. S. · 2009
52. Kwan W. · 2007
53. Clarkson E. · 2012
54. Man M. · 2012
55. Horner A. · 2000
56. Marker T. · 2019
57. 10.1533/9781845694701.3.39810.1533/9781845694701.3.398 ↗
58. Kilinc F. S. · 2013
59. Cahill P. · 1986
60. 10.1016/0010-4361(86)90746-910.1016/0010-4361(86)90746-9 ↗
61. Smith B. · 1986
62. 10.1016/j.compscitech.2007.05.03910.1016/j.compscitech.2007.05.039 ↗
63. 10.1016/j.compositesb.2021.10921710.1016/j.compositesb.2021.109217 ↗
64. 10.1016/j.compositesb.2018.09.01610.1016/j.compositesb.2018.09.016 ↗
65. 10.1002/pc.2453510.1002/pc.24535 ↗
66. 10.1016/j.polymdegradstab.2007.03.02310.1016/j.polymdegradstab.2007.03.023 ↗