journal article·2018-04

Aging characteristics of glass fiber‐reinforced polyamide in hot water and air

Klaus J. Geretschläger, Gernot M. Wallner

Polymer Composites· Volume 39· Issue 4
Publisher page

Abstract

This article focuses on the accelerated aging behavior of a glass fiber‐reinforced and heat stabilized polyamide grade. Accelerated aging of injection molded specimens was achieved by hot air exposure (HAE) and pressure cooker testing (PCT) at elevated temperatures. For both aging routines, characteristic aging indicators were found. For hot air exposure, the carbonyl index obtained from infrared spectra revealed superficial thermo oxidation. For pressure cooker testing, the development of a regular crack pattern and successive surface roughening were observed by light microscopy and laser confocal microscopy. This was accompanied by a significant reduction in molar mass assessed by viscometry. In addition, progressing degradation of mechanical performance was ascertained by tensile testing experiments. At the onset of material cracking, the molar mass was about 25% of the initial value. POLYM. COMPOS., 39:997–1005, 2018. © 2016 Society of Plastics Engineers
Source: crossref · Quality: baseline

Research context

OpenAlex topics: Polymer crystallization and properties · Natural Fiber Reinforced Composites · Mechanical Behavior of Composites

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

Affiliations

Johannes Kepler University Linz, Institute of Polymeric Materials and Testing, Altenberger Strasse 69 Linz 4040 Austria

Funding

European Commission within the Seventh Framework Programme (FP7)

References (26)

Show source-provided references
1. 10.1002/pc.2031210.1002/pc.20312 ↗
2. M.Köhl K.‐A.Weiß S.Saile P.Ohnewein D.Preiss S.Brunold B.Röder Y.Klinger A.Müller T.Lüftinger J.Rekstad M.Meir K.Schnetzinger G.M.Wallner andE.Hochreiter SCOOP ‐ Novel Materials Ideas and Designs for Solar Collectors Made of Polymers ‐ Newsletter 1. Available from:http://www.eu-scoop.org/downloads.htm(accessed on September 22 2015).
3. 10.1016/j.compositesb.2013.11.00110.1016/j.compositesb.2013.11.001 ↗
4. 10.1016/j.polymdegradstab.2009.04.00910.1016/j.polymdegradstab.2009.04.009 ↗
5. A.S.Maxwell W.R.Broughton G.Dean andG.D.Sims Review of accelerated aging methods and lifetime prediction techniques for polymeric materials NPL Report DEPC MPR 016 (2005).
6. 10.1016/j.polymdegradstab.2012.11.00210.1016/j.polymdegradstab.2012.11.002 ↗
7. 10.1016/j.polymdegradstab.2013.04.01210.1016/j.polymdegradstab.2013.04.012 ↗
8. 10.1002/app.2864710.1002/app.28647 ↗
9. 10.1016/j.polymdegradstab.2004.11.02010.1016/j.polymdegradstab.2004.11.020 ↗
10. 10.1016/j.polymdegradstab.2010.06.01810.1016/j.polymdegradstab.2010.06.018 ↗
11. 10.1016/j.polymdegradstab.2007.08.00710.1016/j.polymdegradstab.2007.08.007 ↗
12. 10.1021/i300006a00610.1021/i300006a006 ↗
13. K.J.Geretschläger G.M.Wallner andT.Ramschak Aging behavior and lifetime modelling of polyamide materials for integrated collector storeages Journal of Solar Energy Engineering: Including Wind Energy and Building Energy Conservation(submitted for publication).
14. 10.1016/j.polymdegradstab.2010.02.03010.1016/j.polymdegradstab.2010.02.030 ↗
15. Brandrup J. · 1999
16. 10.1122/1.54963310.1122/1.549633 ↗
17. Mechanische und thermische Eigenschaften Prüfnormen: EN ISO 527 Beuth Berlin [u.a.] (2004).
18. Hässler R. · 2007
19. T.Mettler Thermal Analysis Application Handbook: Thermoplast Collected Applications Mettler-Toledo AG Analytical Switzerland (2008). Available from:http://us.mt.com/us/en/home/applications/Application_Browse_Laboratory_Analytics/Application_Browse_thermal_analysis/TA_Appl_Handb/Thermoplastics.html.
20. 10.3390/ma608349410.3390/ma6083494 ↗
21. 10.1016/0008-6223(95)00117-V10.1016/0008-6223(95)00117-V ↗
22. Cho L.L. · Forensic Sci. J. · 2007 · 6 · 55
23. Smith E. · 2005
24. Y.Horiba Jobin Raman Data and Analysis: Raman Spectroscopy for Analysis and Monitoring HORIBA Jobin Yvon GmbH Germany (2015). Available from:http://www.horiba.com/de/scientific/products/raman-spectroscopy/raman-academy/.
25. Verleye G. · 2001
26. 10.1002/047001114910.1002/0470011149 ↗