Graphene oxide and graphene fiber produced by different nozzle size, feed rate and reduction time with vitamin C

The processing conditions of graphene oxide and graphene fibers are important for final fiber properties. The effect of different processing conditions such as feed rate, nozzle size (length and diameter), and reduction time by vitamin C on fiber properties such as morphology, mechanical properties and electrical conductivity has been analyzed. It has been observed that at the constant feed rates, increase in nozzle length results in higher mechanical properties. For the samples produced with long nozzle, thinner nozzle results to higher mechanical properties than thicker one. Decrease in nozzle length and increase in feed rate and reduction time by vitamin C resulted in an increased crimpy structure of fiber surface. Higher fiber strength was observed when the reduction time was decreased. The increase in the feed rate resulted in an increase of fiber linear densities (tex). All fibers experimented were in the semiconductor range. In this study, it has been seen that short, thin nozzles with 10 ml/h feed rate and reduction with 2.5 h provided better mechanical properties along with electrical conductivity.