La0.8Sr0.2Cr0.5Fe0.5O3- (LSCF) synthesized by molten salt method
Source abstract
Abstract
La0.8Sr0.2Cr0.5Fe0.5O3-δ was synthesised by the molten salt method using NaCl and KCl as the molten salt medium. The specimens were analysed by XRD, SEM, TG and DSC. The results are listed as follows. Firstly, all of them have orthorhombic crystalline perovskite structure under the conditions of 1000-1200 °C; the optimum temperature and holding time for the synthesis of La0.8Sr0.2Cr0.5Fe0.5O3-δ by the molten salt method is 1100°C for 3 hours. Secondly, the thermal and kinetic analysis allow the synthesis of La0.8Sr0.2Cr0.5Fe0.5O3-δ to be divided into three stages, with the first phase being the decomposition of La(OH)3, the second phase being the synthesis of LaFeO3, and the third phase being the synthesis of La0.8Sr0.2Cr0.5Fe0.5O3-δ, with the activation energies of 0.4408 (KJ·mol-1), 0.1188 (KJ·mol-1), and 0.3631 (KJ·mol-1). Finally, the synthesis mechanism of La0.8Sr0.2Cr0.5Fe0.5O3-δ powder synthesized by molten salt method is "dissolution-precipitation".
Source: openaire · Quality: candidate unverified · Source record ↗
Research context
OpenAlex topics: Advanced materials and composites · Metallurgical Processes and Thermodynamics · Nuclear materials and radiation effects
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (33)
Show source-provided references
1. Enhancing the performance of BaxMnO3 (x = 1, 0.9, 0.8, and 0.7) perovskites as catalysts for CO oxidation by decreasing the Ba content
2. Synthesis characterization and effect of La0.8Sr0.2CoO3-δ on the combustion performance of nitroamine-modified bibase propellant
3. Perovskite-type lanthanum ferrite-based photocatalysts: preparation, properties, and applications10.1016/j.jechem.2021.08.023 ↗
4. Tailoring the Composition of BaxBO3(B = Fe, Mn) Mixed Oxides as CO or Soot Oxidation Catalysts in Simulated GDI Engine Exhaust Conditions10.3390/molecules28083327 ↗
5. Oxygen activation on Ba-containing perovskite materials10.1126/sciadv.abn4072 ↗
6. Preparation and research of limiting current oxygen sensor based on Ce0.85Sm0.075Nd0.075O2-δ
7. Facile synthesis of lanthanum strontium cobalt ferrite (LSCF) nanopowders employing an ion-exchange promoted Sol-Gel process
8. Preparation of La0.7Sr0.3Co0.2Fe0.8O3-δ (LSCF 7328) by combination of mechanochemical and solid state reactions10.4028/www.scientific.net/KEM.744.399 ↗
9. Microstructure and performance analysis of solid oxide fuel cell cathode La0.6Sr0.4CoO3–δ–Ce0.8Gd0.2O2–δ co-synthesized by flame method and spray drying method
10. Zr0.84Y0.16O1.92–La0.8Sr0.2Cr0.5Fe0.5O3-δ dual-phase composite hollow fiber membrane targeting chemical reactor applications10.1016/j.memsci.2011.11.010 ↗
11. Preparation of La0.8Sr0.2Cr0.5Fe0.5O3-δ-Zr0.84Y0.16O1.92 asymmetric ceramic oxygen permeable membrane by gel casting
12. Application of perovskite La0.8Sr0.2Cr0.5Fe0.5O3-δ materials in solid oxide fuel cells
13. A high power density solid oxide fuel cell based on nanostructured La0.8Sr0.2Cr0.5Fe0.5O3-δ anode10.1016/j.electacta.2014.10.020 ↗
14. Exploration of using the molten salt method in the preparation of inorganic material powder
15. Preparation of lanthanum courate powder by low-temperature solid-phase reaction and its sintering properties
16. Research progress of iodine extraction methods
17. Preparation of nanocrystalline magnesium aluminum spinel powder by flame spray pyrolysis
18. Current status and prospect of spray drying technology
19. Facile synthesis of hexagonal boron nitride nanoplates via molten-salt-mediated magnesiothermic reduction10.1016/j.ceramint.2015.08.036 ↗
20. Effects of molten salt temperature and holding time on synthesis of hercynite by the molten salt method10.1016/j.ceramint.2022.01.012 ↗
21. Nano LiMn2O4 with spherical morphology synthesized by a molten salt method as cathodes for lithium ion batteries10.1039/c2ra01110g ↗
22. Electrochemical performances of LiFePO4/C composites prepared by the molten salt method10.1016/S1003-6326(09)60218-1 ↗
23. Evolved magnetoelectric physical properties of perovskite superlattices
24. Water absorbency of super absorbent polymer based on flexible polymeric network10.1016/j.eurpolymj.2022.111045 ↗
25. Preparation of lanthanum oxide powder and its effect on grain size
26. Growth of LaCoO3 crystals in molten salt: effects of synthesis conditions10.1039/D0CE01330G ↗
27. Structure and magnetic properties of perovskite manganites La2/3Sr1/3FexMn1-xO3
28. Magnetization reversal in orthorhombic Sr-doped LaFe0.5Cr0.5O3-δ
29. A new method of analyzing thermogravimetric data10.1246/bcsj.38.1881 ↗
30. A quick, direct method for the determination of activation energy from thermogravimetric data
31. Template growth mechanism of spherical Ni(OH)210.1007/s11771-007-0061-9 ↗
32. The effects of processing parameters on molten salt synthesis of CaZrO3 nanopowders using oxide precursors10.1016/j.powtec.2014.02.058 ↗
33. The effects of raw material particle size and salt type on formation of nano-CaZrO3 from molten salts10.1016/j.ceramint.2012.04.024 ↗