journal article·2004-01

Microstructural development of Y-α/(β)-sialons after post heat-treatment and its effect on mechanical properties

Feng Ye, Michael J Hoffmann, Stefan Holzer, Mikio Iwasa

Ceramics International· Volume 30· Issue 2
Publisher page

Abstract

Abstract Dense Y-α and duplex Y-α/β-sialon ceramics were fabricated by hot isostatic pressing (HIP) using the compositions with the formula Y m /3 Si 12-( m + n ) Al m + n O n N 16− n and extra addition of 2 wt.%Y 2 O 3 . The sintered materials were subsequently heat-treated at 1300–1700 °C to investigate the thermal stability of Y-sialons. The results show that α-sialon stabilized by yttrium has high thermal stability. An adjustment of α-sialon phase composition is the dominating reaction during annealing. Post heat-treatment has a little effect on the microstructure and properties of the Y-α/β-sialons, but significantly changes the morphology of α-phase grains in Y-α-sialons from elongated to equiaxed after heat-treatment at 1500 °C for extended time, hence decreasing its toughness.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Advanced ceramic materials synthesis · Nuclear materials and radiation effects · Advanced materials and composites

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (16)

Show source-provided references
1. Contribution to the phase diagram Si3N4–AlN–Al2O3–SiO210.1111/j.1151-2916.1975.tb11502.x ↗
2. The signification of structure and phase equilibria in the development of silicon nitride and sialon ceramics
3. Dense single-phase β-Sialon ceramics by glass-encapsulated hot isostatic pressing10.1007/BF01105715 ↗
4. Microstructural stability of duplex α-β-sialon ceramics10.1016/S0955-2219(96)00218-X ↗
5. Effect of composition, phase content and microstructure on the performance of yttrium sialon ceramics10.1016/0921-5093(89)90613-8 ↗
6. Optimizing mechanical properties and thermal stability of Ln-α-β-Sialon by using duplex Ln elements (Dy and Sm)10.1016/S0955-2219(98)00174-5 ↗
7. Effect of starting composition, type of rare earth sintering additive and amount of liquid phase on α⇆β sialon transformation10.1016/S0955-2219(96)00112-4 ↗
8. Composition of the effectiveness of rare-earth starting additives on the high-temperature stability α-sialon ceramics10.1007/BF01151503 ↗
9. Reversible α⇆β sialon transformation in heat-treatment sialon ceramics10.1016/0955-2219(93)90074-2 ↗
10. Homogeneity region and thermal stability of neodymium-doped α-sialon ceramic10.1111/j.1151-2916.1996.tb07935.x ↗
11. A critical evaluation of indentation techniques for measuring fracture toughness10.1111/j.1151-2916.1981.tb10320.x ↗
12. Microstructure and mechanical properties of in situ β- Si3N4/α′-sialon composite10.1111/j.1151-2916.1994.tb04604.x ↗
13. A tough sialon ceramic based on α- Si3N4 with a whisker-like microstructure10.1038/39542 ↗
14. Microstructure control of in-situ-toughened α-sialon ceramics10.1111/j.1151-2916.2000.tb01472.x ↗
15. Microstructure development of calcium α-sialon ceramics with elongated grains10.1111/j.1551-2916.1999.tb20079.x ↗
16. Hardness and toughness of α-sialon ceramics10.4028/www.scientific.net/MSF.325-326.219 ↗