journal article·2013-12Open access

Separation of the defect-free Fe3O4-Au core/shell fraction from magnetite-gold composite nanoparticles by an acid wash treatment

Hojatollah Montazeri, Amir Amani, Hamid Reza Shahverdi, Emad al din Haratifar, Ahmad Reza Shahverdi

Abstract

Abstract Some undesired nanoparticles, such as malformed structures or incomplete core/shell Fe3O4-Au nanocomposites, might be formed when Fe3O4-Au core/shell nanocomposites are being synthesized. These impurities should be separated before any applications are performed. In this investigation, magnetic cores (Fe3O4) were synthesized using a conventional fabrication method involving coprecipitation of Fe2+ and Fe3+. Carboxyl-capped magnetite-gold composite nanoparticles, measuring ≤50 nm, were then synthesized using a plant extract (Eucalyptus camaldulensis). The prepared carboxyl-capped magnetite-gold composite nanoparticles were further subjected to acid treatment for 18 h and characterized with different instrumentation methods. The results of the investigation showed that acid treatment can be applied successfully to separate defect-free Fe3O4-Au core/shell nanoparticles from different types of Fe3O4-Au nanocomposites, without any considerable changes in their physiochemical properties.
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Research context

OpenAlex topics: Nanoparticle-Based Drug Delivery · Iron oxide chemistry and applications · Nanomaterials for catalytic reactions

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

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