journal article·2016-11

Barium titanate nanometric polycrystalline ceramics fired by spark plasma sintering

Pavel Ctibor, Josef Sedlacek, Vasyl Ryukhtin, Jakub Cinert, Frantisek Lukac

Ceramics International· Volume 42· Issue 14
Publisher page

Abstract

Abstract A series of samples was sintered from nanometric BaTiO 3 powder by spark plasma sintering (SPS). Porosity on ultra-fine size scales, hardly accessible for quantification by conventional techniques, was measured by small angle neutron scattering (SANS). Band gap was estimated from diffuse reflectance measurements. Sintered tablets were polished, sputtered by aluminum to create electrode system and tested in DC and AC electric fields. The results were correlated with the SPS processing parameters and are discussed in connection with other BaTiO 3 samples produced by SPS with or without additional heat treatment. Majority of our SPS fired samples had, even without subsequent thermal treatment, advantageous combination of high permittivity, DC resistivity and low loss factor, seldom reported for SPS technology.
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Research context

OpenAlex topics: Ferroelectric and Piezoelectric Materials · Microwave Dielectric Ceramics Synthesis · Dielectric properties of ceramics

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

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