journal article·2012-04

One step simultaneous synthesis of modified-CVD-made V2O5/TiO2 nanocomposite particles

Min Young Song, Sungmin Chin, Jongsoo Jurng, Young-Kwon Park

Ceramics International· Volume 38· Issue 3
Publisher page

Abstract

Abstract A one step simultaneous synthesis of V 2 O 5 /TiO 2 nanocomposite particles was carried out using a modified-chemical vapor deposition (CVD) process employing two metal-organic precursors. The flow rate of the vanadium precursor was varied from 0 to 3 L/min with the flow rate of the TTIP precursor kept constant. The pure TiO 2 and prepared V 2 O 5 /TiO 2 nanocomposite particles were examined by BET, XRD, XPS, TEM and SEM-EDS. The results showed that both the vanadium concentration and particle size increased with increasing flow rate of the vanadium precursor, whereas the specific surface area decreased. XPS confirmed that the nanocomposite particles consisted of Ti, V and O. The V 2 O 5 /TiO 2 nanocomposite particles had a mean size of 20–40 nm. TEM showed that the flow rate had a significant effect on the particle size. The V 2 O 5 /TiO 2 nanocomposite particles are expected to have a wide range of applications in many fields, such as catalysts, photoelectron materials and sensors.
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Research context

OpenAlex topics: Catalysis and Oxidation Reactions · Catalytic Processes in Materials Science · Transition Metal Oxide Nanomaterials

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References (24)

Show source-provided references
1. Chlorinated organics total oxidation over V2O5/TiO2 catalysts prepared by polyol-mediated synthesis10.1016/j.apcata.2007.02.031 ↗
2. A fully oxidized V2O5/TiO2(001)-anatase system studied with in situ synchrotron photoelectron spectroscopy10.1016/j.susc.2005.03.055 ↗
3. Solid-state potentiometric SO2 sensor combining NASICON with V2O5-doped TiO2 electrode10.1016/j.snb.2008.04.003 ↗
4. Preparation and characterization of mesoporous VOx–TiO2 complex oxides for the selective oxidation of methanol to dimethoxymethane10.1016/j.jcis.2009.03.027 ↗
5. Mode of arrangement of components in mixed vanadia catalyst and its bearing for oxidation catalysis10.1016/S0926-860X(97)00020-3 ↗
6. Structure and reactivity of surface vanadium oxide species on oxide supports10.1016/S0926-860X(97)00021-5 ↗
7. Preparation and properties of vanadia/titania monolayer catalysts10.1016/S0926-860X(97)00024-0 ↗
8. Fabrication and characterization of Ag–TiO2 multiphase nanocomposite thin films with enhanced photocatalytic activity10.1016/j.apcatb.2005.03.009 ↗
9. Synthesis and characterization of high surface area TiO2/SiO2 mesostructured nanocomposite10.1016/j.solidstatesciences.2009.10.009 ↗
10. Influence of deposition temperature on the growth of vacuum evaporated V2O5 thin films10.1016/S0167-577X(03)00185-X ↗
11. Mechanism and characteristics of porous ZnO films by sol–gel method with PEG template10.1016/j.matlet.2007.08.010 ↗
12. Single-step synthesis of MWCNT/ZnO nanocomposite using co-chemical vapor deposition method10.1016/j.matlet.2009.10.015 ↗
13. Preparation of carbon nanotube by rotary CVD on Ni nano-particle precipitated cBN using nickelocene as a precursor10.1016/j.matlet.2010.09.074 ↗
14. Effect of reaction temperature on CVD-made TiO2 primary particle diameter10.1016/S0009-2509(03)00213-6 ↗
15. Synthesis of TiO2 nanoparticles by propane/air turbulent flame CVD process10.1016/j.partic.2009.03.003 ↗
16. Preparation of MnOx/TiO2 ultrafine nanocomposite with large surface area and its enhanced toluene oxidation at low temperature10.1016/j.powtec.2011.01.001 ↗
17. Structural, compositional and magnetic characterization of bulk V2O5 doped ZnO system10.1016/j.apsusc.2009.09.039 ↗
18. Preparation of mesoporous V2O5/TiO2 via spray pyrolysis and its application to the catalytic conversion of 1,2-dichlorobenzene10.1016/j.jiec.2010.12.013 ↗
19. Photocatalytic degradation of methylene blue with TiO2 nanoparticles prepared by a thermal decomposition process10.1016/j.powtec.2010.03.034 ↗
20. Catalytic abatement of acetaldehyde over oxide-supported precious metal catalysts10.1016/j.apcatb.2007.09.017 ↗
21. Phase development in the catalytic system V2O5/TiO2 under oxidising conditions10.1016/j.jeurceramsoc.2005.09.108 ↗
22. Low temperature fabrication of V-doped TiO2 nanoparticles, structure and photocatalytic studies10.1016/j.jhazmat.2009.04.068 ↗
23. Determination of the V2p XPS binding energies for different vanadium oxidation states (V5+ to V0+)10.1016/j.elspec.2004.03.004 ↗
24. Electrospun nanofibers of V-doped TiO2 with high photocatalytic activity10.1016/j.jcis.2010.05.067 ↗