journal article·2020-06

Quantitative phase analyses of biomedical pyrophosphate-bearing monetite and brushite cements by solid-state NMR and powder XRD

Hua Guo, Michael Pujari-Palmer, Yang Yu, Baltzar Stevensson, Håkan Engqvist, Mattias Edén

Ceramics International· Volume 46· Issue 8
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OpenAlex topics: Advanced NMR Techniques and Applications · Chemical Synthesis and Characterization · X-ray Diffraction in Crystallography

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References (60)

Show source-provided references
1. In vitro ageing of brushite calcium phosphate cement10.1016/S0142-9612(03)00293-X ↗
2. Amorphous calcium (ortho)phosphates10.1016/j.actbio.2010.06.031 ↗
3. Dicalcium phosphate cements: brushite and monetite10.1016/j.actbio.2011.08.005 ↗
4. Calcium phosphate cements: study of the β-tricalcium phosphate–monocalcium phosphate system10.1016/0142-9612(89)90089-6 ↗
5. Effects of sulfate, pyrophosphate, and citrate ions on the physicochemical properties of cements made of β-tricalcium phosphate-phosphoric acid-water mixtures10.1111/j.1151-2916.1996.tb08746.x ↗
6. Silver-doped calcium phosphate cements with antimicrobial activity10.1016/j.actbio.2011.06.049 ↗
7. Bioinspired mineral–organic bioresorbable bone adhesive10.1002/adhm.201800467 ↗
8. A novel class of injectable bioceramics that glue tissues and biomaterials10.3390/ma11122492 ↗
9. Adhesive cements that bond soft tissue ex vivo10.3390/ma12152473 ↗
10. The effect of amorphous pyrophosphate on calcium phosphate cement resorption and bone generation10.1016/j.biomaterials.2013.05.001 ↗
11. Cement formulations in the calcium phosphate H2O–H3PO4–H4P2O7 system10.1111/j.1551-2916.2005.00558.x ↗
12. Advanced solid-state 1H/31P NMR characterization of pyrophosphate-doped calcium phosphate cements for biomedical applications: the structural role of pyrophosphate10.1016/j.ceramint.2019.07.047 ↗
13. Mineralization followup with the use of NMR spectroscopy and others10.1002/jbm.10255 ↗
14. Solid state NMR to study calcium phosphate ceramics10.1016/0166-6622(90)80041-2 ↗
15. Nuclear magnetic resonance spectroscopy of bone substitutes10.1016/S8756-3282(99)00144-1 ↗
16. 31P Solid-state NMR study of the chemical setting process of a dual-paste injectable brushite cements10.1002/jbm.b.31372 ↗
17. The monetite structure probed by advanced solid-state NMR experimentation at fast magic-angle spinning10.3390/ijms20246356 ↗
18. PDF-4+ 2019 (Database)
19. FULLPROF: a program for Rietveld refinement and pattern matching analysis
20. An improved broadband decoupling sequence for liquid crystals and solids10.1006/jmre.1999.1896 ↗
21. Ramped-amplitude cross polarization in magic-angle-spinning NMR10.1006/jmra.1994.1208 ↗
22. Hydrogen bonding in the crystalline state. Structure of NaH2PO4·H2O (orthorhombic phase), and crystal chemistry of the NaH2PO4·nH2O series10.1107/S0567740876003051 ↗
23. Calcium phosphates and hydroxyapatite: solid-state NMR experiments and first-principles calculations10.1007/s00723-007-0040-1 ↗
24. High-resolution variable-temperature 31P NMR of solid calcium phosphates10.1021/ja00528a020 ↗
25. Structure refinement for Na2H2P2O7 from X-ray powder diffraction data
26. The crystal structure of β-Ca2P2O710.1107/S0365110X66004225 ↗
27. Crystal structure analysis of β-tricalcium phosphate Ca3(PO4)2 by neutron powder diffraction10.1016/S0022-4596(03)00279-2 ↗
28. Cation substitution in β-tricalcium phosphate investigated using multi-nuclear, solid-state NMR10.1016/j.jssc.2013.10.026 ↗
29. Crystal structure of brushite, calcium hydrogen orthophosphate dihydrate: a neutron-diffraction investigation10.1039/j19710003725 ↗
30. Hydrogen bonding in the crystalline state. CaHPO4 (monetite), P1¯or P1? A novel neutron diffraction study10.1107/S0567740877005706 ↗
31. Solid-state phosphorus-31 nuclear magnetic resonance studies of synthetic solid phases of calcium phosphate: potential models of bone mineral10.1021/bi00320a032 ↗
32. Solid-state 13C and 31P NMR analysis of urinary stones10.1016/S0022-5347(05)67327-2 ↗
33. Investigation of phosphorus site condensation in CaHPO4 by analysis of 31P MAS-NMR tensor and X-ray powder patterns10.1515/zna-2006-7-811 ↗
34. High-resolution solid state NMR experiments for the characterization of calcium phosphate biomaterials and biominerals10.1557/jmr.2011.250 ↗
35. Structure and cation effects on phosphorus-31 NMR chemical shifts and chemical-shift anisotropies of orthophosphates
36. The influence of short-range geometry on the 31P chemical-shift tensor in protonated phosphates10.1006/jmra.1994.1234 ↗
37. 1H MAS and 1H →31P CP/MAS NMR study of human bone mineral10.1007/s00223-002-2111-5 ↗
38. Hydrogen environments in calcium phosphates: 1H MAS NMR at high spinning speeds10.1021/ja00255a009 ↗
39. Proton distributions and hydrogen bonding in crystalline and glassy hydrous silicates and related inorganic materials: insights from high-resolution solid-state nuclear magnetic resonance spectroscopy10.1111/j.1551-2916.2009.03468.x ↗
40. A solid-state NMR investigation of the structure of nanocrystalline hydroxyapatite10.1002/mrc.1774 ↗
41. Three structural roles of water in bone observed by solid-state NMR10.1529/biophysj.105.070243 ↗
42. Proton environments in biomimetic calcium phosphates formed from mesoporous bioactive CaO–SiO2–P2O5 glasses in vitro: Insights from solid-state NMR10.1021/acs.jpcc.7b03469 ↗
43. Discrimination of surface and bulk structure of crystalline hydroxyapatite nanoparticles by NMR10.1021/acs.jpcc.5b08732 ↗
44. Significant precision in crystal structural details. Holly Springs hydroxyapatite10.1107/S0567740869004298 ↗
45. Hydrogen bond formation between citrate and phosphate ions in spherulites of fluorapatite10.1021/la402392b ↗
46. Citrate bridges between mineral platelets in bone10.1073/pnas.1315080111 ↗
47. Nitrogen-rich La–Si–Al–O–N oxynitride glass structures probed by solid state NMR10.1016/j.jnoncrysol.2007.07.027 ↗
48. MATLAB · 2013
49. Efficient symmetry-based homonuclear dipolar recoupling of quadrupolar spins: double-quantum NMR correlations in amorphous solids10.1039/b808295b ↗
50. Low-power broadband homonuclear dipolar recoupling in MAS NMR by two-fold symmetry pulse schemes for magnetization transfers and double-quantum excitation10.1016/j.jmr.2015.09.004 ↗
51. Na/Ca intermixing around silicate and phosphate groups in bioactive phosphosilicate glasses revealed by heteronuclear solid-state NMR and molecular dynamics simulations10.1021/acs.jpcb.5b01130 ↗
52. A unified 23Na NMR chemical shift correlation with structural parameters in multicomponent silicate-based glasses10.1111/jace.16852 ↗
53. 27Al NMR studies of aluminosilicate glasses10.1016/bs.arnmr.2015.04.004 ↗
54. First-principles calculations of NMR parameters for phosphate materials10.1002/mrc.2667 ↗
55. Enhanced stability and local structure in biologically relevant amorphous materials containing pyrophosphate10.1039/c1jm13930d ↗
56. From crystalline to amorphous calcium pyrophosphates: a solid state Nuclear Magnetic Resonance perspective10.1016/j.actbio.2015.10.016 ↗
57. The crystal structures of two calcium orthophosphates: CaHPO4 and Ca(H2PO4)2⋅H2O10.1524/zkri.1961.116.1-2.101 ↗
58. Hydrogen bonding in the cristalline state. NaH2PO4, a crystal structure with a short asymmetrical hydrogen bond10.1107/S0567740874002111 ↗
59. A crystallographic study of the sorption of cadmium on calcium hydroxyapatites: incidence of cationic vacancies10.1006/jssc.1996.0329 ↗
60. Low-temperature ordering of hydrogen atoms in CaHPO4 (monetite): X-ray and neutron diffraction study at 145 K10.1107/S0567740880003056 ↗