journal article·2021-01

Influence of fibres diameter on the AC and DC magnetic characteristics of Fe/Fe3O4 fibres based soft magnetic composites

B.V. Neamţu, M. Pszola, A. Opriş, F. Popa, T.F. Marinca, I. Chicinaş

Ceramics International· Volume 47· Issue 2
Publisher page

Abstract

Abstract Fibres-based soft magnetic composites (FSMCs) have been prepared by using Fe fibres of different diameters (65, 125, 250 and 500 μm). The Fe fibres were coated with a 3 μm thick layer of Fe3O4 via the blackening process and subsequently compacted at 700 MPa. The X-ray diffraction analysis (XRD) was used to prove the formation of the Fe3O4 coating on the surface of the fibres. The thickness and the uniformity of the coating were analysed via scanning electron microscopy (SEM) and energy-dispersive X-ray spectroscopy (EDX). The DC measurements performed on the composite cores revealed that the saturation induction increase from 1.36 to 1.68 T, the maximum relative permeability increase from 550 to 940, and the coercive field decrease from 796 to 454 A/m as the fibre's diameter increase from 65 to 500 μm. By using thinner fibres (65 and 125 μm), composites with low losses and stable initial relative permeability, in the frequency range 50 Hz–10 kHz, can be obtained. To distinguish between different types of losses dissipated by our compacts, and the influence of the fibre's diameter on the different components of the total losses, a numerical model for loss separation is proposed. The comparative evolution of the AC magnetic characteristics of the FSMCs and powder-based SMCs is presented. According to the presented results, this new type of composites can be successfully used to prepare magnetic cores designated to work in the medium to high-frequency range.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Magnetic Properties and Applications · Magnetic properties of thin films · Metallic Glasses and Amorphous Alloys

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (39)

Show source-provided references
1. Review of Fe-6.5 wt%Si high silicon steel—a promising soft magnetic material for sub-kHz application10.1016/j.jmmm.2019.02.089 ↗
2. Soft magnetic material status and trends in electric machines10.1109/TIE.2016.2613844 ↗
3. Soft magnetic composite materials (SMCs)10.1016/j.jmatprotec.2007.02.034 ↗
4. Past, present, and future of soft magnetic composites10.1063/1.5027045 ↗
5. Soft magnetic composites: recent advancements in the technology10.1016/j.mprp.2016.08.003 ↗
6. Preparation of Fe–Si–Ni soft magnetic composites with excellent high-frequency properties10.1016/j.jmmm.2014.12.073 ↗
7. AC magnetic properties of the soft magnetic composites based on Supermalloy nanocrystalline powder prepared by mechanical alloying10.1016/j.mseb.2012.03.029 ↗
8. Soft magnetic composites based on hybrid coated Fe-Si nanocrystalline powders10.1016/j.surfcoat.2017.09.088 ↗
9. Influence of resin type and content on electrical and magnetic properties of soft magnetic composites (SMCs)10.1016/j.powtec.2013.01.006 ↗
10. Design of novel soft magnetic composites based on Fe/resin modified with silica
11. Effect of heat treatment on magnetic properties of iron-based soft magnetic composites with Al2O3 insulation coating produced by sol–gel method10.1016/j.jallcom.2013.07.008 ↗
12. Magnetic properties of iron-based soft magnetic composites with SiO2 coating obtained by reverse microemulsion method10.1016/j.jmmm.2015.01.030 ↗
13. In-situ formation of Fe3O4 and ZrO2 coated Fe-based soft magnetic composites by hydrothermal method10.1016/j.ceramint.2018.11.058 ↗
14. Magnetic properties of iron-based soft magnetic composites with MgO coating obtained by sol–gel method10.1016/j.jmmm.2009.11.008 ↗
15. Properties of iron-based soft magnetic composite with iron phosphate–silane insulation coating10.1016/j.jallcom.2009.03.074 ↗
16. Innovative ferrite nanofibres reinforced soft magnetic composite with enhanced electrical resistivity10.1016/j.jallcom.2018.04.237 ↗
17. Preparation and characterization of iron-based soft magnetic composites with resin bonded nano-ferrite insulation10.1016/j.jallcom.2020.154416 ↗
18. Chemical synthesis of Fe/Fe3O4 core-shell composites with enhanced soft magnetic performances10.1016/j.jmmm.2016.12.006 ↗
19. NiZnCu-ferrite coated iron powder for soft magnetic composite applications10.1016/j.jmmm.2018.05.030 ↗
20. Evolution of the insulation matrix and influences on the magnetic performance of Fe soft magnetic composites during annealing10.1016/j.jallcom.2016.05.277 ↗
21. Enhanced magnetic properties of Fe soft magnetic composites by surface oxidation10.1016/j.jmmm.2015.09.054 ↗
22. Fabrication and growth mechanism of iron oxide insulation matrix for Fe soft magnetic composites with high permeability and low core loss10.1016/j.jallcom.2017.03.229 ↗
23. B.V. Neamţu, M. Pszola, H. Vermeşan, G. Stoian, M. Grigoraş, A. Opriş, L. Cotojman, T.F. Marinca, N. Lupu, I. Chicinaş, Preparation and characterisation of Fe/Fe3O4 fibres based soft magnetic composites, Ceram. Int., https://doi.org/10.1016/j.ceramint.2020.08.165.10.1016/j.ceramint.2020.08.165 ↗
24. Systematic investigation of particle size dependence of magnetic properties in soft magnetic composites10.1016/j.jmmm.2008.02.072 ↗
25. Influence of particle size and compaction pressure on the magnetic properties of iron-phenolic soft magnetic composites10.1016/j.jpcs.2009.08.008 ↗
26. The effect of compaction parameters and particle size on magnetic properties of iron-based alloys used in soft magnetic composites10.1016/j.mseb.2006.07.015 ↗
27. Interplay of domain walls and magnetization rotation on dynamic magnetization process in iron/polymer–matrix soft magnetic composites10.1016/j.jmmm.2016.11.084 ↗
28. Dependence of demagnetizing fields in Fe-based composite materials on magnetic particle size and the resin content10.1016/j.jmmm.2015.04.008 ↗
29. Preparation and characterisation of soft magnetic composites based on Fe fibres10.1007/s10853-019-04088-1 ↗
30. Properties of soft magnetic composites based on Fe fibres coated with SiO2 by hydrothermal method10.1016/j.jallcom.2020.154222 ↗
31. Soft magnetic composites based on oriented short Fe fibres coated with polymer10.1016/j.jallcom.2020.155731 ↗
32. Features of formation of magnetite coatings on low-carbon steel in hot nitrate solutions10.1134/S1023193510100113 ↗
33. An electrochemical route for hot alkaline blackening of steel: a nitrite free approach10.3390/surfaces2020017 ↗
34. Effect of iron particle size and volume fraction on the magnetic properties of Fe/silicate glass soft magnetic composites10.1016/j.jmmm.2014.09.019 ↗
35. Cullity · 2009
36. Magnetic coercivity of Fe3O4 particle systems10.1063/1.348145 ↗
37. On the law of hysteresis10.1109/T-AIEE.1892.5570437 ↗
38. Weiss · 1974
39. Jiles · 1991