Nanostructural, morphological and magnetic studies of PEG/Mn(1−)Zn()Fe2O4 nanoparticles synthesized by co-precipitation
Source abstract
Abstract
Abstract The coating of Polyethylene Glycol (PEG) on zinc substituted manganese ferrite nanoparticles has been reported in the present study. Single phase nanoferrites bearing the chemical formula Mn (1− x ) Zn ( x ) Fe 2 O 4 (0.0≤ x ≤1.0) were produced under low reaction temperature of 75 °C and their morphological, structural and magnetic characterizations were performed. The prepared ferrites were characterized using X-ray diffraction (XRD), field emission scan electron microscopy images (FE-SEM), Fourier transform infrared spectroscopy (FT-IR) and vibrating sample magnetometer (VSM) techniques. XRD revealed the formation of spinel single-phase structure for the samples with Zn-content. The crystallite sizes estimated using Scherer formula were in the range 4.50–15.89 nm. The characteristic bands of PEG as observed in its Fourier transform infrared spectrum technique were also present in PEG layer on Mn–Zn ferrite nanoparticles, hence confirming its presence. The presence of PEG on Mn (1− x ) Zn ( x ) Fe 2 O 4 nanoparticles, spherical formation of PEG coated Mn (1− x ) Zn ( x ) Fe 2 O 4 nanoparticles and reduced agglomeration in the Mn (1− x ) Zn ( x ) Fe 2 O 4 nanoparticles were revealed by FE-SEM. The measurements of magnetic properties at room temperature by VSM showed that all samples behaved superparamagnetic with magnetization ( M ) and coercivity in the range of 1.86–20.66 emu/g and 12.922–30.253 Oe, respectively. The M–H loop of all the samples is narrow with low value of coercivity and retentivity; indicating the superparamagnetic nature of these samples.
Source: openaire · Quality: candidate unverified · Source record ↗
Research context
OpenAlex topics: Magnetic Properties and Synthesis of Ferrites · Electromagnetic wave absorption materials · Multiferroics and related materials
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (70)
Show source-provided references
1. Influence of cobalt on structural and magnetic properties of nickel ferrite nanoparticles10.1016/j.molstruc.2013.08.040 ↗
2. Study of conduction phenomena in indium substituted Mn–Zn nano-ferrites10.1016/j.jmmm.2014.12.031 ↗
3. Preparation and characteristics of Fe3O4-encapsulated BaTiO3 powder by ultrasound-enhanced ferrite plating10.1016/j.jmmm.2003.12.925 ↗
4. Synthesis, structural and dielectric properties of Cr3+ substituted Fe3O4 nano-particles10.1016/j.ceramint.2014.04.061 ↗
5. Modified ferrite plating of Fe3O4 and CuFe2O4 thin films10.1016/S0304-8853(99)00750-7 ↗
6. Preparation of NiFe2O4 architectures for affinity separation of histidine-tagged proteins10.1016/j.matlet.2015.01.039 ↗
7. Synthesis, characterization, magnetic and electrical properties of polyaniline/NiFe2O4 nanocomposite10.1016/j.synthmet.2013.12.022 ↗
8. Cost effective preparation and characterization of nanocrystalline nickel ferrites (NiFe2O4) in low temperature regime10.1016/j.jksus.2014.12.006 ↗
9. Structural and transport properties of nanocrystalline MnFe2O4 synthesized by co-precipitation method10.1016/j.solidstatesciences.2012.08.026 ↗
10. Polyvinylpyrrolidone (PVP)/MnFe2O4 nanocomposite: sol–gel autocombustion synthesis and its magnetic characterization10.1016/j.ceramint.2012.12.081 ↗
11. Synthesis of the nanocrystalline CoFe2O4 ferrite thin films by a novel sol–gel method using glucose as an additional agent10.1016/j.mseb.2011.12.017 ↗
12. Effects of applied magnetic field and pressures on the magnetic properties of nanocrystalline CoFe2O4 ferrite10.1016/j.jmmm.2010.03.003 ↗
13. Optimization of sol–gel synthesis of CoFe2O4 nanowires using template assisted vacuum suction method10.1016/j.jmmm.2014.06.058 ↗
14. Structure and magnetic properties of La substituted ZnFe2O4 nanoparticles synthesized by sol–gel autocombustion method10.1016/j.jmmm.2014.06.062 ↗
15. Structural, magnetic and electrical properties of nanocrystalline zinc ferrite10.1016/j.jallcom.2010.12.168 ↗
16. Physical properties and cation arrangement of oxides with spinel structures I. Cation arrangement in spinels10.1063/1.1746464 ↗
17. Study of structural, electrical and magnetic properties of Cr doped Ni–Mg ferrite nanoparticle10.1016/j.jallcom.2014.03.013 ↗
18. Cation distribution in NiZn‐ferrite films via extended x‐ray absorption fine structure10.1063/1.115591 ↗
19. Structural, microstructural and magnetic properties of NiFe2O4, CoFe2O4 and MnFe2O4 nanoferrite thin films10.1016/j.jmmm.2011.07.029 ↗
20. Reducing the inversion degree of MnFe2O4 nanoparticles through synthesis to enhance magnetization: evaluation of their 1H NMR relaxation and heating efficiency10.1039/C4DT00162A ↗
21. Magnetic properties of nanostructured ferrimagnetic zinc ferrite
22. Structural evolution of ball-milled ZnFe2O410.1016/S0925-8388(01)02011-4 ↗
23. Magnetism of the nanostructured spinel zinc ferrite10.1016/S1359-6462(02)00598-5 ↗
24. Magnetic properties of MnZn ferrite nanoparticles obtained by SHS and sol–gel autocombustion techniques10.1016/j.ceramint.2013.11.133 ↗
25. MnZn ferrite synthesized by sol–gel auto-combustion and microwave digestion routes using spent alkaline batteries10.1016/j.ceramint.2014.11.019 ↗
26. Structural and magnetic properties of Cr doped NiZn-ferrite nanoparticles prepared by surfactant assisted hydrothermal technique10.1016/j.ceramint.2015.01.079 ↗
27. Structural and magnetic properties of cadmium substituted manganese ferrites prepared by hydrothermal route10.1016/j.jmmm.2012.09.004 ↗
28. Characteristics and synthesis of Cu–Ni ferrite nanopowders by coprecipitation method with ultrasound irradiation10.1016/j.jmmm.2003.12.926 ↗
29. Magnetic properties of nanocrystalline Ni–Zn, Zn–Mn, and Ni–Mn ferrites synthesized by reverse micelle technique10.1016/j.physb.2003.12.017 ↗
30. Synthesis, structural and magnetic behavior studies of Zn–Al substituted cobalt ferrite nanoparticles10.1016/j.molstruc.2015.02.006 ↗
31. Effect of Cu–Al substitution on the structural and magnetic properties of Co ferrites10.1016/j.mssp.2015.01.025 ↗
32. Magnetic and structural properties of nano sized Dy-doped cobalt ferrite synthesized by co-precipitation10.1016/j.jmmm.2014.01.016 ↗
33. Magnetic properties of Co1−xZnxFe2O4 spinel ferrite nanoparticles synthesized by starch-assisted sol–gel autocombustion method and its ball milling10.1016/j.jmmm.2014.11.027 ↗
34. Structural and magnetic properties of Ni1−xZnxFe2O4 nano-crystalline ferrites prepared via novel chitosan method10.1016/j.molstruc.2014.01.070 ↗
35. The effect of polyvinyl alcohol (PVA) coating on structural, magnetic properties and spin dynamics of Ni0.3Zn0.7Fe2O4 ferrite nanoparticles10.1016/j.jmmm.2013.08.004 ↗
36. Characterization and magnetic properties of polyethylene glycol modified NiZn ferrite thin films10.1016/j.cap.2010.08.023 ↗
37. Water dispersible oleic acid-coated Fe3O4 nanoparticles for biomedical applications10.1016/j.jmmm.2014.10.137 ↗
38. Synthesis and characterization of carboxymethyl dextran-coated Mn/Zn ferrite for biomedical applications10.1016/j.jmmm.2009.05.023 ↗
39. Interfacing of dextran coated ferrite nanomaterials with cellular system and delayed hypersensitivity on Guinea pigs10.1016/j.colsurfb.2013.10.033 ↗
40. Synthesis and characterization of magnetite nanoparticles coated with lauric acid10.1016/j.matchar.2013.04.001 ↗
41. Effect of hydrolyzing agents on the properties of poly (ethylene glycol)-Fe3O4 nanocomposite10.1007/BF03353655 ↗
42. Synthesis and characterization of ZnFe2O4 magnetic nanoparticles via a PEG-assisted route10.1016/j.jallcom.2007.07.121 ↗
43. Cation distribution and magnetic properties of Zn doped NiFe2O4 nanoparticles synthesized by PEG-assisted hydrothermal route10.1016/j.jallcom.2009.01.014 ↗
44. Structural and magnetic properties of Ni0.8Co0.2−2xCuxMnxFe2O4 spinel ferrites prepared via solution combustion route10.1016/j.jmmm.2015.03.020 ↗
45. Study of the magnetic structure and the cation distributions in MnCo spinel ferrites10.1016/j.physb.2015.01.008 ↗
46. Characterization of soft magnetic spinel ferrite coating prepared by plasma spray10.1016/j.surfcoat.2014.09.029 ↗
47. Influence of Al3+ion concentration on the crystal structure and magnetic anisotropy of nanocrystalline spinel cobalt ferrite10.1016/j.jmmm.2011.03.010 ↗
48. Synthesis, characterization and magnetic properties of monodisperse Ni, Zn-ferrite nanocrystals10.1016/j.jmmm.2014.12.006 ↗
49. Preparation of Zn–Mn ferrite from spent Zn–Mn batteries using a novel multi-step process of bioleaching and co-precipitation and boiling reflux10.1016/j.hydromet.2015.02.007 ↗
50. Structural and magnetic properties of ZnMg-ferrite nanoparticles prepared using the co-precipitation method10.1016/j.ceramint.2012.12.023 ↗
51. Nonstoichiometric zinc ferrite nanocrystals: syntheses and unusual magnetic properties10.1021/jp991626i ↗
52. Synthesis, structure and magnetic properties of nanocrystalline ZnxMn1−xFe2O4 prepared by ball milling10.1016/j.jallcom.2007.11.112 ↗
53. Preparation and characterization of polyethylene glycol coated silica nanoparticles for drug delivery application
54. Infrared study of biocompatible magnetic nanoparticles
55. Structural and magnetic properties of pure and doped nanocrystalline cadmium ferrite10.1016/j.jallcom.2008.08.034 ↗
56. Synthesis and characterization of nano-crystalline Zn-substituted Mg–Ni–Fe–Cr ferrites via surfactant-assisted route10.1016/j.molstruc.2013.10.056 ↗
57. Low temperature hydrothermal synthesis and characterization of Mn doped cobalt ferrite nanoparticles10.1016/j.ceramint.2012.01.001 ↗
58. Studies on the magnetic, magnetostrictive and electrical properties of sol–gel synthesized Zn doped nickel ferrite10.1016/j.jallcom.2011.02.163 ↗
59. AC and DC conductivity of NiZn ferrite nanoparticles in wet and dry conditions10.1016/j.jmmm.2010.02.039 ↗
60. On the chemical synthesis and drug delivery response of folate receptor-activated, polyethylene glycol-functionalized magnetite nanoparticles10.1016/j.actbio.2007.06.006 ↗
61. Synthesis and magnetic properties of Mn–Zn ferrite nanoparticles10.1016/j.jmmm.2006.11.200 ↗
62. Surface spin disorder in NiFe2O4 nanoparticles10.1103/PhysRevLett.77.394 ↗
63. Low temperature synthesis of Ni0.8Zn0.2Fe2O4 powder and its characterization10.1016/0167-577X(96)00010-9 ↗
64. Nanocrystallite size effect on σs and Hc in nanoparticle assemblies10.1016/S0921-4526(02)01785-4 ↗
65. Dielectric properties of NiZn ferrites prepared by the citrate precursor method10.1016/S0921-5107(99)00019-7 ↗
66. Magnetic nanoparticles10.1016/S0304-8853(99)00347-9 ↗
67. Magnetic and structural properties of nickel zinc ferrite nanoparticles synthesized at room temperature10.1063/1.1715132 ↗
68. Brabers · 1995 · 8 · 189
69. Synthesis and characterization of surfactant-coated superparamagnetic monodispersed iron oxide nanoparticles10.1016/S0304-8853(00)01224-5 ↗
70. On the suitability of nanocrystalline ferrites as a magnetic carrier for drug delivery: functionalization, conjugation and drug release kinetics10.1016/j.actbio.2006.10.006 ↗