Synthesis of high-purity bulk Ti2AlN by spark plasma sintering (SPS)
Source abstract
Abstract
Abstract Single-phase bulk Ti 2 AlN was prepared by spark plasma sintering (SPS) at 1200 °C of Ti/Al/TiN powders in stoichiometric proportion. Investigated by X-ray diffraction (XRD) of samples and the sintering process parameter, the reaction procedure could be analyzed. Scanning electron microscopy (SEM) and electron probe micro-analysis (EPMA) coupled with energy-dispersive spectroscopy (EDS) were utilized to investigate the morphology characteristics. When sintered at 1200 °C, Ti 2 AlN phase was well developed with a close and lamellated structure. The distribution of Ti 2 AlN grains was homogeneous.
Source: openaire · Quality: candidate unverified · Source record ↗
Research context
OpenAlex topics: MXene and MAX Phase Materials · Metal and Thin Film Mechanics · Advanced ceramic materials synthesis
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References (5)
Show source-provided references
1. Processing and characterization of Ti2AlC, Ti2AlN and Ti2AlC0.5N0.510.1007/s11661-006-0243-3 ↗
2. Microstructure and nonbasal-plane of epitaxial Ti2AlN thin films10.1063/1.2161943 ↗
3. Single-crystal Ti2AlN thin films10.1063/1.1882752 ↗
4. Layered machinable ceramics for high temperature applications10.1016/S1359-6462(96)00418-6 ↗
5. Effect of shock-activation of post-shock reaction synthesis of ternary ceramics