journal article·2014-09

Novel preparation of hydroxyapatite nanoparticles and nanorods with the aid of complexing agents

Fatemeh Mohandes, Masoud Salavati-Niasari, Zeinab Fereshteh, Mohammadhossein Fathi

Ceramics International· Volume 40· Issue 8
Publisher page

Abstract

Abstract New complexing agents based on Schiff base compounds have been employed to fabricate nanocrystalline hydroxyapatite (HAP). The use of the Schiff bases derived from 2-hydroxybenzophenone led to the formation of HAP nanoparticles and nanorods. Moreover, hollow needle-like nanorods of HAP were formed in the presence of the Schiff base derived from 2-aminophenol. In the crystal growth mechanism proposed for HAP crystals, zero-dimensional (0-D) and one-dimensional (1-D) nanostructures were generated by considering tetradentate and bidentate coordination modes of the Schiff bases, respectively. The synthesized products were characterized by several techniques including proton nuclear magnetic resonance ( 1 H NMR) spectroscopy, transmission electron microscopy (TEM) and X-ray powder diffraction (XRD).
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Bone Tissue Engineering Materials · X-ray Diffraction in Crystallography · Thermal and Kinetic Analysis

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (27)

Show source-provided references
2. Synthesis and characterization of hydroxyapatite nanoparticles and their application in protein adsorption10.1016/j.mseb.2010.03.011 ↗
3. Evaluation and characterization of nanostructure hydroxyapatite powder prepared by simple sol–gel method10.1016/j.matlet.2007.01.028 ↗
4. Synthesis of nanocrystalline hydroxyapatite from Ca(OH)2 and H3PO4 assisted by ultrasonic irradiation10.1016/j.ceramint.2010.05.008 ↗
5. Preparation of nanosized hydroxyapatite particles at low temperatures10.1007/s10853-005-4222-7 ↗
6. Synthesis and characterization of hydroxyapatite nanopowders by emulsion technique10.1021/cm0303437 ↗
7. Structural and spectroscopic studies of hydroxyapatite nanorods formed via microwave-assisted synthesis route10.1111/j.1551-2916.2012.05134.x ↗
8. Synthesis of nanosize single-crystal hydroxyapatite via mechanochemical method10.1016/j.matlet.2008.11.030 ↗
9. Synthesis and characterization of HAP nanorods from a cationic surfactant template method
10. Preparation and characterization of thermally stable nanohydroxyapatite
11. Defect-induced photoluminescence and third-order nonlinear optical response of chemically synthesized chalcopyrite CuInS2 nanoparticles10.1016/j.cplett.2008.10.055 ↗
12. Effects of organic modifiers on the size-controlled synthesis of hydroxyapatite nanorods10.1016/j.apsusc.2006.07.025 ↗
13. Capping agent-assisted synthesis of nanosized hydroxyapatite: comparative studies of their physicochemical properties10.1016/j.jmatprotec.2006.11.013 ↗
14. Size-controlled synthesis of hydroxyapatite nanorods by chemical precipitation in the presence of organic modifiers10.1016/j.msec.2006.10.001 ↗
15. Synthesis of hydroxyapatite particles in catanionic mixed surfactants template10.1016/j.matchemphys.2011.07.078 ↗
16. Preparation of large-sized hydroxyapatite single crystals using homogenous releasing controls10.1016/j.jcrysgro.2007.08.009 ↗
17. Mittheilungen aus dem universitätslaboratorium in pisa: eine neue reihe organischer basen10.1002/jlac.18641310113 ↗
18. Sonochemical and hydrothermal synthesis of PbTe nanocrystals with the aid of a novel capping agent10.1016/j.materresbull.2013.07.010 ↗
19. Schiff-base assisted synthesis of lead selenide nanocrystals10.1016/j.materresbull.2012.12.076 ↗
20. Sonochemical synthesis and characterization of lead iodide hydroxide micro/nanocrystals10.1016/j.ultsonch.2013.05.007 ↗
21. Formation mechanism of nano-sized hydroxyapatite powders through spray pyrolysis of a calcium phosphate solution containing polyethylene10.1016/j.jeurceramsoc.2012.08.029 ↗
22. Structural and spectroscopic studies of hydroxyapatite nanorods formed via microwave-assisted synthesis route10.1111/j.1551-2916.2012.05134.x ↗
23. Sol–gel synthesis of amorphous calcium phosphate and sintering into microporous hydroxyapatite bioceramics10.1111/j.1151-2916.1998.tb02499.x ↗
24. Surfactant-assisted synthesis of hydroxyapatite particles10.1016/j.matlet.2006.02.077 ↗
25. The role of hydrated silica, titania, and alumina in inducing apatite on implants10.1002/jbm.820280103 ↗
26. Infrared spectra of carbonate apatites: v2-region bands10.1016/j.biomaterials.2008.12.007 ↗
27. Location of type B carbonate ion in type A–B carbonate apatite synthesized at high pressure10.1016/j.jssc.2004.04.002 ↗