journal article·2015-12Open access

Hydrothermal synthesis, growth mechanism and gas sensing properties of Zn-doped α-Fe2O3 microcubes

HaoJie Song, Yali Sun, XiaoHua Jia

Ceramics International· Volume 41· Issue 10

Abstract

Monodisperse Zn-doped α-Fe 2 O 3 microcubes were prepared via a facile hydrothermal method with zinc ions as the structure-directing agents. The observations of FE-SEM and TEM showed that the obtained sample has a quasi-cubic shape with an edge length of about 250 nm. It can be found that the dosage of Zn 2+ in the solution had a remarkable effect on the morphology of as synthesized samples. The element analyses of the fabricated microcubes were carried out by XPS and EDS . The investigation on the evolution formation revealed that Zinc ions were critical for controlling the assembly of microcubes. Moreover, the gas sensors based on Zn-doped α-Fe 2 O 3 microcubes were fabricated and the gas sensing performances were investigated. It was found that the gas sensor exhibited high response, good selectivity, fast response and recovery time to acetone at the working temperature of 240 °C.
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Research context

OpenAlex topics: Gas Sensing Nanomaterials and Sensors · Analytical Chemistry and Sensors · Electrochemical Analysis and Applications

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References (24)

Show source-provided references
1. A laser ablation method for the synthesis of crystalline semiconductor nanowires10.1126/science.279.5348.208 ↗
2. Nearly monodisperse and shape-controlled CdSe nanocrystals via alternative routes: nucleation and growth10.1021/ja0173167 ↗
3. Direct electrodeposition of ZnO nanotube arrays in anodic alumina membranes10.1021/jp0711242 ↗
4. Conductive framework supported high rate performance of SnO2 hollow nanofibers for lithium battery anodes
5. Iron oxides semiconductors are efficients for solar water disinfection: a comparison with photo-Fenton processes at neutral pH10.1016/j.apcatb.2014.12.007 ↗
6. Preparation and gas sensing properties of vanadium oxide nanobelts coated with semiconductor oxides10.1016/j.snb.2005.10.012 ↗
7. Multilayered ZnO nanosheets with 3D porous architectures: synthesis and gas sensing application10.1021/jp100792c ↗
8. Electrospun In2O3/α-Fe2O3 heterostructure nanotubes for highly sensitive gas sensor applications10.1039/c3ce40962g ↗
9. Hollow α-Fe2O3 quasi-cubic structures: hydrothermal synthesis and gas sensing properties10.1016/j.matlet.2014.01.047 ↗
10. α-Fe2O3 nanotubes in gas sensor and lithium-ion battery applications10.1002/adma.200401101 ↗
11. Cu-doped α-Fe2O3 hierarchical microcubes: synthesis and gas sensing properties10.1016/j.snb.2013.12.015 ↗
12. Controllable fabrication and growth mechanism of hematite cubes10.1002/crat.201000642 ↗
13. Single-crystal α-Fe2O3 hexagonal nanorings: stepwise influence of different anionic ligands (F− and SCN− anions)10.1039/C0CC03632C ↗
14. Controllable fabrication, growth mechanism, and gas sensing properties of hollow hematite polyhedral10.1039/c2jm34826h ↗
15. Synthesis,characterization, and photocatalytic activity of Zn-Doped SnO2 hierarchical architectures assembled by nanocones10.1021/jp9021272 ↗
16. Metal ions induce growth and magnetism alternation of α-Fe2O3 crystals bound by high-index facets10.1002/chem.201201108 ↗
17. Cornell · 2004 · 525
18. Ristic · J. Mol. Struct. · 2007 · 834 · 45410.1016/j.molstruc.2006.10.016 ↗
19. Controllable fabrication and growth mechanism of hematite cubes10.1002/crat.201000642 ↗
20. Improved photocatalytic and gas sensing properties of α-Fe2O3 nanoparticles derived from β-FeOOH nanospindles10.1016/j.ceramint.2013.07.070 ↗
21. Al-doped ZnO for highly sensitive CO gas sensors10.1016/j.snb.2014.01.068 ↗
22. Characterization of Zn-doped hematite thin films for photoelectrochemical splitting of water
23. New approaches for improving semiconductor gas sensors10.1016/0925-4005(91)80213-4 ↗
24. Synthesis, characterization and gas sensing properties of undoped and Zn-doped γ-Fe2O3-based gas sensors10.1016/j.msea.2006.08.013 ↗