Preparation and mechanical properties of reinforced hydroxyapatite bone cement with nano-ZrO2
Source abstract
Abstract
Abstract In the research described, a new method was investigated to prepare hydroxyapatite (HAp) bone cement using nano-hydroxyapatite, CaO and (NH 4 ) 2 HPO 4 as initial raw materials, and reinforcement effects of HAp bone cement with ZrO 2 nanotubes and ZrO 2 nanoparticles were studied in detail. The morphologies, crystal structure and mechanical properties etc. were characterized by scanning electron microscope (SEM), transmission electron microscope (TEM), X-ray diffractometer (XRD), and electro-mechanical universal testing machine. Results indicated that after solidification the composition of bone cement was hydroxyapatite with good crystallinity and purity. Addition of ZrO 2 nanoparticles or ZrO 2 nanotubes to the bone cement could substantially improve its strength, the optimum addition amount being 20 wt%, however, the enhancement effects between ZrO 2 nanoparticles and ZrO 2 nanotubes were slightly different.
Source: openaire · Quality: candidate unverified · Source record ↗
Research context
OpenAlex topics: Bone Tissue Engineering Materials · Orthopaedic implants and arthroplasty · Titanium Alloys Microstructure and Properties
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (35)
Show source-provided references
1. Processing and properties of hydroxyapatite-based biomaterials for use as hard tissue replacement implants10.1557/JMR.1998.0015 ↗
2. The mechanical properties and osteoconductivity of hydroxyapatite bone scaffolds with multi-scale porosity10.1016/j.biomaterials.2006.08.021 ↗
3. Bone tissue engineering with porous hydroxyapatite ceramics10.1007/s10047-005-0292-1 ↗
4. Porosity-graded hydroxyapatite ceramics to replace natural bone10.1016/S0142-9612(00)00290-8 ↗
5. Development of a, b-plane-oriented hydroxyapatite ceramics as models for living bones and their cell adhesion behavior10.1016/j.actbio.2013.02.001 ↗
6. The characteristics of a hydroxyapatite–chitosan–PMMA bone cement10.1016/j.biomaterials.2004.01.022 ↗
7. Hydroxyapatite cement: an alternative for craniofacial skeletal contour refinements10.1054/bjps.1999.3236 ↗
8. Poly (lactide-co-glycolide)/hydroxyapatite composite scaffolds for bone tissue engineering10.1016/j.biomaterials.2005.08.016 ↗
9. Nano-hydroxyapatite composite biomaterials for bone tissue engineering—a review10.1166/jbn.2014.1893 ↗
10. The promotion of osteointegration under diabetic conditions using chitosan/hydroxyapatite composite coating on porous titanium surfaces10.1016/j.biomaterials.2014.05.028 ↗
11. Electrodeposition of hydroxyapatite coating on AZ91D magnesium alloy for biomaterial application10.1016/j.matlet.2008.02.048 ↗
12. The effect of hydroxyapatite coating on bone growth into porous titanium alloy implants10.1302/0301-620X.71B2.2925737 ↗
13. Bioactive titanium for implants and bone substitutes10.4028/www.scientific.net/KEM.587.387 ↗
14. Augmentation of acrylic bone cement with multiwall carbon nanotubes10.1002/jbm.a.30651 ↗
15. Fatigue testing and performance of acrylic bone-cement materials: state-of-the-art review10.1002/jbm.b.10018 ↗
16. Temperature elevation caused by bone cement polymerization during vertebroplasty10.1016/S8756-3282(99)00127-1 ↗
17. Physical characterization and osteogenic activity of the quaternized chitosan-loaded PMMA bone cement10.1016/j.actbio.2012.03.013 ↗
18. An injectable calcium phosphate cement for the local delivery of paclitaxel to bone10.1016/j.biomaterials.2011.04.010 ↗
19. Calcium phosphate cements: study of the β-tricalcium phosphate—dicalcium phosphate—calcite cements10.1016/0142-9612(90)90121-6 ↗
20. K. Ishikawa, Calcium phosphate cement, Advances in Calcium Phosphate Biomaterials, Springer, 2014, pp. 199–227.10.1007/978-3-642-53980-0_7 ↗
21. Setting reactions and compressive strengths of calcium phosphate cements10.1177/00220345900690121201 ↗
22. Calcium phosphate cements for bone substitution: chemistry, handling and mechanical properties10.1016/j.actbio.2013.11.001 ↗
23. Injectable biphasic calcium phosphate cements as a potential bone substitute10.1002/jbm.b.33018 ↗
24. Apatitic calcium phosphates: possible dental restorative materials
25. A new calcium-phosphate setting cement
26. Ectopic osteogenesis with biphasic ceramics of hydroxyapatite and tricalcium phosphate in rabbits10.1016/S0142-9612(01)00119-3 ↗
27. Differences of bone bonding ability and degradation behaviour in vivo between amorphous calcium phosphate and highly crystalline hydroxyapatite coating10.1016/0142-9612(95)00357-6 ↗
28. In vivo evaluation of plasma sprayed hydroxyapatite coatings having different crystallinity10.1016/S0142-9612(03)00545-3 ↗
29. Biocompatibility of various dental materials in contemporary dentistry: a narrative insight10.1111/j.2041-1626.2012.00140.x ↗
30. Abrasive machining of porcelain and zirconia with a dental handpiece10.1016/S0043-1648(03)00195-9 ↗
31. Fabrication parameter-dependent morphologies of self-organized ZrO2 nanotubes during anodization10.1007/s10008-011-1516-3 ↗
32. Transparent nanocrystalline yttria-stabilized-zirconia calvarium prosthesis10.1016/j.nano.2013.08.002 ↗
33. Porous ZrO2 bone scaffold coated with hydroxyapatite with fluorapatite intermediate layer10.1016/S0142-9612(03)00162-5 ↗
34. Reinforcement of denture base PMMA with ZrO2 nanotubes10.1016/j.jmbbm.2014.01.003 ↗
35. Freestanding ZrO2 nanotube membranes made by anodic oxidation and effect of heat treatment on their morphology and crystalline structure10.1039/c0jm03903a ↗