journal article·2017-08

Bulk boron carbide nanostructured ceramics by reactive spark plasma sintering

D.O. Moskovskikh, K.A. Paramonov, A.A. Nepapushev, N.F. Shkodich, A.S. Mukasyan

Ceramics International· Volume 43· Issue 11
Publisher page

Abstract

Abstract Bulk boron carbide (B 4 C) ceramics was fabricated from a boron and carbon mixture by use of one-step reactive spark plasma sintering (RSPS). It was also demonstrated that preliminary high-energy ball milling (HEBM) of the B+C powder mixture leads to the formation of B/C composite particles with enhanced reactivity. Using these reactive composites in RSPS permits tuning of synthesized B 4 C ceramic microstructure. Optimization of HEBM + RSPS conditions allows rapid (less than 30 min of SPS) fabrication of B 4 C ceramics with porosity less than 2%, hardness of ~35 GPa and fracture toughness of ~ 4.5 MPa m 1/2
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Research context

OpenAlex topics: Advanced ceramic materials synthesis · Advanced materials and composites · Boron and Carbon Nanomaterials Research

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