journal article·2011-12

Analysis of structural, thermal and dielectric properties of LiTi2(PO4)3 ceramic powders

R. Ramaraghavulu, S. Buddhudu

Ceramics International· Volume 37· Issue 8
Publisher page

Abstract

Abstract Lithium titanium phosphate (LiTi2(PO4)3) ceramic powders have been prepared by a solid state reaction method at five different temperatures (800 °C, 900 °C, 1000 °C, 1100 °C and 1200 °C for 5 h each). The XRD profiles have shown that the sample sintered at 1100 °C (optimized) has displayed well-defined features. XRD peaks are in good agreement with the JCPDS Card No. 35-0754 confirming the rhombohedral structure in a space group of R 3 ¯ c . The SEM images of the five samples sintered have been examined. EDAX and Raman spectra have been obtained for the LiTi2(PO4)3 ceramic powder sintered at 1100 °C for analysis. Thermal properties for the as prepared precursor LiTi2(PO4)3 sample, have been analyzed from the TG-DTA profiles. Besides this, dielectric constant, dielectric loss and conductivities (σac and σdc) have also been studied for the LiTi2(PO4)3 ceramic powder.
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Research context

OpenAlex topics: Microwave Dielectric Ceramics Synthesis · Ferroelectric and Piezoelectric Materials · Advanced Battery Materials and Technologies

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