Microwave assisted synthesis of biomorphic hydroxyapatite
Source abstract
Abstract
Abstract Hydroxyapatite has been synthesized using eggshell membrane as bio-template along with the assistance of microwave heating. Eggshell membrane is infiltrated with calcium and phosphorous precursors before heating it in a domestic microwave oven. Hydroxyapatite formed retained the interwoven hierarchical structure of the eggshell membrane. Structural analysis was performed using X-ray diffraction, and the microstructural features are characterized by scanning electron microscopy. Distinct morphological features were present in microwave processed hydroxyapatite when compared to the conventionally processed one. Transmission electron microscopic investigations and BET surface area analysis were also carried out.
Source: openaire · Quality: candidate unverified · Source record ↗
Research context
OpenAlex topics: Bone Tissue Engineering Materials · Additive Manufacturing and 3D Printing Technologies · Collagen: Extraction and Characterization
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (36)
Show source-provided references
1. Biomimetic and bioinspired synthesis of nanomaterials/nanostructures10.1002/adma.201503215 ↗
2. Biochemistry of the organic matrix of the eggshell110.3382/ps.0612040 ↗
3. Collagens of the chicken eggshell membranes10.3109/03008209109152162 ↗
4. Eggshell membrane biomaterial as a platform for applications in materials science10.1016/j.actbio.2014.03.020 ↗
5. Synthesis of biomorphic ZnO interwoven microfibers using eggshell membrane as the biotemplate10.1016/j.matlet.2006.06.091 ↗
6. Nano-silver-decorated microfibrous eggshell membrane: processing, cytotoxicity assessment and optimization, antibacterial activity and wound healing
7. Synthesis and characterizations of hierarchical biomorphic titania oxide by a bio-inspired bottom-up assembly solution technique10.1016/j.jssc.2006.12.027 ↗
8. Biomimetic metal oxides for the extraction of nanoparticles from water10.1039/c3nr34221b ↗
9. Water soluble blue-emitting AuAg alloy nanoparticles and fluorescent solid platforms for removal of dyes from water10.1039/C4RA14176H ↗
10. Development of biomorphic alumina using egg shell membrane as bio-template10.1016/j.ceramint.2017.11.173 ↗
11. Synthesis of ZnO through biomimetization of eggshell membranes using different precursors and its characterization10.1016/j.ceramint.2015.08.005 ↗
12. Microwave versus conventional sintering: a review of fundamentals, advantages and applications10.1016/j.jallcom.2010.01.068 ↗
13. Microwave processing of ceramics10.1016/S1359-0286(98)80011-9 ↗
14. Rapid microwave synthesis of hydroxyapatite phosphate microspheres with hierarchical porous structure10.1016/j.ceramint.2017.12.247 ↗
15. Preparation of a porous hydroxyapatite-carbon composite with the bio-template of sugarcane top stems and its use for the Pb(II) removal10.1016/j.jclepro.2018.03.275 ↗
16. A green sorbent of esterified egg-shell membrane for highly selective uptake of arsenate and speciation of inorganic arsenic10.1016/j.talanta.2013.07.061 ↗
17. Amide modes and protein conformation10.1016/0167-4838(92)90261-B ↗
18. Lecithin-based wet chemical precipitation of hydroxyapatite nanoparticles10.1007/s00396-015-3557-0 ↗
19. Synthesis and characterization of biomimetic hydroxyapatite nanoconstruct using chemical gradient across lipid bilayer10.1021/acsami.5b09042 ↗
20. Chemical characterization of silicon-substituted hydroxyapatite10.1002/(SICI)1097-4636(19990315)44:4<422::AID-JBM8>3.0.CO;2-# ↗
21. Development of hydroxyapatite derived from Indian coral10.1016/0142-9612(96)87651-4 ↗
22. Research of calcium phosphates using fourier transform infrared spectroscopy
23. Synthesis of nano-hydroxyapatite (nHA) from waste mussel shells using a rapid microwave method10.1016/j.matchemphys.2014.11.016 ↗
24. Acclerated microwave processing of nanocrystalline hydroxyapatite10.1007/s10853-005-2957-9 ↗
25. Densification behaviour and mechanisms of synthetic hydroxyapatites10.1016/S0955-2219(00)00154-0 ↗
26. Hinklin · 2009
27. Microwave effect in the fast synthesis of microporous materials: which stage between nucleation and crystal growth is accelerated by microwave irradiation?10.1002/chem.200700098 ↗
28. Microwave chemistry for inorganic nanomaterials synthesis10.1039/b9nr00377k ↗
29. Microwave synthesis of zeolites: 1. Reactor engineering10.1021/jp037358c ↗
30. Microwave-assisted preparation of inorganic nanostructures in liquid phase10.1021/cr400366s ↗
31. Flower-like agglomerates of hydroxyapatite crystals formed on an egg-shell membrane10.1016/j.colsurfb.2010.10.006 ↗
32. Brunauer · 1945
33. Reporting physisorption data for gas/solid systems with special reference to the determination of surface area and porosity (Recommendations 1984)10.1351/pac198557040603 ↗
34. Hierarchically ordered networks comprising crystalline ZrO2 tubes through sol-gel mineralization of eggshell membranes10.1039/b301077e ↗
35. Synthesis of hierarchical mesoporous titania with interwoven networks by eggshell membrane directed sol–gel technique10.1016/j.micromeso.2006.09.041 ↗
36. Characterization of micro and mesoporous solids by physisorption methods and pore-size analysis10.1016/S0926-860X(98)00164-1 ↗