journal article·2018-05

Solution combustion synthesis of ZnO powders using CTAB as fuel

H. Vahdat Vasei, S.M. Masoudpanah, M. Adeli, M.R. Aboutalebi

Ceramics International· Volume 44· Issue 7
Publisher page

Abstract

Abstract Zinc oxide (ZnO) powders have been prepared by solution combustion synthesis method using cetyltrimethylammonium bromide (CTAB) as fuel. The effects of fuel to oxidant ratios (ϕ = 0.5, 0.75, 1 and 1.5) on the combustion behavior, phase evolution, microstructure, optical properties and photocatalytic performance were investigated by thermal analysis, X-ray diffractometry, electron microscopy, and diffuse reflectance spectrometry techniques. The slow decomposition rate of CTAB guaranteed the direct formation of single phase and well-crystalline ZnO powders regardless of fuel content. The specific surface area of the as-combusted ZnO powders with platelet particles increased from 21 ± 1 to 35 ± 2 m 2 /g with fuel content. The band gap energy also increased from 2.99 to 3.13 eV due to the decrease of particle size. The as-combusted ZnO powders at ϕ = 1.5 exhibited the highest photodegradation (~69%) of methylene blue under ultraviolet light irradiation, due to their good crystallinity and smaller particle size.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: ZnO doping and properties · Catalytic Processes in Materials Science · Advanced Photocatalysis Techniques

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

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