journal article·2006-01

Hydroxyapatite formation on oxide films containing Ca and P by hydrothermal treatment

Fu Liu, Fuping Wang, Tadao Shimizu, Kaoru Igarashi, Liancheng Zhao

Ceramics International· Volume 32· Issue 5
Publisher page

Abstract

Abstract Oxide films were formed on titanium by means of microarc oxidation (MAO) using a direct current power supply. The oxide films containing Ca and P were obtained in an electrolyte containing β-glycerophosphate sodium salt pentahydrate (β-GP) and calcium acetate (CA). The surfaces of the oxide films were rough and porous, and the concentration of Ca and P were 7.3 mol% and 6.4 mol%, respectively, when MAO was performed in an electrolyte containing 0.04 M β-GP and 0.10 M CA at 200 A/m 2 current density and 430 V final voltage. The oxide film consists of anatase, rutile and an amorphous phase. After hydrothermal treatment at 190 °C, the hydroxyapatite crystals were precipitated on the oxide film surfaces. The amount of hydroxyapatite crystals increased by increasing the hydrothermal treatment time and the Ca/P ratio in the oxide film.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Bone Tissue Engineering Materials · Titanium Alloys Microstructure and Properties · Dental Implant Techniques and Outcomes

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (18)

Show source-provided references
1. Osseointegrated titanium implants10.3109/17453678108991776 ↗
2. Review-titanium alloys in total joint replacement-a materials science perspective10.1016/S0142-9612(97)00146-4 ↗
3. Electrodeposition of apatite coating on pure titanium and titanium alloys10.1007/BF00776358 ↗
4. Preparation and characterization of hydroxyapatite coating on Ti6Al4V alloy by a sol–gel method10.1111/j.1151-2916.1999.tb01719.x ↗
5. The effect of alkali- and heat-treatment titanium and apatite-formed titanium on osteoblastic differentiation of bone marrow cells10.1002/1097-4636(20001215)52:4<652::AID-JBM9>3.0.CO;2-W ↗
6. Structural characterization of pulsed laser-deposited hydroxyapatite film on titanium substrate10.1016/S0142-9612(97)00024-0 ↗
7. Preparation of bioactive titanium metal via anodic oxidation treatment10.1016/S0142-9612(03)00626-4 ↗
8. Functionally graded Ti/HAP coatings on Ti–6Al–4V obtained by chemical solution deposition10.1016/S0272-8842(01)00055-4 ↗
9. Six-year of hydroxyapatite-coated total hip replacement10.1302/0301-620X.77B4.7615595 ↗
10. Changes in phases and crystallinity of plasma-sprayed hydroxyapatite coatings under heat treatment: a quantitative study10.1002/jbm.820291204 ↗
11. In vivo tensile testing of fluorapatite and hydroxyapatite plasma-sprayed coatings10.1002/jbm.820280506 ↗
12. Graded surface structure of bioactive titanium prepared by chemical treatment10.1002/(SICI)1097-4636(199905)45:2<100::AID-JBM4>3.0.CO;2-0 ↗
13. Formation of a bioactive graded surface structure on Ti–15Mo–5Zr–3Al alloy by chemical treatment10.1016/S0142-9612(99)00190-8 ↗
14. Apatite formation induced by silica gel in a simulated body fluid10.1111/j.1151-2916.1992.tb04470.x ↗
15. Apatite formation on zirconium metal treated with aqueous NaOH10.1016/S0142-9612(01)00110-7 ↗
16. The role of hydrated silica, titania, and alumina in inducing apatite on implants10.1002/jbm.820280103 ↗
17. Preparation of bioactive titanium metal via anodic oxidation treatment10.1016/S0142-9612(03)00626-4 ↗
18. Preparation of bioactive Ti and its alloys via simple chemical surface treatment10.1002/(SICI)1097-4636(199611)32:3<409::AID-JBM14>3.0.CO;2-B ↗