journal article·2010-03

Properties of Si3N4–TiN composites fabricated by spark plasma sintering by using a mixture of Si3N4 and Ti powders

Norhayati Ahmad, Hidekazu Sueyoshi

Ceramics International· Volume 36· Issue 2
Publisher page

Abstract

Abstract Si 3 N 4 –TiN composites were successfully fabricated via planetary ball milling of 70 mass% Si 3 N 4 and 30 mass% Ti powders, followed by spark plasma sintering (SPS) at 1250–1350 °C. The sintering mechanism for SPS was a hybrid of dissolution–reprecipitation and viscous flow. The electrical resistivity decreased with increasing sintering temperature up to a minimum at 1250 °C and then increased with the increasing sintering temperature. The composites prepared by SPS at 1250–1350 °C could be easily machined by electrical discharge machining. Composite prepared by SPS at 1300 °C showed a high hardness (17.78 GPa) and a good machinability.
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Research context

OpenAlex topics: Advanced ceramic materials synthesis · Advanced materials and composites · Metal and Thin Film Mechanics

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