journal article·2014-01

ZnO nanoswords and nanopills: Hydrothermal synthesis, characterization and optical properties

A. Moulahi, F. Sediri

Ceramics International· Volume 40· Issue 1
Publisher page

Abstract

Abstract Nanostructured hexagonal zinc oxide pills and swords-like were hydrothermally synthesized using zinc sulfate heptahydrate (ZnSO4·7H2O) as an inorganic precursor and adipic acid (HOOC(CH2)4COOH) as a structure-directing agent. The structure, the crystallinity, the morphology and the composition of the materials were investigated by X-ray diffraction (XRD), scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FTIR), Raman spectroscopy and X-ray photoelectron spectroscopy (XPS). XRD study demonstrated the existence of wrutzite ZnO of high degree of crystallinity with crystallite size in the range of 70–80 nm. The optical properties of the as-synthesized ZnO were investigated by UV–visible absorption and room temperature photoluminescence (RTPL). The band gap for ZnO nanswords and nanopills was found to be 3.25 and 3.27 eV, respectively.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: ZnO doping and properties · Gas Sensing Nanomaterials and Sensors · Ga2O3 and related materials

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (59)

Show source-provided references
1. A comprehensive review of ZnO materials and devices10.1063/1.1992666 ↗
2. Amino acid-assisted synthesis of ZnO hierarchical architectures and their novel photocatalytic activities10.1021/cg800126r ↗
3. ZnO/TiO2nanocable structured photoelectrodes for CdS/CdSe quantum dot co-sensitized solar cells10.1039/C2NR32663A ↗
4. Transparent electrode with ZnO nanoparticles in tandem organic solar cells10.1016/j.solmat.2010.04.020 ↗
5. A comparative studyon electroluminescence from ZnO-based double heterojunction light emitting diodesgrown on different lattice mismatch substrates10.1016/j.jallcom.2013.04.036 ↗
6. Synthesis and ethanol sensing properties of selfassembled monocrystalline ZnO nanorod bundles by poly (ethylene glycol)-assisted hydrothermal process10.1021/jp8082166 ↗
7. Synthesis of CdZnO thin film as a potential candidate for optical switches10.1016/j.optlastec.2010.02.009 ↗
8. Ag nanoparticle embedded ZnO nanorods synthesized via a photochemical method and its gas-sensing properties10.1016/j.snb.2009.10.007 ↗
9. Synthesis, surfacemodification and photocatalytic property of ZnO nanoparticles10.1016/j.powtec.2008.07.004 ↗
10. Influence of size scale and morphology onantibacterial properties of ZnO powders hydrothemally synthesized using different surface stabilizing agents10.1016/j.colsurfb.2012.07.033 ↗
11. ZnOnanofluids: green synthesis, characterization, and antibacterial activity10.1016/j.matchemphys.2010.01.020 ↗
12. Staircase in the electron mobility of a ZnO quantum dot assembly due to shell filling10.1103/PhysRevLett.89.036801 ↗
13. Diameter dependent photocatalytic activity of ZnO nanowires grown by vapor transport technique10.1016/j.cplett.2012.04.054 ↗
14. ZnO based nanowires grown by chemical vapour deposition for selective hydrogenation of acetylene alcohols10.1039/c1cy00074h ↗
15. Room temperature ZnO growth by rf magnetron sputtering on top of photoactive P3HT: PCBM for organic solar cells10.1039/C0JM02354J ↗
16. One-step synthesis of Zn/ZnO hollow nanoparticles by the laser ablation in liquid technique10.1088/1612-2011/10/5/055903 ↗
17. Chemical synthesis and visible photoluminescence emission from monodispersed ZnO nanoparticles
18. Hydrothermal electrochemical synthesis of ZnO nanorods10.1021/cg9003593 ↗
19. The effect of aminoalcohols (MEA, DEA and TEA) on morphological control of nanocrystalline ZnO powders and its optical properties10.1016/j.jpcs.2010.01.008 ↗
20. Template-free synthesis of zinc oxide hollow microspheres in aqueous solution at low temperature10.1021/jp077573j ↗
21. Hydrothermal synthesis of nanostructured zinc oxide and study of their optical properties10.1016/j.materresbull.2011.12.027 ↗
22. Modelling and simulation of continuous hydrothermal flow synthesis process for nano-materials manufacture10.1016/j.supflu.2011.07.002 ↗
23. Low temperature synthesis of flowerlike ZnO nanostructures by cetyltrimethylammonium bromide-assisted hydrothermal process10.1021/jp036826f ↗
24. Solvothermal growth of highly oriented wurtzite-structured ZnO nanotube arrays on zinc foil10.1002/crat.200800633 ↗
25. ZnO nanocones: solvothermal synthesis and photoluminescence properties10.1016/j.materresbull.2007.08.023 ↗
26. Effect of hydrothermal temperature on structure and photochromic properties of WO3 powder10.1016/j.apt.2011.02.009 ↗
27. Low temperature solution synthesis and characterization of ZnO nano-flowers10.1016/j.materresbull.2006.11.035 ↗
28. Surface polarity-dependent cathodoluminescence in hydrothermally grown ZnO hexagonal rods10.1021/jp209834d ↗
29. Effective conversion efficiency enhancement of solar cell using ZnO/PS antireflection coating layers10.1016/j.solener.2011.10.030 ↗
30. Effect of surface groups on the luminescence property of ZnO nanoparticles synthesized by sol–gel route10.1016/j.susc.2011.09.006 ↗
31. Raman study of structural disorder in ZnO nanopowders10.1002/jrs.2546 ↗
32. Surface enhanced Raman scattering and photoluminescence properties of catalytic grown ZnO nanostructures10.1007/s00339-009-5309-9 ↗
33. Hierarchical shelled ZnO structures made of bunched nanowire arrays10.1002/adfm.200600390 ↗
34. A novel mercury-media route to synthesize ZnO hollow microspheres10.1016/j.ceramint.2009.11.017 ↗
35. Preparation of ZnO nanorods and optical characterizations10.1016/j.physe.2005.02.005 ↗
36. Low temperature synthesis and characterization of rosette-like nanostructures of ZnO using solution process10.1016/j.solidstatesciences.2008.07.009 ↗
37. Micro-Raman and XPS studies of pure ZnO ceramics10.1016/j.physb.2010.03.020 ↗
38. Synthesis of nanowires, nanorods and nanoparticles of ZnO through modulating the ratio of water to methanol by using a mild and simple solution method10.1016/j.matchemphys.2004.09.006 ↗
39. Improvement of optical properties of post-annealed ZnO nanorods10.1016/j.physe.2010.04.013 ↗
40. Reversible band gap tuning of metal oxide films using hydrogen and oxygen plasmas10.1016/j.tsf.2012.12.044 ↗
41. X-ray photoelectron spectroscopy and auger electron spectroscopy studies of Al-doped ZnO films10.1016/S0169-4332(99)00601-7 ↗
42. Chemical synthesis and visible photoluminescence emission from monodispersed ZnO nanoparticles
43. Rapid chemical synthesis and optical properties of ZnO ellipsoidal nanostructures10.1016/j.apt.2010.02.010 ↗
44. Controllable synthesis of ZnO nanocrystals via a surfactant-assisted alcohol thermal process at a low temperature10.1016/j.matlet.2005.04.031 ↗
45. The ultraviolet emission mechanism of ZnO thin film fabricated by sol–gel technology10.1016/j.jeurceramsoc.2007.02.053 ↗
46. Optical properties and electronic structure of amorphous germanium10.1002/pssb.19660150224 ↗
47. Microbundles of zinc oxide nanorods: assembly in ionic liquid [EMIM]+[BF4]−, photoluminescence and photocatalytic properties10.1016/j.jssc.2011.01.032 ↗
48. Room-temperature surface-erosion route to ZnO nanorod arrays and urchin-like assemblies10.1002/chem.200400498 ↗
49. Directed assembly of ZnO nanowires on a Si substrate without a metal catalyst using a patterned ZnO seed layer10.1088/0957-4484/16/2/020 ↗
50. ZnO nanocrystals: surprisingly ‘Alive’10.1021/cm902240c ↗
51. Carrier recombination dynamics through defect states of ZnO nanocrystals: from nanoparticles to nanorods10.1016/j.cplett.2012.05.028 ↗
52. Synthesis of ZnO nanowire arrays and their photoluminescence property10.1016/j.jallcom.2009.01.005 ↗
53. Preparation and photocatalytic property of a novel dumbbell-shaped ZnO microcrystal photocatalyst10.1016/j.jhazmat.2009.08.022 ↗
54. Interaction of hydrogen with ZnO nanopowders-evidence of hydroxyl group formation10.1088/0957-4484/23/1/015705 ↗
55. Raman study of the influence of hydrogen on defects in ZnO10.1063/1.2748719 ↗
56. Wet chemical approaches to patterned arrays of well-aligned ZnO nanopillars assisted by monolayer colloidal crystals10.1021/cm802839u ↗
57. Mechanisms behind green photoluminescence in ZnO phosphor powders10.1063/1.362349 ↗
58. Oriented growth of urchin-like zinc oxide micro/nano-scale structures in aqueous solution10.1016/j.materresbull.2012.01.006 ↗
59. Catalytic growth of zinc oxide nanowires by vapor transport10.1002/1521-4095(200101)13:2<113::AID-ADMA113>3.0.CO;2-H ↗