Preparation and characterization of TiO2, ZnO, and TiO2/ZnO nanofilms via sol–gel process

Abstract The preparation of the TiO 2 , ZnO, and TiO 2 /ZnO nanofilms was conducted on glass via sol–gel process. The prepared film was detailedly characterized by means of OM, SEM, XRD, and EDS. The results showed that the obtained pure TiO 2 was composed of nanoparticles. For pure ZnO it consisted of nanoparticles and large agglomerates. Both the microstructural morphology and the crystallization of the prepared TiO 2 /ZnO composite film were strongly related to the Ti/Zn ratio in the film. With a Ti/Zn ratio less than 1/1, the composite film was absence of cracks. Poor crystallization was definitely observed for the composite film with Ti/Zn ratio of 3/1 and 1/1. The EDS analysis revealed homogeneous distribution of Ti and Zn elements in the film.