Properties of β-Ca3(PO4)2 bioceramics prepared using nano-size powders
Source abstract
Abstract
Abstract Nano-size β-TCP powders with average grain size of 100 nm were prepared by the precipitation method. The sinterability of the nano-size powders, and the microstructure, mechanical strength and the in vitro degradability of the prepared β-TCP bioceramics were investigated. The results showed that the nano-size powders possessed superior sintering properties as compared to the micro-size powders. The densification temperature and phase transition temperature of β-TCP bioceramics prepared using nano-size powders was clearly lower than that prepared using micro-size powders, and the maximum value of the bending strength, elastic modulus, Vickers hardness and compressive strength of the samples fabricated from nano-size powders were more than two-times higher as compared to those of samples fabricated from micro-size powders. Furthermore, the degradability of the β-TCP bioceramics fabricated from nano-size powders was much lower than for micro-size powders, suggesting the possible control of the degradability of the bioceramics by regulating powder size.
Source: openaire · Quality: candidate unverified · Source record ↗
Research context
OpenAlex topics: Bone Tissue Engineering Materials · Orthopaedic implants and arthroplasty · Advanced materials and composites
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (40)
Show source-provided references
1. LeGeros · 1993
2. Bioceramics10.1111/j.1151-2916.1998.tb02540.x ↗
3. Tricalcium phosphate as a bone substitute
4. Clinical applications of calcium phosphate biomaterials: a review10.1016/0272-8842(93)90050-2 ↗
5. Qu · 1994 · 7 · 91
6. Calcium phosphate ceramics as bone substitutes
7. Bioceramics: material characteristic versus in vivo behavior10.1002/j.1097-4636.1987.tb00019.x ↗
8. Evolution of bone transplantation: molecular, cellular and tissue strategies to engineer human bone10.1016/0142-9612(96)85762-0 ↗
9. Synthesis and fabrication of β-tricalcium phosphate ceramics for potential prosthetic application10.1007/BF01028337 ↗
10. Sintering and characterization of HA and TCP bioceramics with control of their strength and phase purity10.1023/A:1018538212328 ↗
11. The effect of powder processing on densification, microstructure and mechanical properties of hydroxyapatite10.1016/S0272-8842(01)00102-X ↗
12. The cleavage strength of polycrystals
13. Dependence of mechanical strength of brittle polycrystalline specimens on porosity and grain size10.1111/j.1151-2916.1959.tb13596.x ↗
14. Comparison of stress concentration versus minimum solid area based mechanical property—porosity relations10.1007/BF00367582 ↗
15. Dense polycrystalline β-tricalcium phosphate for prosthetic applications10.1007/BF00591468 ↗
16. Oriented growth of surface grains in sintered β-tricalcium phosphate bioceramics10.1016/S0167-577X(00)00346-3 ↗
17. Fabricating densified hydroxyapatite ceramics from a precipitated precursor10.1016/S0167-577X(98)00160-8 ↗
18. Synthesis, characterization and thermal behavior of apatitic tricalcium phosphate10.1016/S0254-0584(02)00466-2 ↗
19. In-situ synthesis of biphasic calcium phosphate ceramics using microwave irradiation10.1016/S0254-0584(01)00293-0 ↗
20. Structural characterization of room-temperature synthesized nano-sized β-tricalcium phosphate10.1016/j.biomaterials.2003.10.046 ↗
21. Manufacture of macroporous calcium hydroxyapatite bioceramics10.1016/S0955-2219(99)00131-4 ↗
22. Use of commercial porous ceramic particles for sustained drug delivery10.1016/S0378-5173(02)00357-5 ↗
23. 1996
24. Pore and grain growth kinetics10.1111/j.1151-2916.1969.tb11941.x ↗
25. 1922
26. Elliott · 1994
27. Preparation of α- and β-TCP ceramics, with and without magnesium addition10.1016/0272-8842(94)90050-7 ↗
28. Phase diagrams of Ca3(PO4)2–Mg3(PO4)2 and Ca3(PO4)2–CaNaPO4 systems10.1246/bcsj.31.201 ↗
29. The biodegradation mechanism of calcium phosphate biomaterials in bone10.1002/jbm.10259 ↗
30. Degradation of calcium phosphate ceramics10.1002/(SICI)1097-4636(199901)44:1<78::AID-JBM9>3.0.CO;2-6 ↗
31. Biodegradation behavior of various calcium phosphate materials in bone tissue10.1002/jbm.820170505 ↗
32. Evaluation of a biodegradable ceramic10.1002/jbm.820110204 ↗
33. Biodegradable ceramic implants in bone10.1016/0030-4220(71)90238-6 ↗
34. Review on the dissolution models of calcium apatites10.1016/S0960-8974(02)00004-9 ↗
35. In vitro stability of biphasic calcium phosphate ceramics10.1016/0142-9612(93)90122-I ↗
36. Effect of bioactive ceramic composition and structure on in vitro behaviour. III. Porous versus dense ceramics10.1002/jbm.820281108 ↗
37. de Groot · 1988
38. An investigation of bioactive glass powders by sol-gel processing10.1002/jab.770020403 ↗
39. Degradation behavior of a new bioceramics: Ca2P2O7 with addition of Na4P2O7·10H2O10.1016/S0142-9612(97)00016-1 ↗
40. Macroporous calcium phosphate ceramics for bone substitution: a tracer study on biodegradation with 45Ca tracer10.1016/0142-9612(91)90053-D ↗