journal article·2009-03

Mullite whiskers derived from kaolin

B.M. Kim, Y.K. Cho, S.Y. Yoon, R. Stevens, H.C. Park

Ceramics International· Volume 35· Issue 2
Publisher page

Abstract

Abstract Short mullite whiskers prepared by firing compacts of kaolin and NH 4 Al(SO 4 ) 2 ·12H 2 O powders, with a small addition (0.8, 1.5 wt%) of NaH 2 PO 4 ·2H 2 O, in air 1300 and 1400 °C for 15 h have been characterized in terms of whisker morphology, composition and structure. Relatively uniform whisker shaped crystals grew within the silicate glass matrix. After chemically leaching the glass matrix with HF solution using a microwave heating source, the resulting whiskers were exposed as isolated crystals and exhibited an aspect ratio of >17 (∼0.5 μm in diameter). The mullite whiskers had a composition of 51.06 mol% Al 2 O 3 and 48.94 mol% SiO 2 , with an orthorhombic crystallographic structure.
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Research context

OpenAlex topics: Glass properties and applications · Advanced ceramic materials synthesis · Microwave Dielectric Ceramics Synthesis

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References (17)

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