Two-step sintering of nanocrystalline 8Y2O3 stabilized ZrO2 synthesized by glycine nitrate process
Source abstract
Abstract
Abstract Two-step sintering was employed to consolidate nanocrystalline 8 mol% yittria stabilized zirconia processed by glycine-nitrate method. Results verified the applicability of this method to suppress the final stage of grain growth in the system. The grain size of the high density compacts (>97%) produced by two-step sintering method was seven times less than the pieces made by the conventional sintering technique. Up to ∼96% increase in the fracture toughness was observed (i.e. from 1.61 to 3.16 MPa m1/2) with decreasing of the grain size from ∼2.15 to ∼295 nm. A better densification behavior was also observed at higher compacting pressures.
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OpenAlex topics: Advanced ceramic materials synthesis · Advanced materials and composites · Nuclear materials and radiation effects
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References (47)
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1. Sol–gel production of zirconia nanoparticles with a new organic precursor10.1016/j.ces.2006.09.006 ↗
2. Comparison of nanosized zirconia synthesized by gas and liquid phase methods10.1016/j.jeurceramsoc.2005.10.006 ↗
3. Sintering behavior of nanocrystalline zirconia prepared by chemical vapor synthesis10.1111/j.1151-2916.2000.tb01266.x ↗
4. New insights of the glycine-nitrate process for the synthesis of nano-crystalline 8YSZ10.1111/j.1551-2916.2007.01681.x ↗
5. K.G. Kanade, J.O. Baeg, S.K. Apte, T.L. Prakash, B.B. Kale, Synthesis and characterization of nanocrystallined zirconia by hydrothermal method, Mater. Res. Bull. (2007), in press.10.1016/j.materresbull.2007.03.025 ↗
6. Solvothermal synthesis and processing of yttria-stabilized zirconia nanopowder10.1111/j.1551-2916.2005.00161.x ↗
7. Fabrication, microstructure and properties of a YSZ electrolyte for SOFCs10.1016/j.jpowsour.2006.11.054 ↗
8. Dense yttria stabilized zirconia: sintering and microstructure10.1016/S0272-8842(02)00099-8 ↗
9. Low temperature sintering of 8YSZ electrolyte film for intermediate temperature solid oxide fuel cells10.1016/j.ssi.2004.12.010 ↗
10. Characteristics of 8mol% yttria stabilized zirconia powder prepared by spray drying process10.1016/j.jmatprotec.2007.01.019 ↗
11. Influence of alumina addition on grain growth and room temperature mechanical properties of 8YSCZ/Al2O3 composites10.1016/j.compscitech.2004.10.024 ↗
12. Fracture energy and crack growth in surface treated yttria stabilized zirconia for SOFC applications10.1016/S0921-5093(01)01863-9 ↗
13. Fracture toughness (KIC), hardness, sintering and grain growth behavior of 8YSCZ/Al2O3 composites produced by colloidal processing10.1016/j.jallcom.2004.08.084 ↗
14. The influence of shaping method on the grain size dependence of strength in dense submicrometer alumina10.1016/0955-2219(96)00044-1 ↗
15. Preparation and electric properties of dense nanocrystalline zinc oxide ceramics10.1111/j.1151-2916.2002.tb00214.x ↗
16. Interfacial thermal resistance in nanocrystalline yittria-stabilized zirconia10.1016/S1359-6454(02)00057-5 ↗
17. Photoluminescence properties of nanocrystalline ZnO ceramics prepared by pressureless sintering and spark plasma sintering10.1111/j.1551-2916.2005.00259.x ↗
18. Fracture toughness of nanocrystalline ZrO2–3mol% Y2O3 determined by Vickers indentation10.1016/1359-6462(95)00587-0 ↗
19. Two-step sintering of ceramics with constant grain-size, I. Y2O310.1111/j.1551-2916.2005.00763.x ↗
20. Preparation of nanostructured TiO2 ceramics by spark plasma sintering10.1016/S0025-5408(03)00084-9 ↗
21. Hot pressing of nanocrystalline TiO2 (anatase) ceramics with controlled microstructure10.1016/j.jeurceramsoc.2006.11.073 ↗
22. Colloidal processing, sintering and static grain growth behavior of alumina-doped cubic zirconia10.1016/j.ceramint.2004.10.011 ↗
23. Microstructural evolution in 8mol% Y2O3-stabilized cubic zirconia (8YSCZ) with SiO2 addition10.1016/j.msea.2004.07.057 ↗
24. S. Tekeli, M. Guru, Microstructural design and high temperature tensile deformation behaviour of 8mol% yttria stabilized cubic zirconia (8YCSZ) with SiO2 additions, Ceram. Int. (2006), in press.
25. T. Chen, S. Tekeli, R.P. Dillon, M.L. Mecartney, Phase stability, microstructural evolution and room temperature mechanical properties of TiO2 doped 8mol% Y2O3 stabilized ZrO2 (8Y-CSZ), Ceram. Int. (2006), in press.
26. Low temperature processing of dense nanocrystalline scandia-doped zirconia (ScSZ) ceramics10.1016/j.ssi.2005.09.005 ↗
27. Enhanced specific grain boundary conductivity in nanocrystalline Y2O3-stabilized zirconia10.1016/S0167-2738(98)00452-4 ↗
28. Sintering dense nanocrystalline oxide with-out final stage grain growth10.1038/35004548 ↗
29. M. Mazaheri, A.M. Zahedi, S.K. Sadrnezhaad, Two-step sintering of nanocrystalline ZnO compacts: effect of temperature on densification and grain growth, J. Am. Ceram. Soc.,in press.
30. Low-temperature sintering and mechanical property evaluation of nanocrystalline 8mol% yttria fully stabilized zirconia10.1111/j.1551-2916.2007.01683.x ↗
31. Two-stage sintering of nano-sized yttria stabilized zirconia process by powder injection molding10.1016/j.jmatprotec.2007.04.097 ↗
32. Two-step sintering of ceramics with constant grain-size, II: BaTiO3 and Ni–Cu–Zn ferrite10.1111/j.1551-2916.2005.00728.x ↗
33. Densification and grain growth of Al2O3 nanoceramics during pressureless sintering10.1111/j.1551-2916.2005.00654.x ↗
34. Two-stage sintering of alumina with submicrometer grain size10.1111/j.1551-2916.2006.01408.x ↗
35. Fabrication of dense nanostructured silicon carbide ceramics through two-step sintering10.1111/j.1151-2916.2003.tb03560.x ↗
36. Fully dense, fine-grained, doped zinc oxide varistors with improved nonlinear properties by thermal processing optimization10.1111/j.1151-2916.2003.tb03470.x ↗
37. Average grain size in polycrystalline ceramics10.1111/j.1151-2916.1969.tb11975.x ↗
38. A critical evaluation of indentation techniques for measuring fracture toughness: I, direct crack measurements10.1111/j.1151-2916.1981.tb10320.x ↗
39. From powders to sintered pieces: forming, transformations and sintering of nanostructured ceramic oxides10.1016/S0032-5910(02)00183-3 ↗
40. Effect of nanopowder deagglomeration on the densities of nanocrystalline ceramic green bodies and their sintering behavior10.1016/S0965-9773(99)00348-7 ↗
41. Compressibility of the structural and functional ceramic nanopowders10.1016/j.jeurceramsoc.2006.04.003 ↗
42. Powder preparation and compaction behavior of fine-grained Y-TZP10.1007/BF00575369 ↗
43. Morphology and sintering behavior of yttria stabilized zirconia (8-YSZ) powders synthesized by spray pyrolysis10.1016/j.ceramint.2004.01.010 ↗
44. Guo · 1998
45. Fracture toughness of nanocrystalline tetragonal zirconia with low yittria content10.1016/S1359-6454(02)00283-5 ↗
46. The flexural strength, fracture toughness, hardness and densification behavior of various amount of Al2O3-doped 8YSCZ/Al2O3 composites used as an electrolyte for solid oxide fuel cell10.1016/j.matdes.2004.10.011 ↗
47. Ceramic Fuel Cells10.1111/j.1151-2916.1993.tb03645.x ↗