The correlations between structural and optical properties of magnetite nanoparticles synthesised from natural iron sand
Source abstract
Abstract
Abstract The correlations between structural and optical properties of magnetite (Fe3O4) nanoparticles were analyzed by using X-Ray Diffraction (XRD) and Fourier Transform Infrared (FTIR) Spectroscopy. The magnetite was synthesised from the iron sand using NaOH, HCl, and NaCl as a solvent. From the quantitative analysis of XRD spectra, the crystallite size (D), strain ( e ), stress ( σ ), energy deformation (u), porosity, and specific surface area were determined. The Kramers Kronig (K–K) relations was applied to the FTIR spectra to determine the optical properties: refractive index (n), extinction coefficient (k), the complex dielectric function ( e ), and the energy loss function (Im(-1/e)). The uniform strain was produced from the NaOH and HCl as the solvent. The magnetite had higher porosity with NaCl as a solvent and was directly proportional to the optical phonon vibration. We found a perfect correlation; when the difference between two optical phonon increases, the crystallite size decreases, and the strain will be uniform.
Source: openaire · Quality: candidate unverified · Source record ↗
Research context
OpenAlex topics: Magnetic Properties and Synthesis of Ferrites · Iron oxide chemistry and applications · Pigment Synthesis and Properties
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (61)
Show source-provided references
1. Magnetite Fe3O4 nanoparticles synthesis by wet chemical reduction and their characterization10.1088/2043-6262/6/3/035009 ↗
2. Mechanical properties of an iron oxide formed by corrosion in reinforced concrete structure10.1016/j.corsci.2006.03.007 ↗
3. Modification and characterization of Fe3O4 nanoparticles for use in adsorption of alkaloids10.3390/molecules23030562 ↗
4. Synthesis and characterization of uniform and crystalline magnetite nanoparticles via oxidation-precipitation and modified co-precipitation Methods10.1016/S1452-3981(23)14431-2 ↗
5. Facile synthesis of biocompatible Fe3O4-based nanoparticles for pH-responsive dual-model magnetic resonance imaging-guided tumor eradication by photo thermal therapy10.1016/S1872-2040(19)61158-8 ↗
6. Catechol derivates-coated Fe3O4 and γ-Fe2O3 nanoparticles as potential MRI contrast agents10.1016/j.jcis.2009.09.043 ↗
7. Electronic properties of composite iron (II, III) oxide (Fe3O4) carbonaceous absorber materials by electron spectroscopy10.1016/j.elspec.2018.09.008 ↗
8. Enhancement of absorbing frequency and photo-catalytic performance by temperature treatment of composites Fe3O4-AC nanoparticle10.1016/j.apt.2019.11.007 ↗
9. Zerovalent iron-sand filtration can reduce the concentration of multiple antimicrobials in conventionally treated reclaimed water10.1016/j.envres.2019.02.012 ↗
10. High purity Fe3O4 from local iron sand extraction10.1088/1742-6596/1011/1/012005 ↗
11. Magnetic behavior of natural magnetite (Fe3O4) extracted from beach sand obtained by mechanical alloying method10.1063/1.4991127 ↗
12. Synthesis of magnetite (Fe3O4) Nanoparticles from iron sands by co precipitation-ultrasonic methods
13. Green synthesis of magnetite nanostructures from naturally available iron sands via sonochemical method10.1246/bcsj.20170317 ↗
14. A sonochemical method for synthesis of Fe3O4 nanoparticles and thermal stable PVA-based magnetic nanocomposite10.1016/j.jiec.2013.12.098 ↗
15. Methods and strategies for the synthesis of diverse nanoparticles and their applications: a comprehensive overview
16. Phase and magnetic properties of Fe3O4/SiO2 natural materials based using polyethylene glycol media10.1088/1757-899X/515/1/012017 ↗
17. Preparation of magnetic chitosan using local iron sand for mercury removal10.1016/j.heliyon.2019.e01731 ↗
18. Synthesis of nanoparticles Fe3O4/PEG/PPy-based on natural iron sand10.1016/j.matpr.2018.04.040 ↗
19. Structural, magnetic, optical and antibacterial properties of magnetite ferrofluids with PEG-20000 template10.1016/j.matpr.2019.06.204 ↗
20. The effect of Mg-Al additive composition on microstructure, magnetic properties, and microwave absorption on BaFe12−2xMgxAlxO19 (x = 0–0.5) material synthesized from natural iron sand10.1016/j.matlet.2019.126612 ↗
21. Effect of divalent heavy metal, cations on the synthesis and characteristics of magnetite10.1016/j.chemgeo.2020.119669 ↗
22. Synthesis of magnetite/silica nanocomposites from natural sand to create a drug delivery vehicle10.1016/j.heliyon.2020.e03784 ↗
23. Synthesis of magnetite/silica nanocomposites from natural sand to create a drug delivery vehicle10.1016/j.jksus.2020.08.009 ↗
24. Synthesis of magnetite nanoparticles from iron ore tailings using a novel reduction-precipitation method10.1016/j.jallcom.2018.03.278 ↗
25. Synthesis and characterization of magnetite nanoparticles for photocatalysis of nitrobenzene10.1016/j.jscs.2019.12.004 ↗
26. Optimization of frequency and stirring rate for synthesis of magnetite (Fe3O4) nanoparticles by using coprecipitation- ultrasonic irradiation methods10.1016/j.proeng.2017.03.010 ↗
27. Comparison of transmission FTIR, ATR, and DRIFT spectra: implications for assessment of bone bioapatite diagenesis10.1016/j.jas.2014.03.008 ↗
28. Magnetic domain interactions of Fe3O4 nanoparticles embedded in a SiO2 matrix10.1038/s41598-018-23460-w ↗
29. Optical and structural properties of X-doped (X = Mn, Mg, and Zn) PZT nanoparticles by Kramers–Kronig and size strain plot methods10.1016/j.ceramint.2012.04.012 ↗
30. X-ray diffraction analysis of nanocomposite Fe3O4/activated carbon by Williamson–Hall and size-strain plot methods10.1016/j.nanoso.2019.100396 ↗
31. Modification in electronic, structural, and magnetic properties based on composition of composites Copper (II) Oxide (CuO) and carbonaceous material
32. Porosity investigation of compacted bentonite using XRD profile modeling10.1016/j.jconhyd.2011.10.005 ↗
33. Quantitative analysis of X-ray diffraction spectra for determine structural properties and deformation energy of Al, Cu and Si
34. Analysis of structural properties of X-ray diffraction for composite copper-activated carbon by modified Williamson Hall and size-strain plotting methods
35. Fe3O4 magnetic nanoparticle synthesis from tailings by ultrasonic chemical co-precipitation10.1016/j.matlet.2011.03.065 ↗
36. Determination of binding energy for Cu and Cu2O based X-ray diffraction spectrum10.1088/1742-6596/979/1/012055 ↗
37. X-ray diffraction analysis by Williamson-Hall Halder wagner and size strain plot methods of CdSe nanoparticles-a comparative study10.1016/j.matchemphys.2019.122021 ↗
38. Size-strain separation in diffraction line profile analysis10.1107/S1600576718005411 ↗
39. Excellent electromagnetic wave absorption of Co/Fe2O3 composites by additional activated carbon for tuning the optical and magnetic properties10.1016/j.jallcom.2021.158780 ↗
40. Darminto, nanoscale clustering and magnetic properties of Mn x Fe3−x O4 particles prepared from natural magnetite10.1007/s10948-015-3111-9 ↗
41. Effect of pH on the morphology of ZnO nanostructures and its influence on structural and optical properties10.1016/j.physb.2014.09.044 ↗
42. Nanocomposites Fe/activated carbon/PVA for Microwave Absorber: synthesis and characterization10.1155/2018/9823263 ↗
43. The effect of solvents, acetone, water, and ethanol, on the morphological and optical properties of ZnO nanoparticles prepared by microwave
44. Determination of the thickness and optical constants of amorphous silicon10.1088/0022-3735/16/12/023 ↗
45. On the accurate determination of absorption coefficient from reflectance and transmittance measurements: application to Fe-doped GaN10.1116/1.4954211 ↗
46. The effect of Fe3+-doped on structure and optical properties of mesoporous Al2O3/SiO2 composite10.1016/j.mssp.2015.11.001 ↗
47. Optical analysis of nanostructured rose Bengal thin films using Kramers-Kronig approach: new trend in laser power attenuation10.1016/j.optlastec.2018.11.024 ↗
48. The role of solvent environment on the optical behavior of chemically synthesized nanoparticles
49. Electronic and optical properties of Al2O3/SiO2 thin films grown on Si substrate10.1088/0022-3727/43/25/255301 ↗
50. Composition dependence of dielectric and optical properties of Hf-Zr-silicate thin films grown on Si (100) by atomic layer deposition10.1016/j.tsf.2016.09.001 ↗
51. Electronic and optical properties of selected polymers studied by reflection electron energy loss spectroscopy10.1063/1.3688327 ↗
52. Quantitative analysis of reflection electron energy loss spectra to determine electronic and optical properties of Fe-Ni alloy thin films10.1016/j.elspec.2015.11.005 ↗
53. Stopping powers and in elastic mean free path of 200eV–50 keV electrons in polymer PMMA, PE, and PVC10.1016/j.apradiso.2014.10.001 ↗
54. Stopping powers and inelastic mean free path from quantitative analysis of experimental REELS spectra for electrons in Ti, Fe, Ni, and Pd10.1002/sia.6713 ↗
55. Quantitative analysis of diffraction and infra-red spectra of composite cement/BaSO4/Fe3O4 for determining correlation between attenuation coefficient, structural and optical properties10.1016/j.ceramint.2020.04.170 ↗
56. Study on optical phonon vibration and gamma ray shielding properties of composite geopolymer fly ash-metal10.1016/j.radphyschem.2020.109250 ↗
57. Optical properties determined from infrared spectroscopy and structural properties from diffraction spectroscopy of composites Fe/CNs/PVA for electromagnetic wave absorption10.1016/j.optmat.2020.110639 ↗
58. Effect of sugar palm fiber (SPF) to the structural and optical properties of bioplastic (SPF/Starch/Chitosan/Polypropylene) in supporting mechanical properties and degradation performance10.1007/s10924-020-02019-9 ↗
59. The correlation between structural and optical properties of zinc hydroxide nanoparticle in supports photocatalytic performance10.1016/j.optmat.2020.110780 ↗
60. Structural and optical properties of Fe-doped ruddlesden-popper Ca3Ti2-xFexO7-δ nanoparticles10.1016/j.matchemphys.2020.122810 ↗
61. The effects of porosity on optical properties of semiconductor chalcogenide films obtained by the chemical bath deposition10.1186/1556-276X-7-483 ↗