journal article·2020-10

Characterization of ZrB2–TiC composites reinforced with short carbon fibers

Hamid Istgaldi, Behzad Nayebi, Zohre Ahmadi, Peyman Shahi, Mehdi Shahedi Asl

Ceramics International· Volume 46· Issue 14
Publisher page

Abstract

Abstract Solid solution formation, phase evolution, microstructure development, and mechanical behavior of ZrB2–TiC composites with/without carbon fiber additive were investigated. Fully dense composites were manufactured by spark plasma sintering route under 40 MPa load at 1900 °C for 420 s. FESEM and XRD studies were carried out to unveil the densification and toughening mechanisms in the sintered specimens. Results showed that the addition of only 1 wt% short carbon fibers increased the hardness from 21.8 GPa to 23.5 GPa. Moreover, a 3 % enhancement in the indentation fracture toughness was also observed due to the incorporation of short carbon fibers. The in-situ formation of ZrC and TiB2 phases were identified and related to a chemical reaction between the ZrB2 and TiC constituents. The solid solution development between the ZrB2 matrix and the in-situ formed TiB2 was also proved by the microstructural observation and the shifted peaks of ZrB2 in the XRD patterns.
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Research context

OpenAlex topics: Advanced ceramic materials synthesis · Advanced materials and composites · Boron and Carbon Nanomaterials Research

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