journal article·2022-06

Influence of curing temperature on the hydration and strength development of Class G Portland cement

Xueyu Pang, Lijun Sun, Min Chen, Ming Xian, Guodong Cheng, Yang Liu, Jiankun Qin

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Abstract

A broad experimental program has been performed to characterize the hydration and strength development of a Class G oil well cement under various curing temperatures from 15 to 87 °C. The progress of hydration was monitored by isothermal calorimetry , thermo-gravimetric analysis, and quantitative X-ray diffraction based on Rietveld refinement; while the strength development was evaluated by both nondestructive ultrasonic tests and destructive crush tests. Test results indicate that heat of hydration, non-evaporable water content and degree of hydration of the cement follow approximately linear relationships, which are largely independent of curing temperature; the obtained proportionality constants agree well with those estimated by previously proposed empirical equations. The influences of curing temperature on the hydration rate and strength development rate can be modeled by an equivalent age method coupled with the Arrhenius law. The apparent activation energy obtained from hydration analysis was higher than that obtained from strength development analysis.
Source: expertdata · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Drilling and Well Engineering · Concrete and Cement Materials Research · Enhanced Oil Recovery Techniques

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (88)

Show source-provided references
1. Hewlett · 1998 · 783
2. 2021 · 9
3. 2019 · 76
4. A comparison study of Portland cement hydration kinetics as measured by chemical shrinkage and isothermal calorimetry10.1016/j.cemconcomp.2013.03.007 ↗
5. Effect of the hydration temperature on the microstructure of class G cement: C-S-H composition and density10.1016/j.cemconres.2017.02.008 ↗
6. Cement hydration kinetics study in the temperature range from 15 °C to 95 °C10.1016/j.cemconres.2021.106552 ↗
7. Effects of high pressure and temperatures on strength of oil-well cements
8. Research advances in oil well cement subjected to high temperature and high pressure curing environment10.12677/JOGT.2020.421002 ↗
9. Long-term strength retrogression of silica-enriched oil well cement system: a comprehensive multi-approach analysis10.1016/j.cemconres.2021.106424 ↗
10. Influences of different admixtures on the properties of oil well cement systems at 200 °C10.1016/j.cemconcomp.2021.104202 ↗
11. Monitoring Portland cement hydration: comparison of methods10.1016/0008-8846(90)90054-2 ↗
12. Application of the Rietveld refinement procedure in assaying powdered mixtures10.1017/S0885715600013026 ↗
13. The existence of amorphous phase in Portland cements: physical factors affecting Rietveld quantitative phase analysis10.1016/j.cemconres.2014.03.002 ↗
14. Quantitative analysis of C-S-H in hydrating alite pastes by in-situ XRD10.1016/j.cemconres.2013.06.001 ↗
15. The early hydration of Ordinary Portland Cement (OPC): an approach comparing measured heat flow with calculated heat flow from QXRD10.1016/j.cemconres.2011.09.001 ↗
16. Use of X-ray diffraction to quantify amorphous supplementary cementitious materials in anhydrous and hydrated blended cements10.1016/j.cemconres.2014.06.011 ↗
17. A new approach in quantitative in-situ XRD of cement pastes: correlation of heat flow curves with early hydration reactions10.1016/j.cemconres.2010.09.014 ↗
18. Hydration kinetics modeling of the effect of curing temperature and pressure on the heat evolution of oilwell cement10.1016/j.cemconres.2013.08.014 ↗
19. Simultaneous measurements of heat of hydration and chemical shrinkage on hardening cement pastes10.1007/s10973-009-0586-2 ↗
20. Monitoring chemical shrinkage using pressure sensors
21. Modeling the effect of curing temperature and pressure on cement hydration kinetics
22. Cement chemical shrinkage as measure of hydration kinetics and its relationship with nonevaporable water
23. Early hydration and setting of oil well cement10.1016/j.cemconres.2010.03.014 ↗
24. Nonevaporable water from neat OPC and replacement materials in composite cements hydrated at different temperatures10.1016/S0008-8846(03)00208-4 ↗
25. Effect of curing temperature on the nonevaporable water in Portland cement blended with geothermal silica waste10.1016/j.cemconcomp.2010.07.004 ↗
26. Assessment of hydration degree of cement in the fly ash-cement pastes based on the calcium hydroxide content
27. Cement degree of hydration in mortar and concrete10.1007/s10973-019-08800-w ↗
28. Hydration of binary Portland cement blends containing silica fume: a decoupling method to estimate degrees of hydration and pozzolanic reaction
29. Effect of temperature on the microstructure of calcium silicate hydrate (C-S-H)10.1016/j.cemconres.2013.06.008 ↗
30. Structural properties of calcium silicate pastes: II, effect of curing temperature10.1111/j.1151-2916.1979.tb19079.x ↗
31. Influence of curing temperature on cement paste microstructure measured by 1H NMR relaxometry10.1016/j.cemconres.2019.05.002 ↗
32. Taylor · 1997
33. Compressive strength model for concrete10.1680/macr.12.00167 ↗
34. Improved ultrasonic wave reflection technique to monitor the setting of cement-based materials10.1016/j.ndteint.2005.06.012 ↗
35. Early age microstructure of Portland cement mortar investigated by ultrasonic shear waves and numerical simulation10.1016/j.cemconres.2004.09.004 ↗
36. Comparison of ultrasonic wave reflection method and maturity method in evaluating early-age compressive strength of mortar10.1016/j.cemconcomp.2006.02.003 ↗
37. Continuous monitoring of setting and hardening of mortar and concrete10.1016/j.conbuildmat.2003.10.002 ↗
38. Ultrasonic in-situ monitoring of setting process of high-performance concrete10.1016/j.cemconres.2003.10.012 ↗
39. Ultrasound monitoring of the influence of different accelerating admixtures and cement types for shotcrete on setting and hardening behaviour10.1016/j.cemconres.2005.03.011 ↗
40. Monitoring the setting of concrete containing blast-furnace slag by measuring the ultrasonic p-wave velocity10.1016/j.cemconres.2008.04.006 ↗
41. Investigation of the influence of curing temperature and silica fume content on setting and hardening process of the blended cement paste by an improved ultrasonic apparatus10.1016/j.conbuildmat.2012.01.011 ↗
42. An ultrasonic device for nondestructive testing of oilwell cements at elevated temperatures and pressures10.2118/9283-PA ↗
43. Nano-chemo-mechanical signature of conventional oil-well cement systems: effects of elevated temperature and curing time10.1016/j.cemconres.2014.08.008 ↗
44. Cement strength retrogression issues in offshore deep water applications–do we know enough for safe cementing
45. Portland cement solutions for ultra-high temperature wellbore applications10.1016/j.cemconcomp.2016.05.018 ↗
46. Multiscale characterization of oilwell cement cured HPHT conditions, ARMA 21–1114
47. The superstructure of C3S from synchrotron and neutron powder diffraction and its role in quantitative phase analyses10.1016/S0008-8846(02)00796-2 ↗
48. Tricalcium silicate Ca3O[SiO4]: the monoclinic superstructure10.1524/zkri.1985.172.14.297 ↗
49. Rietveld crystal structure refinements, crystal chemistry and calculated powder diffraction data for the polymorphs of dicalcium silicate and related phases
50. Magnesium doping on brownmillerite Ca2FeAlO510.1016/j.jssc.2007.04.009 ↗
51. The A16O18 rings of tetrahedra in the structure of Ca8.5NaAl6O1810.1107/S0567740875004736 ↗
52. A refinement of the crystal structure of gypsum CaSO4.2H2O10.1107/S0567740874004055 ↗
53. Investigation of the crystal structure of γ-CaSO4, CaSO4·0.5H2O, and CaSO4·0.6H2O by powder diffraction methods10.1006/jssc.1995.1260 ↗
54. Crystal structure of gorgeyite K2Ca5(SO4)6·H2O
55. Hydrogen thermal motion in calcium hydroxide: Ca(OH)210.1107/S0108768193003556 ↗
56. X-ray determination of electron-density distributions in oxides, MgO, MnO, CoO, and NiO, and atomic scattering factors of their constituent atoms,P
57. X-ray study of the electron density in calcite, CaCO3
58. State-of-the-art high-resolution powder X-ray diffraction (HRPXRD) illustrated with Rietveld structure refinement of quartz, sodalite, tremolite, and meionite10.3749/canmin.46.5.1501 ↗
59. Scrivener · 2016
60. 2013
61. Critical examination of drying damage to cement pastes10.1680/adcr.2000.12.2.79 ↗
62. Comparison of methods for arresting hydration of cement10.1016/j.cemconres.2011.06.003 ↗
63. Application of the Rietveld method to the analysis of anhydrous cement10.1016/j.cemconres.2010.10.003 ↗
64. The effect of water ratio on microstructure and composition of the hydration products of Portland cement pastes
65. Correction for preferred orientation in Rietveld refinement10.1107/S0021889889000725 ↗
66. Microstructural properties: texture and macrostress effects
67. Cong · Cem. Concr. Res. · 1995 · 25 · 123710.1016/0008-8846(95)00116-T ↗
68. Investigation of the structure of ettringite by time-of-flight neutron powder diffraction techniques10.1016/j.cemconres.2005.08.004 ↗
69. Oriented decomposition and reconstruction of hydrogarnet, Ca3Al2(OH)1210.1127/ejm/5/6/1133 ↗
70. Crystal structure change in grossular-Si-free katoite solid solution: oxygen position splitting in katoite10.2465/jmps.190424 ↗
71. Effect of temperature on the hydration of the main clinker phases in Portland cements: part I, neat cements10.1016/S0008-8846(98)00115-X ↗
72. A generalized scale factor model for Portland cement hydration
73. Measuring and modeling cement hydration kinetics at variable temperature conditions10.1016/j.conbuildmat.2020.120788 ↗
74. Simulations of hydration kinetics of Portland cement by scale factor method
75. Modeling the effect of curing pressure on the viscosity evolution of oilwell cement
76. A rheological approach to study the early-age hydration of oil well cement: effect of temperature, pressure and nanoclay10.1016/j.conbuildmat.2019.04.177 ↗
77. Experimental study of the effect of curing temperature and pressure on the property evolution of oilwell cement, ARMA 21–1397
78. Pore structure evolution and strength development of G-type elastic oil well cement. A combined 1H-NMR and ultrasonic study10.1016/j.cemconres.2015.02.018 ↗
79. Effect of pressure on early hydration of class H and white cement10.1016/j.cemconres.2010.01.013 ↗
80. Oil-well cement and C3S hydration under high pressure as seen by in situ X-ray diffraction, temperatures ≤80 °C with no additives10.1111/j.1551-2916.2010.04284.x ↗
81. The effect of pressure on tricalcium silicate hydration at different temperatures and in the presence of retarding additives10.1016/j.cemconres.2012.04.008 ↗
82. Modeling cement hydration by connecting a nucleation and growth mechanism with a diffusion mechanism part I: C3S hydration in dilute suspensions10.1515/secm-2013-0258 ↗
83. Modeling cement hydration by connecting a nucleation and growth mechanism with a diffusion mechanism part II: Portland cement paste hydration10.1515/secm-2013-0259 ↗
84. The dispersion model for hydration of Portland cement: I. General concepts10.1016/0008-8846(84)90024-3 ↗
85. Influence of curing temperature dependent microstructure on early-age concrete strength development10.1016/j.cemconres.2017.08.022 ↗
86. 2019 · 10
87. Calcium hydroxide as a binder in Portland cement paste10.1111/j.1151-2916.1970.tb12004.x ↗
88. Effects of temperature and water-to-cement ratio on autogenous shrinkage of oil well cement