journal article·2025-07Open access

Preliminary characterization and evaluation of local concrete sludges for use as supplementary cementitious materials

Ashfaque Ahmed Jhatial, Iveta Nováková, Eirik Gjerløw, Christian John Engelsen

Abstract

Concrete sludge (CS) is an emerging supplementary cementitious material (SCMs). However, the diverse range of SCMs and their various sources for each necessitate initial characterization and evaluate the potential of CS as a SCM. In this study, CS were collected from seven different concrete producers (designated as CS1 to CS7) in the Northern Norway region. This preliminary characterization aims to provide valuable insights into the feasibility of using CS in cement or concrete production. It was determined that the chemical composition of CS was found to meet the EN 450–1 requirements, while most of the CS evaluated, exhibited hydraulic characteristics. The Rankin Classification of analyzed CS indicates a prevalent hydraulic nature, with most CS exhibiting CaO/SiO 2 ratios greater than 2.0, thus suggesting potential for hydraulic applications. It was also observed that with 30 minutes of pulverizing, the particle size of the CS samples exhibited an average decrease ranging from 6.8 % to 78 %. This variation is likely due to differences in initial particle size and composition. Larger particles are generally more susceptible to breakdown during pulverization, which explains the higher reduction observed in some samples. Conversely, samples with higher coarse sand content and the resistance of specific aggregates to grinding exhibited the smallest reduction. These differences highlight the impact of material composition on the effectiveness of the pulverization process. An increase in the specific surface area and a decrease in the particle size of CS were observed after grinding, showing the potential for mechanical activation of CS as a potential SCM. However, prolonged pulverization beyond 30 minutes is not recommended, as only marginal improvement beyond 30 minutes of pulverization were observed. The XRD analysis revealed that the CS samples contained 2.29–28.47 %, with an average of 8.3 % amorphous content, reflecting the variation of cement paste in the CS. The findings suggest that CS can be categorized into two SCMs based on their operation: precast CS, characterized by siliceous and alkali-rich properties, and ready-mix CS, which is lime-rich and exhibits hydraulic properties, enabling tailored applications in cement and concrete production. • Concrete sludge from seven Northern Norway producers met EN 450–1 and showed hydraulic properties suitable for SCMs. • XRF and XRD analyses show varied chemical and mineralogical compositions, with 2.29–28.47 % amorphous content. • CS from similar operations (e.g., truck washing, drilling) shows consistent properties for standard use. • CS as SCM supports sustainability, reduces the environmental impact of cement production, and offer potential cost savings.
Source: openalex_inverted_index · Quality: baseline

Research context

OpenAlex topics: Concrete and Cement Materials Research · Recycling and utilization of industrial and municipal waste in materials production · Innovative concrete reinforcement materials

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (28)

Show source-provided references
1. Recent progress in green cement technology utilizing low-carbon emission fuels and raw materials: a review10.3390/su11020537 ↗
2. Challenges against CO2 abatement strategies in cement industry: a review10.1016/j.jes.2020.11.020 ↗
3. A review on emerging cementitious materials, reactivity evaluation and treatment methods10.3390/buildings13020526 ↗
4. N.Z. Roadmap, “A Global Pathway to keep the 1.5° C Goal in Reach,” International Energy Agency, 2023.
5. Smart materials and technologies for sustainable concrete construction
6. Investigating the influence of oil shale ash and basalt composite fibres on the interfacial transition zone in concrete10.3390/buildings14071952 ↗
7. Recycling of fresh concrete slurry waste as supplementary cementing material: characterization, application and leaching of selected elements10.1016/j.conbuildmat.2021.124061 ↗
8. The influence of concrete sludge from residual concrete on fresh and hardened cement paste properties10.3390/ma16062531 ↗
9. The cement industry on the way to a low-carbon future10.1016/j.cemconres.2019.105792 ↗
10. EMRCO, “European Ready Mixed Concrete Organization, Ready-Mixed Concrete Industry Statistics: Year 2018,” 2019. Accessed: Jul. 03, 2024. [Online]. Available: 〈http://ermco.eu/new/wp-content/uploads/2020/08/ERMCO-Statistics-30.08.2019-R4-1.pdf〉.
11. Evaluation of concrete recycling system efficiency for ready-mix concrete plants10.1016/j.wasman.2016.07.015 ↗
12. Supplementary cementitious materials: new sources, characterization, and performance insights10.1016/j.cemconres.2019.05.008 ↗
13. ASTM C618-19, “Standard Specification for Coal Fly Ash and Raw or Calcined Natural Pozzolan for Use in Concrete, ASTM International, West Conshohocken, PA, 2019, 〈www.astm.org〉,” 2019.
14. University of Massachusetts, “Convert oxides to elements (and vice versa).”
15. EN 1097-7, “Tests for mechanical and physical properties of aggregates - Part 7: Determination of the particle density of filler - Pyknometer method,” 2022.
16. Assessment of the quantitative accuracy of Rietveld/XRD analysis of crystalline and amorphous phases in fly ash10.1039/C7AY00337D ↗
17. Effect of ball-milling time on chemical property of coconut shell powder10.1088/1742-6596/1572/1/012021 ↗
18. EN 450-1, “Fly ash for concrete - Definition, specifications and conformity criteria,” 2012.
19. Effect of nano-magnesium oxide on the expansion performance and hydration process of cement-based materials10.3390/ma14133766 ↗
20. Synergistic effect of dry sludge from waste wash water of concrete plants and zeolitic by-product on the properties of ternary blended ordinary Portland cements10.1016/j.jclepro.2019.118493 ↗
21. P.J. Jadhav, N.A. Mohite, V.S. Kadam, and M.M. More, “Effect of concrete sludge from residual concrete on hardened cement paste properties.”
22. Technological characterization of selected mineral additives10.1088/1757-899X/385/1/012048 ↗
23. Valorization of industrial byproducts and wastes as sustainable construction materials
24. Utilization of sludge from ready-mixed concrete plants as a substitute for limestone fillers10.1016/j.conbuildmat.2016.02.044 ↗
25. Investigation on grinding impact of fly ash particles and its characterization analysis in cement mortar composites10.1016/j.asej.2019.02.001 ↗
26. Mechanical activation of fly ash: physical, mineralogical and morphological characterization of ground fly ashes
27. Crystallography
28. Nanomaterials, their types and properties