journal article·2025-07Open access

Effect of silane coupling agent on flexural properties of fiber-reinforced geopolymer-cemented aeolian sand

Shuai Pang, Jiaze Li, Mengjie Li, Changzhi Zhao, Henghui Fan, Xiangdong Zhang

Abstract

To enhance the flexural properties of polypropylene fiber (PPF)-reinforced geopolymer-bonded aeolian sand and increase the service life of trench backfill materials, this study improves the flexural performance by two methods: soaking fibers in a diluted silane coupling agent (KH570) solution of varying concentrations and directly adding KH570 during specimen preparation. The flexural behavior of the specimens under different conditions was tested using three-point bending tests. Additionally, digital image correlation (DIC) technology was employed to observe the progressive failure evolution of the specimens, and the mechanical parameter evolution was analysed. The mechanism of KH570 modification was revealed using scanning electron microscope (SEM) microanalysis. The results show that soaking the fibers in a 1.5 % KH570 diluted solution makes the fiber surface uniformly rough, increasing the specific surface area, which enhances the wrapping ability of the geopolymer-bonded aeolian sand around the fibers. In the three-point bending test, the maximum crack width was reduced by 54.96 %, the farthest crack extension was shortened by 6.80 mm, and the maximum generalized crack area decreased by 42.39 %. Incorporating 1.5 % KH570 into the specimens effectively improved the physico-chemical properties of the fiber-matrix interface, promoted product formation, and strengthened the interfacial bonding ability. As a result, the flexural performance of the specimens significantly improved. In the three-point bending test, the maximum crack width reduced by 0.64 mm, the farthest crack extension decreased by 10.56 mm, the crack area shrank by 9.37 mm², and the crack fractal dimension decreased by 0.132. During the failure process, with increasing load, the displacement field of the specimens gradually evolved from uniform deformation to localized non-uniformity. After reaching the peak load, significant changes were observed in the displacement field. The research findings have significant implications for the selection of pipeline backfill materials, their service life, and environmental protection. • Enhancement of flexural properties of geopolymers by silane coupling agents. • Effective improvement of physicochemical properties at fiber-geopolymer interfaces. • Improvement of fiber surface roughness by silane coupling agent. • The damage mechanism of the specimen was analysed by digital scattering. • Development of pipe trench backfill materials for solid waste substrates to improve solid waste utilization.
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Research context

OpenAlex topics: Concrete and Cement Materials Research · Geotechnical Engineering and Soil Stabilization · Innovative concrete reinforcement materials

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (46)

Show source-provided references
1. Assessing the impact of renewable energy investment, green technology innovation, and industrialization on sustainable development: a case study of China10.1016/j.renene.2023.01.014 ↗
2. Impact of natural resource mining on sustainable economic development: the role of education and green innovation in China
3. Stability analysis of tunnel under coal seam goaf: Numerical and physical modeling10.1016/j.undsp.2022.12.006 ↗
4. Identifying the potential soil pollution areas derived from the metal mining industry in China using MaxEnt with mine reserve scales (MaxEnt_MRS)10.1016/j.envpol.2023.121687 ↗
5. Environmentally sound management of industrial solid waste: a paradigm of proposed bi-tetrahedron10.1016/j.resconrec.2023.107212 ↗
6. Sustainable utilization of red mud waste (bauxite residue) and slag for the production of geopolymer composites: a review
7. The composition, recycling and utilisation of Bayer red mud10.1016/j.resconrec.2018.11.006 ↗
8. A review on the utilization of red mud for the production of geopolymer and alkali activated concrete10.1016/j.conbuildmat.2021.124170 ↗
9. Characteristic, hazard and iron recovery technology of red mud-a critical review10.1016/j.jhazmat.2021.126542 ↗
10. Comprehensive utilization and environmental risks of coal gangue: a review10.1016/j.jclepro.2019.117946 ↗
11. Evaluation of potential hazards and pollution characteristics of heavy metals in soil of coal gangue accumulation area
12. Industrial progress of resource utilisation technology of calcium carbide slag
13. Lateral soil–pipeline interaction in sand backfill:effect of trench dimensions10.1016/j.compgeo.2015.05.014 ↗
14. Influence of soil backfill on vibration-based pipeline leakage detection10.1061/(ASCE)PS.1949-1204.0000435 ↗
15. Research status and prospect of low-strength fluid filling materials [J]
16. Research progress on heavy metal pollution characteristics of solid waste roadbed fill materials
17. Utilisation of solid waste resources is an element of high-quality development
18. Synthesis and characterization of fly ash geopolymer paste for goaf backfill: Reuse of soda residue10.1016/j.jclepro.2020.121045 ↗
19. Numerical simulation on backfilling of buried pipes using controlled low strength materials10.3390/app12146901 ↗
20. Mechanical and flexural performance of synthetic fiber reinforced geopolymer concrete10.1016/j.conbuildmat.2018.07.110 ↗
21. Effect of fly ash dosage and early curing temperature on tensile properties of EGC
22. Nanomaterial and fiber-reinforced sustainable geopolymers: a systematic critical review10.1016/j.conbuildmat.2023.133325 ↗
23. Eco-efficient cements: potential economically viable solutions for a low-CO2 cement-based materials industry10.1016/j.cemconres.2018.03.015 ↗
24. Engineering and microstructural properties of carbon-fiber-reinforced fly-ash-based geopolymer composites
25. Flexural fracture parameters of polypropylene fiber reinforced geopolymer10.1016/j.jmrt.2023.03.035 ↗
26. Engineering properties of different fiber-reinforced metakaolin-red mud based geopolymer mortars10.1016/j.conbuildmat.2023.131496 ↗
27. Feasibility of using ultra-high ductility cementitious composites for concrete structures without steel rebar10.1016/j.engstruct.2018.05.037 ↗
28. Silane coupling agents used for natural fiber/polymer composites: a review10.1016/j.compositesa.2010.03.005 ↗
29. Study on the performance of silane coupling agent modified polypropylene fiber cement mortar
30. Mechanical properties of modified polypropylene fiber cementitious composites
31. Influence of polypropylene fiber surface modification on dry shrinkage of cement-soil [J]
32. Study on the compressive strength and failure mechanism of fiber-reinforced polymer green filling materials10.1016/j.conbuildmat.2024.138990 ↗
33. Research on improving the flexural performance of alkali-activated geopolymer cemented coal gangue through layered addition of fibers
34. Durability of low-carbon geopolymer concrete: a critical review
35. GB/T 3356–2014, Test method for flexural properties of aligned fiber reinforced polymer matrix composites.
36. Determination of the fracture energy of mortar and concrete by means of three-point bend tests on notched beames
37. JSCE Standard SF4, Method of test for flexural strength and flexural toughness of fiber reinforced concrete. 1984, 58-61.10.1520/CCA10229J ↗
38. Study on the influence of pre-existing micro-cracks on the rock fracture performance
39. Flexural properties of fiber-reinforced alkali slag-red mud geopolymer10.1016/j.conbuildmat.2023.130708 ↗
40. Study on shear resistance and crack resistance and toughening mechanism of fiber reinforced cement stabilized aeolian sand10.1016/j.tafmec.2022.103700 ↗
41. Mechanical properties and interface microscopic characterisation of fiber-reinforced slag-fly ash geopolymer agglutinated iron tailings filling materials
42. Research on the physico-mechanical properties of fly ash geological polymer filling
43. Study of localized deformation in geopolymer cemented coal gangue-fly ash backfill based on the digital speckle correlation method10.1016/j.conbuildmat.2019.04.208 ↗
44. Study on the failure characteristics of phosphorus slag-slag-red mud glue tailing sand filling body under cyclic loading and unloading conditions
45. Effect of silane coupling agent modification on the anti-cracking effect of polypropylene fiber
46. Effects of silanes and silane derivatives on cement hydration and mechanical properties of mortars10.1016/j.conbuildmat.2016.11.004 ↗