DEF of high-performance concrete with rapid, non-standard heat-treatment
Source abstract
Abstract
High-performance concrete is often heat treated to increase early strength. Standardized temperature conditions for at least 24 hours and sulphate-resistant cement thereby preventing delayed ettringite formation (DEF). In contrast, this paper investigates the risk of DEF for rapidly heat-treated HPC with a minimum temperature duration of 1 hour to achieve a rapid early strength for stripping. In addition, a binder is used that does not exhibit increased sulphate resistance. For this purpose, standard prisms (L x W x H = 16 ×4 x 4 [cm]) are heat treated at 80 °C between 1 and 6 hours without a pre-storage time. Samples with a temperature duration of 24 hours serve as reference. First, the pore structure is analyzed using Mercury porosimetry to identify damage to the concrete matrix due to the rapid heat treatment. The investigation of DEF is achieved by two common approaches. The sulphate resistance is determined by means of wet-dry cycles on specimens for 90 days, whereby the changes in mass and strain as well as the cracking pattern on the concrete surface serves as a qualitative evaluation criterion. In addition, the SVA method on specimens directly after heat treatment, which determines the change in mechanical properties and the swelling behavior of the concrete, leads to a quantitative evaluation of sulfate resistance. The measured pore distribution of the samples shows a significant increase of the capillary pores of up to 109% for decreasing temperature durations. However, the porosity does not affect the sulphate resistance of the concrete. The wet-dry cycles cause no damage due to DEF, since the change in mass and strains decreases with increasing cycles from up to 62.7% to -2.5%. Furthermore, no visual differences were detected on the concrete surface between specimens with and without sulphate attack. As a result of the SVA test, maximum absolute strains of about 0.1 mm/m occur that are below the limit value of 0.152 mm/m. Also, the mechanical properties do not show a reduction in strength, but even an increase in tensile strength. In conclusion, the high-performance concrete formulation used in combination with rapid heat treatment investigated here did not result in detectable damage due to DEF.
Source: openalex_inverted_index · Quality: baseline
Research context
OpenAlex topics: Concrete and Cement Materials Research · Concrete Properties and Behavior · Innovative concrete reinforcement materials
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (64)
Show source-provided references
1. Industrializing precast productions
2. Accuracy limits of modular concrete structures – Part 2: Probabilistic evaluation of assembling with bolted connection10.1002/best.202200011 ↗
3. Geometric evaluation and optimization of module arrangement in load bearing structures – towards adaptive manufacturing in civil engineering10.1002/bate.202100027 ↗
4. Accuracy limits of modular concrete structures – Part 1: Description of geometric deviations due to shrinkage10.1002/best.202200010 ↗
5. Experiments on shrinkage reduction of high-performance concrete components by heat treatment10.1002/best.202100028 ↗
6. Influence of different curing methods on the compressive strength of ultra-high-performance concrete: a comprehensive review
7. Day · 1992
8. Hewlett · 2019
9. Thermal stability and decomposition mechanisms of ettringite at <120°C10.1016/S0008-8846(01)00558-0 ↗
10. Stark · 2013
11. Michael Stegmaier, Properties of heat cured self-compacting concrete. doctoral thesis. University of Stuttgart, Stuttgart, 2005.
12. Current knowledge of external sulfate attack10.1680/adcr.14.00089 ↗
13. Early-age mechanical properties and microstructures of Portland cement mortars containing different admixtures exposed to seawater
14. A literature review on delayed ettringite formation: mechanism, affect factors and suppressing methods10.1680/jmacr.20.00268 ↗
15. State-of-the-art review on plastic cracking of concrete10.1016/j.conbuildmat.2019.07.197 ↗
16. Neville · 2011
17. The pozzolanic reaction of coal fly ash and its effects on the sulfate resistance of concrete
18. Deutscher Ausschuss für Stahlbeton (DAfStb), DAfStb Heft 554 Sulfatangriff auf Beton. Heft 554, Beuth Verlag, Berlin, 2006.
19. The distribution of sulfur in present-day clinkers of variable sulfur content10.1016/S0008-8846(96)00171-8 ↗
20. Influence of the clinker SO3 on the cement characteristics10.1016/j.cemconres.2011.04.015 ↗
21. Thaumasite formation: a cause of deterioration of portland cement and related substances in the presence of sulphates10.1016/0008-8846(75)90004-6 ↗
22. The effect of C3A content on sulfate durability of Portland limestone cement mortars10.1016/j.conbuildmat.2012.04.091 ↗
23. Time to failure for concrete exposed to severe sulfate attack10.1016/S0008-8846(02)01097-9 ↗
24. Pore structure and chloride permeability of concrete containing nano-particles for pavement10.1016/j.conbuildmat.2010.07.032 ↗
25. Influence of water-binder ratio on the microstructure of air-entrained concrete10.1088/1757-899X/392/2/022001 ↗
26. The effect of natural pozzolan on delayed ettringite formation of the heat-cured mortars10.1016/j.conbuildmat.2013.07.016 ↗
27. The effect of the partial cement substitution with fly ash on Delayed Ettringite Formation in heat-cured mortars10.1007/s12205-016-0778-9 ↗
28. Gerd Wischers, 1967. Merkblatt für die Herstellung geschlossener Betonoberflächen bei einer Wärmebehandlung, Beton 17 (4) (1967) 142–160.
29. Reaktionen im Zementstein durch Wärmebehandlung
30. Influence of blended powders on properties of ultra-high strength fibre reinforced self compacting concrete subjected to elevated temperatures
31. Effect of GFRP rebars and polypropylene fibers on flexural strength in high-performance concrete beams with glass powder and microsilica
32. Influence of high-performance polypropylene fibre and heat-treated dura oil palm shell on durability properties of lightweight concrete10.1080/19648189.2018.1509022 ↗
33. Mechanical properties of high performance concrete reinforced with basalt fiber and polypropylene fiber10.1016/j.conbuildmat.2018.11.181 ↗
34. Shrinkage characteristics of heat-treated ultra-high performance concrete and its mitigation using superabsorbent polymer based internal curing method10.1016/j.cemconcomp.2018.03.003 ↗
35. Ultra-high-performance fiber-reinforced concrete. Part III: fresh and hardened properties
36. Ultra-high-performance fiber-reinforced concrete. Part II: hydration and microstructure
37. Fehling · 2005
38. Deutscher Ausschuss für Stahlbeton (DAfStb), Sachstandbericht Ultrahochfester Beton. Heft 561, Beuth Verlag, Berlin, 2008.
39. DIN EN 1992–1-1, Eurocode 2: Design of concrete structures: Part 1–1: General rules and rules for buildings; German version EN 1992–1-1:2004 + AC:2010, Beuth Verlag, 2011.
40. ACI Committee 209, Guide for Modeling and calculating Shrinkage and Creep in Hardenend Concrete (ACI 209.2R-08), 2009.
41. Deutscher Ausschuss für Stahlbeton (DAfStb), Wärmebehandlung von Beton, Beuth Verlag, Berlin, 2012.
42. ACI Committee 517, Accelerated Curing of Concrete at Atmospheric Pressure -State of the Art, ACI Journal Proceedings 77 (1980). https://doi.org/10.14359/7018.10.14359/7018 ↗
43. E. Fehling, M. Schmidt, S. Stürwald, 2008. Ultra high performance concrete (UHPC): Proceedings of the Second International Symposium on Ultra High Performance Concrete, Kassel, Germany, March 05–07, 2008, Kassel University Press, Kassel, 2008.
44. Thermal and hydrothermal treatment of UHPC: influence of the process parameters on the phase composition of ultra-high performance concrete10.1617/s11527-021-01633-w ↗
45. EN 197–1:2011, Cement - Part 1: Composition, specifications and conformity criteria for common cements; German version EN 197–1:2011, Beuth Verlag GmbH, Berlin, 2011.
46. Sagmeister · 2017
47. J. Stindt, P. Forman, P. Mark, 2021. Influence of a Rapid Heat Treatment on the Shrinkage of High-Performance Concrete, in: E. Júlio, J. Valença, A. S. Louro (Eds.), Concrete Structures: New Trends for Eco-Efficiency and Performance: Proceedings for the 2021 fib Symposium, held online from Lisbon, Portugal, 2021, 439–438.
48. Influence of rapid heat treatment on the shrinkage and strength of high-performance concrete10.3390/ma14154102 ↗
49. DIN 66139:2012–03, Pore size analysis – Representation of pore size distributions, Beuth Verlag GmbH, Berlin.
50. ISO 15901–1, Evaluation of pore size distribution and porosity of solid materials by mercury porosimetry and gas adsorption: Part 1: Mercury porosimetry (ISO 15901–1:2016), Beuth Verlag GmbH, 2019.
51. Microcracking as a precursor to delayed ettringite formation in cement systems10.1016/0008-8846(96)00134-2 ↗
52. Some factors affecting delayed ettringite formation in heat-cured mortars10.1016/j.cemconres.2007.07.004 ↗
53. Durability and Testing – Chemical Matrix Degradation Processes
54. Bollmann K., 2000. Ettringitbildung in nicht wärmebehandelten Betonen. doctoral thesis. Bauhaus University, Weimar, 2000.
55. H.öhling Björn, 2014. Application of radio-wave technology in concrete industry. doctoral thesis. TU Dresden, Dresden, 2014.
56. DIN EN 12390–3, Testing hardened concrete - Part 3: Compressive strength of test specimens; German version EN 12390–3:2019, Beuth Verlag GmbH, Berlin, 2019.
57. DIN EN 12390–5, Testing hardened concrete - Part 5: Flexural strength of test specimens; German version EN 12390–5:2019, Beuth Verlag GmbH, Berlin, 2019.
58. Thermal conductivity of humid air10.1007/s10765-012-1254-5 ↗
59. Zement-Taschenbuch, 51st ed. Zement-Taschenbuch, Verlag Bau + Technik, Düsseldorf, 2008.
60. Microstructural Investigation of Heat-Treated Ultra-High Performance Concrete for Optimum Production
61. Influencing factors for the effectivity of heat treatment of ultrahigh performance concrete (UHPC)10.1002/best.201600059 ↗
62. Ultra-high performance concrete: mechanical performance, durability, sustainability and implementation challenges10.1007/s40069-016-0157-4 ↗
63. Entropy evolution during crack propagation in concrete under sulfate attack10.1016/j.conbuildmat.2019.03.083 ↗
64. Experimental study on sulfate resistance of shotcrete with different liquid accelerators