journal article·2024-12Open access

Experimental investigation and optimization of one-part alkali-activated self-compacting concrete mixes

Kaku Mahendra, Mattur C. Narasimhan, Gundupalli Bhanu Prakash, Amit Kumar Das

Abstract

Emphasizing the growing importance of sustainability, alkali-activated materials (AAMs) have emerged as a revolutionary alternative for cement in the construction sector. This study delves into the fresh, mechanical, and microstructural properties of O ne- P art A lkali-activated S elf-compacting C oncrete (OPASC) mixes. While mixtures of Ground Granulated Blast Furnace Slag (GGBFS) and Fly Ash (FA) were utilized as the precursors, powdered sodium metasilicate was employed to function as the activator. To streamline experimental design and reduce the economic demands of extensive testing, the Taguchi-Grey Relational Analysis (GRA) was utilized to identify optimal multi-response parameter levels. This method considered binder content (B) within a range of 700–800 kg/m³, water-to-binder (W/B) ratios between 0.38 and 0.42, and Na 2 O percentages from 5% to 7% as key input variables. Results indicated that the designed mixes recorded workability values satisfying the EFNARC guidelines, compressive strengths greater than 60 MPa, split-tensile strengths in the range of 3.5-4.6 MPa, and flexural strengths varying between 5.5-7.2 MPa. The mix parameters for the optimal mix, with the highest mean grey relational grade, were identified from the Taguchi-GRPA approach as B = 750 kg/m 3 , W/B = 0.4, and N = 6%. Microstructural analysis revealed the formation of C/N-A-S-H type gels, which are instrumental in developing a compact matrix enhancing the mechanical properties. A good agreement between actual experimental results obtained for a different set of verification mixes with those predicted by regression-equations confirmed the potency of the Taguchi-GRA approach in optimizing the OPASC mix parameters. • Utilization of industrial waste has resulted in enhanced properties of OPASC mixes. • All OPASC mixes exhibited superior fresh and mechanical properties. • Taguchi-GRA demonstrated high predictive accuracy for the evaluated properties. • Microstructural analysis revealed dense morphology with C/N-A-S-H gel phases.
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Research context

OpenAlex topics: Concrete and Cement Materials Research · Innovative concrete reinforcement materials · Concrete Properties and Behavior

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References (70)

Show source-provided references
1. Global CO 2 emissions from cement production, 1928–201810.5194/essd-11-1675-2019 ↗
2. History, recent progress, and future challenges of alkali-activated binders – an overview10.1016/j.conbuildmat.2024.136141 ↗
3. Advances in understanding alkali-activated materials10.1016/j.cemconres.2015.04.013 ↗
4. A review on alkali-activated binders: materials composition and fresh properties of concrete10.1016/j.conbuildmat.2020.119788 ↗
5. Luukkonen · 2022
6. One part alkali activated materials: a state-of-the-art review
7. Experimental comparisons between one-part and normal (two-part) alkali-activated slag binders10.1016/j.conbuildmat.2021.125177 ↗
8. Preparation of drying powder inorganic polymer cement based on alkali-activated slag technology10.1016/j.powtec.2017.02.036 ↗
9. One part alkali-activated materials for construction – a review10.1016/j.matpr.2023.07.116 ↗
10. Texture, morphology and strength performance of self-compacting alkali-activated concrete: role of fly ash as GBFS replacement10.1016/j.conbuildmat.2020.121368 ↗
11. Factors affecting production and properties of self-compacting geopolymer concrete – a review10.1016/j.conbuildmat.2022.128174 ↗
12. The effects of precursors on rheology and self-compactness of geopolymer concrete10.1680/jmacr.17.00495 ↗
13. A newly developed self-compacting geopolymer concrete under ambient condition10.1016/j.conbuildmat.2020.121822 ↗
14. Effects of fly ash characteristics and alkaline activator components on compressive strength of fly ash-based geopolymer mortar10.1016/j.conbuildmat.2018.04.092 ↗
15. Mechanical and microstructural characterization of fly ash blended self-compacting concrete containing granite waste10.1016/j.conbuildmat.2021.125480 ↗
16. Studies on development of high performance, self-compacting alkali activated slag concrete mixes using industrial wastes10.1016/j.conbuildmat.2018.11.242 ↗
17. High strength one-part alkali-activated slag blends designed by particle packing optimization10.1016/j.conbuildmat.2021.124004 ↗
18. Drying shrinkage of one-part alkali-activated slag concrete
19. Fresh and hardened properties of one-part fly ash-based geopolymer binders cured at room temperature: effect of slag and alkali activators10.1016/j.jclepro.2019.03.290 ↗
20. Fresh, hardened, and microstructural properties of ambient cured one-part alkali-activated self-consolidating concrete
21. Optimization of high-strength self-consolidating concrete mix design using an improved Taguchi optimization method10.1016/j.conbuildmat.2019.117547 ↗
22. Mix design optimization for fresh, strength and durability properties of ambient cured alkali activated composite by Taguchi method10.1016/j.conbuildmat.2021.122822 ↗
23. Multi-response optimization using Taguchi-Grey relational analysis for composition of fly ash-ground granulated blast furnace slag based geopolymer concrete10.1016/j.conbuildmat.2020.118049 ↗
24. Study of the defrosting behavior of concrete by using Taguchi-based grey relational analysis method10.1016/j.conbuildmat.2022.126324 ↗
25. Ground granulated blast furnace slag for use in cement, mortar and concrete — specification
26. Standard Specification for Slag Cement for Use in Concrete and Mortars
27. IS 3812 (Part 1): 2013 (Reaffirmed 2022), PULVERIZED FUEL ASH — SPECIFICATION, Bur. Indian Stand. Dehli. (2017) 1–12.
28. Standard Specification for Coal Fly Ash and Raw or Calcined Natural Pozzolan for Use in Concrete
29. Coarse and fine aggregate for concrete - specification
30. EFNARC for Self-Compacting Concrete
31. Fresh concrete - methods of sampling, testing and analysis: part 6 tests on fresh self compacting concrete
32. Fresh concrete - methods of sampling, testing and analysis: part 7 - determination of setting time of concrete by penetration resistance
33. Methods of Tests for Strength of Concrete
34. Splitting tensile strength of concrete
35. The use of Taguchi, ANOVA, and GRA methods to optimize CFD analyses of ventilation performance in buildings10.1016/j.buildenv.2022.109587 ↗
36. Optimization of concrete containing waste crumb rubber mix design for thermal insulating applications using Taguchi method10.1016/j.conbuildmat.2024.136636 ↗
37. Rheology of alkali-activated materials: A review10.1016/j.cemconcomp.2021.104061 ↗
38. Development of high strength one-part geopolymer mortar using sodium metasilicate10.1016/j.conbuildmat.2019.117611 ↗
39. Effect of calcium-rich compounds on setting time and strength development of alkali-activated fly ash cured at ambient temperature
40. Fresh mechanical and durability properties of alkali-activated fly ash-slag concrete: a review10.1007/s41062-021-00711-w ↗
41. Effect of GGBFS on setting, workability and early strength properties of fly ash geopolymer concrete cured in ambient condition10.1016/j.conbuildmat.2014.05.080 ↗
42. Influence of activator Na2O concentration on residual strengths of alkali-activated slag mortar upon exposure to elevated temperatures
43. Effects of the curing regime, acid exposure, alkaline activator dosage, and precursor content on the strength development of mortar with alkali-activated slag and fly ash binder: a critical review
44. An overview of factors influencing the properties of alkali-activated binders10.1016/j.jclepro.2020.124972 ↗
45. ACI 318-05 · 2005
46. Eurocode 2 · 2004
47. Setting and mechanical properties of alkali-activated fly ash/slag concrete manufactured at room temperature10.1016/j.conbuildmat.2013.05.107 ↗
48. Engineering properties of inorganic polymer concretes (IPCs)10.1016/j.cemconres.2006.10.008 ↗
49. Magnesia modification of alkali-activated slag fly ash cement10.1007/s11595-011-0182-8 ↗
50. Development of an eco-friendly Ultra-High Performance Concrete (UHPC) with efficient cement and mineral admixtures uses10.1016/j.cemconcomp.2014.09.024 ↗
51. Mechanical properties of fly-ash-based geopolymer concrete
52. Flexural strength and elastic modulus of ambient-cured blended low-calcium fly ash geopolymer concrete10.1016/j.conbuildmat.2016.11.034 ↗
53. Multi-objective optimization of parameters affecting Organic Rankine Cycle performance characteristics with Taguchi-Grey Relational Analysis10.1016/j.rser.2019.109483 ↗
54. Improvement of early strength of fly ash-slag based one-part alkali activated mortar10.1016/j.conbuildmat.2020.118533 ↗
55. Preparation of cleaner one-part geopolymer by investigating different types of commercial sodium metasilicate in China10.1016/j.jclepro.2018.08.060 ↗
56. Study of seawater mixed one-part alkali activated GGBFS-fly ash10.1016/j.cemconcomp.2019.103484 ↗
57. Effect of fly ash characteristics on delayed high-strength development of geopolymers10.1016/j.conbuildmat.2015.10.172 ↗
58. Mix composition and characterisation of one-part geopolymers with different activators10.1016/j.conbuildmat.2019.07.083 ↗
59. Production of durable high-strength self-compacting geopolymer concrete with GGBFS as a precursor10.1007/s10163-023-01851-0 ↗
60. Upcycling end-of-life bricks in high-performance one-part alkali-activated materials
61. Role of slag in microstructural development and hardening of fly ash-slag geopolymer10.1016/j.cemconres.2012.10.004 ↗
62. Compatibility studies between N-A-S-H and C-A-S-H gels. Study in the ternary diagram Na2O–CaO–Al2O3–SiO2–H2O10.1016/j.cemconres.2011.05.006 ↗
63. Workability, autogenous shrinkage and microstructure of alkali-activated slag/fly ash slurries: effect of precursor composition and sodium silicate modulus
64. Microstructure and durability of alkali-activated materials as key parameters for standardization
65. Fly ash-slag interaction during alkaline activation: influence of activators on phase assemblage and microstructure formation10.1016/j.conbuildmat.2016.06.099 ↗
66. Analysis of theoretical carbon dioxide emissions from cement production: methodology and application10.1016/j.jclepro.2021.130270 ↗
67. Evaluation of environmental sustainability of one-part geopolymer binder concrete
68. Life cycle assessment of a new industrial process for sustainable construction materials
69. One-part eco-friendly alkali-activated concrete – an innovative sustainable alternative10.1016/j.conbuildmat.2023.133741 ↗
70. Efficient mix design of one-part alkali-activated concrete using packing density method and its optimization through Taguchi-GRA10.1016/j.conbuildmat.2024.136869 ↗