journal article·2019-06

Thermal analysis and Knudsen effusion mass spectrometry combined in a specially-adapted commercial skimmer coupled instrument (Netzsch)

Pavel Brož, František Zelenka, Jiří Sopoušek, Martina Hejduková, Tereza Kuběnová, Ondřej Zobač

Calphad· Volume 65
Publisher page

Abstract

Abstract The paper is aimed at informing on Netzsch STA 409 CD/3/403/5/G apparatus, a specially-adapted type of the commercial STA 409 CD - QMS 403/5 Skimmer Coupling Instrument combining methods of thermal analysis with Knudsen effusion mass spectrometry. Construction parameters as well as advantages and disadvantages of the instrument are presented. The instrument can be used for a broad spectrum of studies in materials field from which some of them, including e.g. thermodynamic and phase transformations studies, study of surface and catalytic processes, investigation of materials on multiscale level, are demonstrated. The new multifunction design as well as the instrument capabilities are discussed with respect to already published information.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Rare-earth and actinide compounds · Advanced Chemical Physics Studies · High-pressure geophysics and materials

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (16)

Show source-provided references
1. Modern methods of thermal analysis10.1080/10408348108085520 ↗
2. Combination of thermal analysis and Knudsen effusion mass spectrometry for study of metal materials on macro- and nano-scale10.1149/04601.0069ecst ↗
3. Specially-adapted type of Netzsch STA Instrument as a tool for Knudsen effusion mass spectrometry10.1016/j.ijms.2015.04.002 ↗
4. Die Gesetze der Molekularströmung und der inneren Reibungsströmung der Gase durch Röhren10.1002/andp.19093330106 ↗
5. Die Molekularströmung der Gase durch Öffnungen und die Effusion10.1002/andp.19093330505 ↗
6. High-temperature mass spectrometry: instrumental techniques, ionization cross-sections, pressure measurements, and thermodynamic data10.1351/pac200577040683 ↗
7. Ag-Cu colloid synthesis: bimetallic nanoparticle characterisation and thermal treatment10.1155/2014/638964 ↗
8. F. Zelenka, P. Broz, A. Styskalik, D. Skoda, O. Zobac, Study of surface effects on Ag-Cu nanoparticles by Knudsen effusion mass spectrometry, in: Proceedings of the NANOCON 2014, 6th International Conference, 2015, pp. 820–825.
9. Netzsch-Gerätebau, Thermal Properties of the Elements, 〈http://www.netzsch-thermal-analysis.com/en/literature-digital-media/literature/posters.html〉.
10. Hultgren · 1973
11. Corrected values for boiling points and enthalpies of vaporization of elements in handbooks10.1021/je1011086 ↗
12. Greenwood · 1997
13. Los Alamos National Laboratories, Periodic Table of Elements, 〈http://periodic.lanl.gov/70.shtml〉.
14. Lide · 1994
15. Holleman · 2007
16. The phase diagram of the Yb–Si system10.1016/S0925-8388(02)00809-5 ↗