Synthesis and thermal expansion of SrREE4(SiO4)3O apatites
Source abstract
Abstract
This article presents the results of the optimization of solid-phase synthesis of oxysilicates of the composition SrREE4(SiO4)3O (REE: La–Lu, except Ce, Pm, Tm, Yb) having the structure of apatite. The new synthesis technique allows for reducing the temperature of the final stage and avoiding impurities of REEO(OH) and REE2O2CO3 in the final product. The crystal structure of SrEu4(SiO4)3O (a = 9.50029(37) Å, c = 7.02540(31) Å, V = 549.130(49) Å3, R-Bragg = 2.721%) was refined for the first time. This is a study of the thermal expansion of compounds in the temperature range of 173–373 K. The effect of the internal periodicity of changes in the linear and volumetric coefficients of thermal expansion in a number of studied compounds was revealed.
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Research context
OpenAlex topics: Luminescence Properties of Advanced Materials · Crystal Structures and Properties · Inorganic Chemistry and Materials
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
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