journal article·2010-06

Synthesis and characterization of ternary compound, Mn2SnTe4

Gerzon E. Delgado, Asiloé J. Mora, Jines E. Contreras, Luis Betancourt

Bulletin of Materials Science· Volume 33· Issue 3
Publisher page

Abstract

Mn2SnTe4 was synthesized by direct fusion using the anneal method. X-ray powder diffraction analysis indicated that this material crystallizes in the olivine-type structure, space group Pnma, Z = 4, with unit cell parameters: a = 14.020(2) A, b = 8.147(1) A, c = 6.607(1) A, V = 754.7(2) A3. The Rietveld refinement converged to the figures of merit, Rp = 6.9%, Rwp = 8.5%, Rexp = 6.0%, χ2 = 2.0 and S = 1.4.
Source: openaire · Quality: candidate unverified · Source record ↗

Research context

OpenAlex topics: Inorganic Chemistry and Materials · X-ray Diffraction in Crystallography · Crystal Structures and Properties

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

References (20)

Show source-provided references
1. Boultif A and Löuer D 2004 J. Appl. Cryst. 37 72410.1107/S0021889804014876 ↗
2. Bragg W L and Brown G B 1926 Z. Kristallogr. 63 53810.1524/zkri.1926.63.1.538 ↗
3. Cagliotti G, Paoletti A and Ricci F P 1958 Nucl. Instrum. 3 22310.1016/0369-643X(58)90029-X ↗
4. Delgado J M 1998 Inst. Phys. Conf. Series 152 45
5. Delgado G E, Chacón C, Delgado J M and Sagredo V 1992 Phys. Status Solidi (a) 134 6110.1002/pssa.2211340103 ↗
6. Delgado G E, Mora A J, Marcano G and Rincón C 2008 Cryst. Res. Technol. 43 43310.1002/crat.200711049 ↗
7. Delgado G E, Betancourt L, Mora A J, Contreras J, Grima-Gallardo P and Quintero M 2009 Av. Quím. 4 710.53766/AVANQUIM/2009.04.01.01 ↗
8. Furdyna J K and Kossut J 1988 Diluted magnetic semiconductors, semiconductors and semimetals (eds) R K Willardson and A C Beer (New York: Academic Press), Chap. 1, Vol. 25
9. Henao J A, Delgado J M and Quintero M 1998 Powder Diffraction 13 19610.1017/S0885715600010101 ↗
10. ICSD 2008 Inorganic Crystal Structure Database (Set 2008-1), Gemlin Institute, Karlsruhe, Germany
11. Jumas J C, Philippot E and Maurin M 1977 Acta Crystallogr. B33 385010.1107/S0567740877012205 ↗
12. Lamarche G, Lamarche F and Lamarche A M 1994 Physica B219 194
13. McGuire M A, Scheidemantel T J, Badding J V and DiSalvo F J 2005 Chem. Mater. 17 618610.1021/cm0518067 ↗
14. Parthé E 1995 Intermetallic compounds, principles and applications (eds) J H Westbrook and R L Fleischer (Chichester, UK: John Wiley & Sons), Vol. 1
15. Rietveld H M 1969 J. Appl. Crystallogr. 2 6510.1107/S0021889869006558 ↗
16. Rodriguez-Carvajal J 2008 Fullprof, version 4.4, LLB, CEACNRS, France
17. Roisnel T and Rodriguez-Carvajal J 2001 Mater. Sci. Forum 378–381 11810.4028/www.scientific.net/MSF.378-381.118 ↗
18. Shannon R D 1976 Acta Crystallogr. A32 75110.1107/S0567739476001551 ↗
19. Vincent H, Bertaut E F, Baur W H and Shannon R D 1976 Acta Crystallogr. B32 174910.1107/S056774087600633X ↗
20. Wintenberger M and Jumas J C 1980 Acta Crystallogr. B36 199310.1107/S0567740880007789 ↗