journal article·2013-12

Structural characterization of electrodeposited boron

ASHISH JAIN, C GHOSH, T R RAVINDRAN, S ANTHONYSAMY, R DIVAKAR, E MOHANDAS, G S GUPTA

Bulletin of Materials Science· Volume 36· Issue 7
Publisher page

Abstract

Structural characterization of electrodeposited boron was carried out by using transmission electron microscopy and Raman spectroscopy. Electron diffraction and phase contrast imaging were carried out by using transmission electron microscopy. Phase identification was done based on the analysis of electron diffraction patterns and the power spectrum calculated from the lattice images from thin regions of the sample. Raman spectroscopic examination was carried out to study the nature of bonding and the allotropic form of boron obtained after electrodeposition. The results obtained from transmission electron microscopy showed the presence of nanocrystallites embedded in an amorphous mass of boron. Raman microscopic studies showed that amorphous boron could be converted to its crystalline form at high temperatures.
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Research context

OpenAlex topics: Boron and Carbon Nanomaterials Research · Ion-surface interactions and analysis · Diamond and Carbon-based Materials Research

SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.

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