Large scale synthesis and characterization of Ni nanoparticles by solution reduction method
Source abstract
Abstract
Ni nanoparticles were mass synthesized by solution reduction process successfully. The influence of the parameters on the particle size of Ni nanoparticles were studied and the referential process parameters were obtained. The morphology and structure of the synthesized Ni nanoparticles were characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD), Brunauer-Emmett-Teller (BET) surface area analysis and infrared spectroscopy (IR). The results show that Ni nanoparticles are of high purity and are covered by hydroxyethyl carboxymethyl cellulose (HECMC) layer and the mean size being about 31 nm. The magnetic measurement revealed that Ni nanoparticles are ferromagnetic.
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Research context
OpenAlex topics: Carbon Nanotubes in Composites · Chemical and Physical Properties of Materials · Copper-based nanomaterials and applications
SciVX discovery tags are terminology-based. OpenAlex topics are source-provided classifications.
References (19)
Show source-provided references
1. Degen A and Matek J 1999 NanoStruct. Mater. 12 22510.1016/S0965-9773(99)00104-X ↗
2. Hinotsu T, Jeyadevan B, Chinnasamy C N, Shinoda K and Tohji K 2004 J. Appl. Phys. 95 747710.1063/1.1688534 ↗
3. Hou Y L and Gao S 2004 J. Alloy. Compd. 365 11210.1016/S0925-8388(03)00651-0 ↗
4. Gray D E 1972 America institute of physics handbook (New York: McGraw-Hill Book Company)
5. Guo P S, Sun Z, Chen Y W and Zheng Z H 2006 Mater. Lett. 60 96610.1016/j.matlet.2005.10.079 ↗
6. Kumar D, Yarmolenko S, Sankar J, Narayan J, Zhou H and Tiwari A 2004 Compos. Part B-Eng. 35 14910.1016/j.compositesb.2003.08.002 ↗
7. La Mer V K and Dinegar R H 1950 J. Am. Chem. Soc. 72 484710.1021/ja01167a001 ↗
8. Liu Q, Liu H J, Liang Y Y, Xu Zh and Yin G 2006 Mater. Res. Bull. 41 69710.1016/j.materresbull.2005.10.013 ↗
9. Liu X S, Meridor U, Zhao P, Song G B, Frydmanc A and Gedanken A 2006 J. Magn. Magn. Mater. 301 1310.1016/j.jmmm.2005.06.009 ↗
10. Luo Zh S, Chen Ch L, Zhao D J, Luo Sh L and Li Zh Ch 2006 Chem. Phys. Lett. 421 58410.1016/j.cplett.2006.01.119 ↗
11. Ni X M, Su X B, Yang Z B and Zheng H G 2003 J. Cryst. Growth 252 61210.1016/S0022-0248(03)00954-0 ↗
12. Pfeil and Leonard B 1987 US Patent 4,673,430
13. Sun C Q 2003 Prog. Mater. Sci. 48 52110.1016/S0079-6425(03)00010-0 ↗
14. Swanson H E and Tatge E 1953 Nat. Bur. Stand. (US) Circ. 539 1 13
15. Syukri T Ban, Ohya Y and Takahashi Y 2003 Mater. Chem. Phys. 78 64510.1016/S0254-0584(02)00185-2 ↗
16. Törnqvist E, Adams E D, Copel M, Gustafsson T and Graham W R 1984 J. Vac. Sci. Technol. A2 93910.1116/1.572486 ↗
17. Wei Zh Q, Xia T D, Bai L F, Wang J, Wu Zh G and Yan P X 2006 Mater. Lett. 60 76610.1016/j.matlet.2005.10.008 ↗
18. Yu X F, Liu X, Zhang K and Hu Z Q 1999 J. Phys. Condens. Matter. 11 93710.1088/0953-8984/11/4/001 ↗
19. Zheng H G, Liang J H, Zeng J H and Qian Y T 2001 Mater. Res. Bull. 36 94710.1016/S0025-5408(01)00569-4 ↗