journal article·2014-01-27Open access

GC-MS Characterisation of Sapogenins from Sisal Waste and a Method to Isolate Pure Hecogenin

Jener David G. Santos, Alexsandro Branco

BioResources· Volume 9· Issue 1

Abstract

Five steroidal sapogenins (tigogenin, neotigogenina, hecogenin, gloriogenin, and dehydrohecogenin) were characterised by gas chromatography coupled with mass spectrometry (GC-MS) from a hydrolysed extract of sisal waste. In addition, pure hecogenin, an important raw material for the pharmaceutical industry, was obtained from this waste by selective liquid-liquid extraction of saponins with only hecogenin as aglycone, followed by acid hydrolysis. The yield of pure hecogenin was 460 mg.Kg-1 of sisal waste.
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Research context

OpenAlex topics: Phytochemical Studies and Bioactivities · Phytochemistry and Bioactive Compounds · Natural product bioactivities and synthesis

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